Skip to main content

Part of the book series: Ellis Horwood Series in Food Science and Technology ((EHSFST))

  • 518 Accesses

Abstract

Amino acid analysis is a very important area in food science because nine amino acids are essential components of the diet, namely histidine, isoleucine, leucine, lysine, methionine, phenylalanine, threonine, tryptophan and valine. In addition, the amino acid composition of proteins is an important aspect of the characterization of proteins, and free amino acids are of significance in the flavour of some foods e.g. cheese (Wood et al., 1985).

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 39.99
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 54.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

Similar content being viewed by others

References

  • Abdel-Moety, E. M. (1988). First-derivative spectrophotometric and GLC determination of caffeine in foods and pharmaceuticals. Zeitschrift fur Lebensmittel-Untersuchung und Forschung, 186 (5) 412–416.

    Article  Google Scholar 

  • Anderson, R. J. and Hall, R. C. (1980). Hall bipolar pulse, differential electrolytic conductivity detector for GC: design and applications. Am. Lab., 12, 108–124.

    Google Scholar 

  • Bankhead, R. R., Weingartner, K. E., Kuntz, D. A. and Erdman, J. W. (1978). Effects of sodium bicarbonate blanch on the retention of micronutrients in soy beverage. J. Food Sci., 43, 345–348.

    Article  Google Scholar 

  • Bayer, E. (1958). In Gas Chromatography 1958, D. H. Desty (ed), Butterworths Scientific, London, pp. 333.

    Google Scholar 

  • Buser, W. and Erbersdopler, H. F. (1984). Determination of lysinoalanine as the heptafluorobutyryl isobutyl ester derivative by GLC. J. Chromatogr., 303, 234–237.

    Article  Google Scholar 

  • Fazio, T., Damico, J., Howard, J. W., White, R. H. and Watts, J. (1971). Gas chromatographic determination and mass spectrometric confirmation of Nnitrosodimethylamine in smoke processed marine fish. J. Agric. Food Chem., 19, 250–253.

    Article  Google Scholar 

  • Fine, D. H., Lieb, D. and Rufeh, F. (1975). Principle of operation of the thermal energy analyzer for the trace analysis of volatile and non-volatile N-nitroso compounds. J. Chromatogr., 107, 351–357.

    Article  Google Scholar 

  • Frank, H., Nicholson, G. J. and Bayer, E. (1977). Rapid gas chromatographic separation of amino acid enantiomers with a novel chiral stationary phase. J. Chromatogr. Sci, 15, 174–176.

    Google Scholar 

  • Frank, H., Rettenmeier, A., Weicker, H., Nicholson, G. J. and Bayer, E. (1980). A new gas chromatographic method for determination of amino acid levels in human serum. Clin. Chim. Acta, 105, 201–211.

    Article  Google Scholar 

  • Funazo, K., Tanaka, M. and Shono, T. (1979). Analysis of nitrite ion in water by electron capture gas chromatography. Chem. Lett., 309–310.

    Google Scholar 

  • Funazo, K., Tanaka, M. and Shono, T. (1980). Determination of nitrite at parts-perbillion levels by derivatization and electron capture gas chromatography. Anal. Chem., 52, 1222–1224.

    Article  Google Scholar 

  • Gavinelli, M., Airoldi, L. and Fanelli, R. (1986). A new method for quantitative analysis of volatile nitrosamines in food by simultaneous distillation-extraction. J. High Resolut. Chromatogr. Chromatogr. Commun., 9 (4), 257–259.

    Article  Google Scholar 

  • Gehrke, C. W. and Leimer, K. (1970). Trimethylsilylation of amino acids. Effect of solvents on derivatization using bis-(trimethylsilyl) trifluoroacetamide. J. Chromatogr., 53, 201-208.

    Google Scholar 

  • Gough, T. A. and Sugden, K. (1973). A study of the stability of a nitrogen-selective thermionic detector. J. Chromatogr., 86, 65–71.

    Article  Google Scholar 

  • Gough, T. A., Webb, K. S. and Eaton, R. F. (1977). Simple chemiluminescent detector for the screening of foodstuffs for the presence of volatile nitrosamines. J. Chromatogr., 137, 293–303.

    Article  Google Scholar 

  • Hasegawa, K. and Okamoto, N. (1980). Studies on the gas chromatographic analysis of lysinoalanine in alkali-treated food proteins. Agric. Biol. Chem., 44, 649–655.

    Article  Google Scholar 

  • Hasegawa, K., Mukai, K., Gothoh, M., Honjo, S. and Matoba, T. (1987). Determination of the lysinoalanine content in commercial foods by gas chromatography —selected ion monitoring. Agric. Biol. Chem., 51 (11), 2889–2894.

    Article  Google Scholar 

  • Heaney, R. K. & Fenwick, G. R. (1980). The analysis of glucosinolates in Brassica species using gas chromatography. Direct determination of the thiocyanate ion precursors, glucobrassicin and neoglucobrassicin. J. Sci. Food Agric., 31, 593–599.

    Article  Google Scholar 

  • Hunter, I. R., Dimick, K. P. and Corse, J. W. (1956). Determination of amino acids by ninhydrin oxidation and gas chromatography. Separation of leucine and isoleucine. Chem. Ind., 16, 294–295.

    Google Scholar 

  • Husek, P. and Macek, K. (1975). Gas chromatography of amino acids. J. Chromatogr., 113, 139–230.

    Article  Google Scholar 

  • Ishida, H. Sekine, H., Kimura, S. and Sekiya, S. (1986). Gas chromatographic determination of theobromine in foods. J. Food Hygienic Soc. of Japan,27(1), 75–80. (Food Science and Technology Abstracts (1987), 6K.10).

    Google Scholar 

  • Klatsmanyi, J. and Zala, P. (1982). Gas chromatographic determination of the quinine content of tonic beverages. Elelmiszervizsgalati—Kozlernenyek,28(1/2), 49–53. (Food Science and Technology Abstracts (1984) 8H1680).

    Google Scholar 

  • Koenig, W. A. (1985). Analysis of peptide antibiotics by glass capillary GC—MS. In Glass capillary chromatography in clinical medicine and pharmacology, Jaeger, H. (ed.), Marcel Dekker Inc., New York, p. 551.

    Google Scholar 

  • McGregor, D. I. Mullin, W. J. and Fenwick, G. R. (1983). Analytical methodology for determining glucosinolate composition and content. J. Assoc. Off. Anal. Chem., 66(4), 826–849.

    Google Scholar 

  • Mackenzie, S. L. and Tenaschuk, D. (1979). Quantitative formation of N(O,S)heptafluorobutyryl isobutyl amino acids for GC analysis. J. Chromatogr., 171, 195–209.

    Article  Google Scholar 

  • Masters, P. M. and Friedman, M. (1979). Racemization of amino acids in alkali-treated food proteins. J. Agric. Food Chem., 27, 507–511.

    Article  Google Scholar 

  • Moodie, I. A. (1981). Gas—liquid chromatography of amino acids. The heptafluoro- butyryl—isobutyl ester derivative of tryptophan. J. Chromatogr., 208, 60–66.

    Article  Google Scholar 

  • Olsen, O. and Sorensen, H. (1979). Isolation of glucosinolates and the identification of 0(a-L-rhamnopyranosyloxy) benzylglucosinolate from Reseda odorata. Phytochem. 18, 1547–1552.

    Article  Google Scholar 

  • Olsen, O. and Sorensen, H. (1980). Sinalbin and other glucosinolates in seeds of double low rape species and Brassica napus cv Bronowski. J. Agric. Food Chem., 28, 43–48.

    Article  Google Scholar 

  • Osterdahl, B. G. (1983). Volatile N-nitrosamines in beer and other alcoholic beverages. Var Foda, 35 (5), 221–230.

    Google Scholar 

  • Palframan, J. F., MacNab, J. and Crosby, N. T. (1973). An evaluation of the alkali flame ionization detector and the Coulson electrolytic detector in the analysis of N-nitrosamines in food. J. Chromatogr., 76, 307–319.

    Article  Google Scholar 

  • Pearce, R. J. (1977). Amino acid analysis by GLC of N-heptafluorobutyryl isobutyl esters. J. Chromatogr., 136, 113–126.

    Article  Google Scholar 

  • Rhoades, J. W. and Johnson, D. E. (1970). Gas chromatography and selective detection of N-nitrosamines. J. Chromatogr. Sci., 8, 616–617.

    Google Scholar 

  • Riedmann, M. (1974). Gaschromatographisches Screening von Nitrosaminen in Lebensmitteln mit den Stickstoff-Flamnenionisations detektor. J. Chromatogr., 88, 376–381.

    Article  Google Scholar 

  • Ross, H. D. and Hotchkiss, J. H. (1985). Determination of nitrate in dried foods by GC-thermal energy analyzer. J. Assoc. Offic. Anal. Chem., 68 (1), 41–43.

    Google Scholar 

  • Rucka, I., Kocan, A. and Madaric, A. (1985). Determination of N-nitrosodimethylamine in brewers malt and beer by gas chromatography-mass spectrometry. Bulletin Potravinarskeho Vyskumu,24(2/3), 105–111. (Food Science and Technology Abstracts (1986), 3H139.)

    Google Scholar 

  • Sasakawa, K. and Kato, T. (1985). Determination of piperine in seasoned meat by gas chromatography. Reports of the Central Customs Laboratory, 25, 19–24. (Food Science and Technology Abstracts (1987), 8S13.)

    Google Scholar 

  • Siezen, P. J. and Mague, T. H. (1977). GLC of the N-heptafluorobutyryl isobutyl esters of fifty biologically interesting amino acids. J. Chromatogr., 130, 151–160.

    Article  Google Scholar 

  • Song, P. J. and Hu, J. F. (1988). N-Nitrosamines in Chinese foods. Food and Chem.Toxicol. 26 (3), 205–208.

    Article  Google Scholar 

  • Sosulski, F. W. and Dabrowski, K. J. (1984). Determination of glucosinolates in canola meal and protein products by desulphation and capillary gas-liquid chromatography. J. Agric. Food Chem., 32 (5), 1172–1175.

    Article  Google Scholar 

  • Tanaka, A., Nose, N. and Watanabe, A. (1980). Gas chromatographic determination of nitrite in foods as trimethylsilyl derivative of 1H-benzotriazole. J. Chrotnatogr., 194, 21–31.

    Article  Google Scholar 

  • Tanaka, A., Nose, N., Yamada, F., Saito, S. and Watanabe, A. (1981). Determination of nitrite in human, cow and market milks by GLC and electron-capture detection. J. Chromatogr., 206, 531–540.

    Article  Google Scholar 

  • Thies, W. (1979). Detection and utilization of a glucosinolate sulfohydrolase in the edible snail, Helix pomatia. Die Naturwissenschaften 66, 364–365.

    Article  Google Scholar 

  • Truscott, R. J. W., Minchinton, I. R., Burke, D. G. & Sang, J. P. (1982). A novel methoxyindole glucosinolate. Biochem. Biophys. Res. Commun., 107, 1368–1375.

    Article  Google Scholar 

  • van Etten, C. H., Daxenbichler, M. E., Williams, P. H. and Kwolek. W. F. (1976). Glucosinolate and derived products in cruciferous vegetables. Analysis of the edible part from twenty-two varieties of cabbage. J. Agric. Food Chem., 24(3), 452–455.

    Google Scholar 

  • Vitzthum, O., Barthels, M. and Kwasny, H. (1974). Rapid gas-chromatographic determination of caffeine in caffeine-containing and decaffeinated coffees with the nitrogen-sensitive detector. Z. Lebensm. Unters. Forsch. 154, 135–141.

    Article  Google Scholar 

  • Weerasinghe, D. K., Fernando, R. S. and Chandradasa, P. B. (1982). A convenient rapid estimation of caffeine in tea. Tea Quarterly, 51 (4), 175–179.

    Google Scholar 

  • Wood, A. F., Aston, J. W. and Douglas, G. K. (1985). The determination of free amino acids in cheese by capillary column gas-liquid chromatography. Aust. J. Dairy Technol. 40, 166–169.

    Google Scholar 

  • Wu, W. S. and Saschenbrecker, P. W. (1977). Nitration of benzene as method for determining nitrites and nitrates in meat and meat products. J. Assoc. Offic. Anal. Chem. 60, 1137–1141.

    Google Scholar 

  • Wu, H.-L. Chen, S.-H., Lin, S.-J., Hwang, W.-R., Funazo, K., Tanaka, M. and Shono, T. (1983). Gas chromatographic determination of inorganic anions as pentafluorobenzyl derivatives. J. Chromatogr.,269 183–190.

    Google Scholar 

  • Wu, H., Chen, S., Funazo, K., Tanaka, M. and Shono, T. (1984). Electron-capture gas chromatographic determination of nitrite as the pentafluorobenzyl derivative. J. Chromatogr., 291, 409–415.

    Article  Google Scholar 

  • Zagalak, M. J., Curtis, H.-Ch., Leimbacher, W., Redweik, U. (1977). Quantitation of deuterated and non-deuterated phenylalanine and tyrosine in human plasma using the selective ion monitoring method with combined GC–MS. J. Chromatogr., 142, 523–531.

    Article  Google Scholar 

Download references

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 1990 Ellis Horwood Limited

About this chapter

Cite this chapter

Gordon, M.H. (1990). Amino acids and other nitrogen-containing compounds. In: Gordon, M.H. (eds) Principles and Applications of Gas Chromatography in Food Analysis. Ellis Horwood Series in Food Science and Technology. Springer, Boston, MA. https://doi.org/10.1007/978-1-4613-0681-8_6

Download citation

  • DOI: https://doi.org/10.1007/978-1-4613-0681-8_6

  • Publisher Name: Springer, Boston, MA

  • Print ISBN: 978-1-4612-8024-8

  • Online ISBN: 978-1-4613-0681-8

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics