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Journal of Materials Science
Erschienen in: Journal of Materials Science 4/2018

12.10.2017 | Metals

A whole pattern iterative refinement method for powder X-ray diffraction spectra of two-phase coherent alloys

verfasst von: P. A. Ferreirós, G. H. Rubiolo

Erschienen in: Journal of Materials Science | Ausgabe 4/2018

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Abstract

An iterative refining method using FullProf software (Rietveld refinement) as a multi-input–output black-box with cyclic feedback is proposed in order to accurately measure the lattice misfit in two-phase coherent alloys. The method uses two X-ray diffraction spectra taken on the same powder sample. In addition, it requires the volumetric fraction of the phases and the size of the crystallite in the precipitated phase as derived from the measurements made by the transmission electron microscopy–energy dispersive spectroscopy technique. The measurement of the lattice misfit in a Fe2AlV-strengthened ferritic Fe76Al12V12 alloy is shown as an application of the method.
Vorheriger Artikel Theoretical investigations of group IV alloys in the Lonsdaleite phase
Nächster Artikel Electroless Ni–P alloys on nanoporous ATO surface of Ti substrate

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Metadaten
Titel
A whole pattern iterative refinement method for powder X-ray diffraction spectra of two-phase coherent alloys
verfasst von
P. A. Ferreirós
G. H. Rubiolo
Publikationsdatum
12.10.2017
Verlag
Springer US
Erschienen in
Journal of Materials Science / Ausgabe 4/2018
Print ISSN: 0022-2461
Elektronische ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-017-1682-5

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