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Topics in Catalysis

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21.08.2018 | Original Paper

A Novel Raman Setup Based on Magnetic-Driven Rotation of Sample

verfasst von: Matteo Signorile, Francesca Bonino, Alessandro Damin, Silvia Bordiga

Erschienen in: Topics in Catalysis | Ausgabe 14/2018

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Abstract

The Raman characterization of catalysts (as for any material) is generally a difficult task, since the numerous drawbacks affecting this technique, e.g. overlapping with photoemission phenomena and excitation induced sample damaging. These side effects are detrimental toward advanced applications of Raman spectroscopy, as in situ and/or operando ones. If photoemission can be often avoided by changing the excitation wavelength, the sample damaging requires to take advantage of specific tools, developed ad hoc. The aim of this work is to show the potentialities of a novel Raman setup, specifically designed for the in situ study of catalytic materials, where the sample is moved by means of a magnetic-driven sample-holder, reducing the excitation induced damaging to a negligible extent. Various examples related to catalysis field (involving inorganic, organic and mixed systems) are reported to support this statement.

Vorheriger Artikel Continuous Wave and Pulse EPR Characterization of Open-Shell Ti3+ Ions Generated in Hybrid SiO2–TiO2 Monoliths

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Titel: A Novel Raman Setup Based on Magnetic-Driven Rotation of Sample
verfasst von: Matteo Signorile
Francesca Bonino
Alessandro Damin
Silvia Bordiga
Publikationsdatum: 21.08.2018
Verlag: Springer US
Erschienen in: Topics in Catalysis / Ausgabe 14/2018
Print ISSN: 1022-5528
Elektronische ISSN: 1572-9028
DOI: https://doi.org/10.1007/s11244-018-1033-z

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