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01.09.2014 | Original Article | Ausgabe 6/2014

Environmental Earth Sciences 6/2014

Alteration kinetics of natural stones due to sodium sulfate crystallization: can reality match experimental simulations?

Zeitschrift:
Environmental Earth Sciences > Ausgabe 6/2014
Autoren:
Teresa Diaz Gonçalves, Vânia Brito
Wichtige Hinweise

Electronic supplementary material

The online version of this article (doi:10.​1007/​s12665-014-3085-0) contains supplementary material, which is available to authorized users.

Abstract

Salt decay is a very destructive mechanism that affects frequently the porous building materials of our architectural heritage. Sodium sulfate is one of the salts found in this context. It usually demonstrates high destructive power in salt crystallization tests because it can crystallize not only during evaporative processes but also when the temperature drops or when the salt solution comes into contact with pre-existing crystals. However, the use of extreme temperatures or successive wet/dry cycles also makes these tests unrepresentative of reality. To verify whether sodium sulfate can also be so destructive in field conditions, we have performed crystallization tests consisting of a single isothermal drying event. Three natural stones, relevant for the architectural heritage, were used for the purpose: Bentheimer sandstone, Ançã limestone, and a current Portuguese limestone of low porosity. The stones gave rise to distinct salt decay patterns: efflorescence, multilayer delamination and unilayer delamination, respectively. These morphological alterations were characterized at the micrometer scale by a new method based on what we have called the alteration kinetics curve. Such curve is calculated from topographic profiles obtained by a non-contact optical technique. The multilayer and unilayer delamination decay were also monitored by time-lapse photography. The work led us to conclude that sodium sulfate can indeed be also very destructive in field-representative conditions. Moreover, it showed that the optical method can be a valuable aid in the development of more realistic salt crystallization tests.

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Zusatzmaterial
Supplementary material 1 (AVI 29388 kb)
12665_2014_3085_MOESM1_ESM.avi
Supplementary material 2 (AVI 70933 kb)
12665_2014_3085_MOESM2_ESM.avi
Supplementary material 3 (MP4 10040 kb)
Supplementary material 4 (AVI 60800 kb)
12665_2014_3085_MOESM4_ESM.avi
Supplementary material 5 (MP4 7916 kb)
Supplementary material 6 (MP4 4058 kb)
Literatur
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