Skip to main content
Erschienen in: Wood Science and Technology 1-2/2009

01.02.2009 | Original

A portable NMR sensor for moisture monitoring of wooden works of art, particularly of paintings on wood

verfasst von: L. Senni, C. Casieri, A. Bovino, M. C. Gaetani, F. De Luca

Erschienen in: Wood Science and Technology | Ausgabe 1-2/2009

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

It is proposed the use of a mobile device based on a NMR single-sided sensor for in situ non-invasive determination of the moisture content (MC) of wood items, especially items of Cultural Heritage interest. The MC is obtained through the moisture volume fraction, which is an appropriate quantity for the sensor and corresponds to the fraction of its measurements sensitive volume occupied by water. The device has been used here to track changes in MC of wood specimens caused by changes over time of the environmental relative humidity. The kinetics of water adsorption has been related to results obtained with the gravimetric method. Measurements on an old painting, the Pietà (1516–1517), oil on a poplar wood panel by Sebastiano del Piombo (1485 Venice, 1547 Rome), Civic Museum, Viterbo, Italy, have shown, conclusively, the good sensitivity of the sensor and its capability to behave as a non-invasive and in situ utilizable device. Results of in situ painting measurements show that the NMR sensor can track moisture fluctuations that are outside the sensitivity range and precision of electro-hygrometric approach.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Literatur
Zurück zum Zitat Almeida G, Gagne S, Hernandez RE (2006) A NMR study of water distribution in hardwoods at several equilibrium moisture contents. Wood Sci Technol 41:293–307CrossRef Almeida G, Gagne S, Hernandez RE (2006) A NMR study of water distribution in hardwoods at several equilibrium moisture contents. Wood Sci Technol 41:293–307CrossRef
Zurück zum Zitat Anferova S, Anferov V, Adams M, Blumler P, Routley N, Hailu K, Kupferschlager K, Mallett MJD, Schroeder G, Sharma S, Blumich B (2002) Construction of a NMR-MOUSE with short dead time. Concept Magn Reson 15:15–25CrossRef Anferova S, Anferov V, Adams M, Blumler P, Routley N, Hailu K, Kupferschlager K, Mallett MJD, Schroeder G, Sharma S, Blumich B (2002) Construction of a NMR-MOUSE with short dead time. Concept Magn Reson 15:15–25CrossRef
Zurück zum Zitat Appelt S, Häsing FW, Kühn H, Perlo J, Blümich B (2005) Mobile high resolution xenon nuclear magnetic resonance spectroscopy in the earth’s magnetic field. Phys Rev Lett 94:197602.1–197602.4CrossRef Appelt S, Häsing FW, Kühn H, Perlo J, Blümich B (2005) Mobile high resolution xenon nuclear magnetic resonance spectroscopy in the earth’s magnetic field. Phys Rev Lett 94:197602.1–197602.4CrossRef
Zurück zum Zitat Araujo CD, MacKay AL, Hailey JRT, Whittall KP, Le H (1992) Proton magnetic resonance techniques for characterization of water in wood. Wood Sci Technol 26:101–113CrossRef Araujo CD, MacKay AL, Hailey JRT, Whittall KP, Le H (1992) Proton magnetic resonance techniques for characterization of water in wood. Wood Sci Technol 26:101–113CrossRef
Zurück zum Zitat Borgia GC, Brown RJS, Fantazzini P (1998) Uniform-penalty inversion of multiexponential decay data. J Magn Reson 132:65–77PubMedCrossRef Borgia GC, Brown RJS, Fantazzini P (1998) Uniform-penalty inversion of multiexponential decay data. J Magn Reson 132:65–77PubMedCrossRef
Zurück zum Zitat Bortolotti V, Camaiti M, Casieri C, De Luca F, Fantazzini P, Terenzi C (2006) Water absorption kinetics in different wettability conditions studied at pore and sample scales in porous media by NMR with portable single-sided and laboratory imaging devices. J Magn Reson 181:287–295PubMedCrossRef Bortolotti V, Camaiti M, Casieri C, De Luca F, Fantazzini P, Terenzi C (2006) Water absorption kinetics in different wettability conditions studied at pore and sample scales in porous media by NMR with portable single-sided and laboratory imaging devices. J Magn Reson 181:287–295PubMedCrossRef
Zurück zum Zitat Bowyer JL, Shmulsky R, Haygreen JG (2003) Forest products and wood science (2007), 5th edn. Blackwell Publishing, Ames Bowyer JL, Shmulsky R, Haygreen JG (2003) Forest products and wood science (2007), 5th edn. Blackwell Publishing, Ames
Zurück zum Zitat Camaiti M, Casieri C, De Luca F, Fantazzini P, Terenzi C (2007) The use of portable single-sided relaxometry and laboratory imaging NMR devices in stone conservation. Stud Conserv 52:39–47 Camaiti M, Casieri C, De Luca F, Fantazzini P, Terenzi C (2007) The use of portable single-sided relaxometry and laboratory imaging NMR devices in stone conservation. Stud Conserv 52:39–47
Zurück zum Zitat Casieri C, Senni L, Romagnoli M, Santamaria U, De Luca F (2004) Determination of moisture fraction in wood by mobile NMR device. J Magn Reson 171:363–372 Casieri C, Senni L, Romagnoli M, Santamaria U, De Luca F (2004) Determination of moisture fraction in wood by mobile NMR device. J Magn Reson 171:363–372
Zurück zum Zitat Casieri C, De Luca F, Fantazzini P (2005) Pore-size evaluation by single-sided nuclear magnetic resonance measurements: compensation of water self-diffusion effect on transverse relaxation. J Appl Phys 97:043901.1–043901.10 Casieri C, De Luca F, Fantazzini P (2005) Pore-size evaluation by single-sided nuclear magnetic resonance measurements: compensation of water self-diffusion effect on transverse relaxation. J Appl Phys 97:043901.1–043901.10
Zurück zum Zitat Cignini R, Melzi R, Tedoldi F, Casieri C, De Luca F (2006) Large surface mapping by unilateral NMR scanner. Magn Reson Imaging 24:813–818PubMed Cignini R, Melzi R, Tedoldi F, Casieri C, De Luca F (2006) Large surface mapping by unilateral NMR scanner. Magn Reson Imaging 24:813–818PubMed
Zurück zum Zitat Eidmann G, Savelsberg R, Blümler P, Blümich B (1996) The NMR MOUSE, a mobile universal surface explorer. J Magn Reson 122:104–109 Eidmann G, Savelsberg R, Blümler P, Blümich B (1996) The NMR MOUSE, a mobile universal surface explorer. J Magn Reson 122:104–109
Zurück zum Zitat Einspahr DW, Benson MK, Peckham JR (1967) Wood property variation in Populus. In: Proceedings of the Lake States Tree improvement conference. US Department of Agriculture, Forest Service Research Paper NC-23 Einspahr DW, Benson MK, Peckham JR (1967) Wood property variation in Populus. In: Proceedings of the Lake States Tree improvement conference. US Department of Agriculture, Forest Service Research Paper NC-23
Zurück zum Zitat Fechete R, Demco DE, Blumich B (2003) Order parameters of the orientation distribution of collagen fibers in Achilles tendon by H-1 NMR of multipolar spin states. NMR Biomed 16:479–483PubMed Fechete R, Demco DE, Blumich B (2003) Order parameters of the orientation distribution of collagen fibers in Achilles tendon by H-1 NMR of multipolar spin states. NMR Biomed 16:479–483PubMed
Zurück zum Zitat Maunu SL (2002) NMR studies of wood and wood products. Prog Nucl Magn Res Sp 40:151–174CrossRef Maunu SL (2002) NMR studies of wood and wood products. Prog Nucl Magn Res Sp 40:151–174CrossRef
Zurück zum Zitat Meiboom S, Gill D (1958) Modified spin-echo method for measuring nuclear relaxation times. Rev Sci Instrum 29:688–691CrossRef Meiboom S, Gill D (1958) Modified spin-echo method for measuring nuclear relaxation times. Rev Sci Instrum 29:688–691CrossRef
Zurück zum Zitat Menon RS, MacKay AL, Hailey JRT, Bloom M, Burgess AE, Sawnson JS (1987) An NMR determination of the physiological water distribution in wood during drying. J Appl Polym Sci 33:1141–1155CrossRef Menon RS, MacKay AL, Hailey JRT, Bloom M, Burgess AE, Sawnson JS (1987) An NMR determination of the physiological water distribution in wood during drying. J Appl Polym Sci 33:1141–1155CrossRef
Zurück zum Zitat Perlo J, Casanova F, Blümich B (2005) Velocity imaging by ex situ NMR. J Magn Reson 173:254–258PubMedCrossRef Perlo J, Casanova F, Blümich B (2005) Velocity imaging by ex situ NMR. J Magn Reson 173:254–258PubMedCrossRef
Zurück zum Zitat Perlo J, Casanova F, Blumich B (2007) Ex situ NMR in highly homogeneous fields: H-1 spectroscopy. Science 315:1110–1112PubMedCrossRef Perlo J, Casanova F, Blumich B (2007) Ex situ NMR in highly homogeneous fields: H-1 spectroscopy. Science 315:1110–1112PubMedCrossRef
Zurück zum Zitat Reeb JE (1995) Wood and moisture relationships. Oregon State University Bulletin EM8600 Reeb JE (1995) Wood and moisture relationships. Oregon State University Bulletin EM8600
Zurück zum Zitat Rowell RM, Barbour RJ (1989) Archaeological wood: properties, chemistry and preservation. Advances in chemistry series 225. American Chemical Society, Washington DC Rowell RM, Barbour RJ (1989) Archaeological wood: properties, chemistry and preservation. Advances in chemistry series 225. American Chemical Society, Washington DC
Zurück zum Zitat Simpson WT (1993) Specific gravity, moisture content, and density relationship for wood. US Department of Agriculture, Forest Service, Forest Products Laboratory Gen Tech Rep FPL-GTR-76 Simpson WT (1993) Specific gravity, moisture content, and density relationship for wood. US Department of Agriculture, Forest Service, Forest Products Laboratory Gen Tech Rep FPL-GTR-76
Zurück zum Zitat Skaar C (1988) Wood-water relations. Springer, Berlin Skaar C (1988) Wood-water relations. Springer, Berlin
Zurück zum Zitat Torgovnikov GI (1993) Dielectric properties of wood and wood-based materials. Series in wood science. Springer, Berlin Torgovnikov GI (1993) Dielectric properties of wood and wood-based materials. Series in wood science. Springer, Berlin
Zurück zum Zitat Viola I, Bubici S, Casieri C, De Luca F (2004) The codex major of the Collectio Altaempsiana: a non-invasive NMR study of paper. J Cult Herit 5:257–261CrossRef Viola I, Bubici S, Casieri C, De Luca F (2004) The codex major of the Collectio Altaempsiana: a non-invasive NMR study of paper. J Cult Herit 5:257–261CrossRef
Zurück zum Zitat Watson AT, Chang CTP (1997) Characterizing porous media with NMR methods. Prog Nucl Mag Res Sp 31:343–386CrossRef Watson AT, Chang CTP (1997) Characterizing porous media with NMR methods. Prog Nucl Mag Res Sp 31:343–386CrossRef
Zurück zum Zitat Wood Handbook: US Department of Agriculture (1987) Wood as an engineering material. Agriculture Handbook 72. Washington DC Wood Handbook: US Department of Agriculture (1987) Wood as an engineering material. Agriculture Handbook 72. Washington DC
Metadaten
Titel
A portable NMR sensor for moisture monitoring of wooden works of art, particularly of paintings on wood
verfasst von
L. Senni
C. Casieri
A. Bovino
M. C. Gaetani
F. De Luca
Publikationsdatum
01.02.2009
Verlag
Springer-Verlag
Erschienen in
Wood Science and Technology / Ausgabe 1-2/2009
Print ISSN: 0043-7719
Elektronische ISSN: 1432-5225
DOI
https://doi.org/10.1007/s00226-008-0200-y

Weitere Artikel der Ausgabe 1-2/2009

Wood Science and Technology 1-2/2009 Zur Ausgabe

Editorial

Editorial