Preparation of Zirconium and Hafnium Metals by Bomb Reduction of Their Fluorides

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© 1957 ECS - The Electrochemical Society
, , Citation O. N. Carlson et al 1957 J. Electrochem. Soc. 104 51 DOI 10.1149/1.2428495

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1 Institute for Atomic Research and Department of Chemistry, Iowa State College, Ames, Iowa

Dates

  1. Received 23 February 1956

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1945-7111/104/1/51

Abstract

A bomb process for preparing Zr and Hf metals with Ca by the reduction of their tetrafluorides is described. A detailed method of preparing the high purity tetrafluorides is presented, and the purity and physical properties of the metals obtained are discussed.

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