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Journal of Materials Science

Erschienen in:

07.05.2019 | Chemical routes to materials

3D conductive NiCo/NiCoO_x hybrid nanoclusters modified with amorphous FeOOH nanosheets for sensitive nonenzymatic glucose sensor

verfasst von: Duoming Wu, Zehua Zou, Xiaoying Lu, Kailu Guo, Nian Yang, Cailing Xu

Erschienen in: Journal of Materials Science | Ausgabe 15/2019

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Abstract

Developing a cost-effective electrocatalyst with high activity and excellent stability is very significant to nonenzymatic glucose detection. Herein, we have constructed 3D NiCo/NiCoO_x nanocluster electrode modified by amorphous FeOOH nanosheets owing to the similar electrocatalytic activity of FeOOH to natural peroxidases. The NiCo nanoclusters can provide an excellent conductivity and high active surface areas, while the amorphous two-dimensional ultrathin structure of FeOOH stimulates more open metal sites for glucose oxidation. Besides, the strong synergetic effects among ternary Fe, Ni and Co are beneficial to the transport of charge. Though comprehensive electrochemical measurements, it is found that the as-prepared electrode possesses the prominent activity toward glucose oxidation with high sensitivity of 7138 µA mM⁻¹ cm⁻², a wide linear range of 1 µM and 8 mM, a low detection limit of 0.82 µM, good selectivity and excellent stability, all of which is mainly derived from the more active sites, rapid mass transport and superior electron transfer. This research provides a model system for developing more available electrocatalysts for glucose detection.

Vorheriger Artikel Hydrogel-coated Fe3O4 nanoparticles as an efficient heterogeneous Fenton catalyst for degradation of phenol

Nächster Artikel Microneedle array sensors based on carbon nanoparticle composites: interfacial chemistry and electroanalytical properties

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Titel: 3D conductive NiCo/NiCoOx hybrid nanoclusters modified with amorphous FeOOH nanosheets for sensitive nonenzymatic glucose sensor
verfasst von: Duoming Wu
Zehua Zou
Xiaoying Lu
Kailu Guo
Nian Yang
Cailing Xu
Publikationsdatum: 07.05.2019
Verlag: Springer US
Erschienen in: Journal of Materials Science / Ausgabe 15/2019
Print ISSN: 0022-2461
Elektronische ISSN: 1573-4803
DOI: https://doi.org/10.1007/s10853-019-03662-x

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