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2020 | OriginalPaper | Buchkapitel

Design and Applications in Catalytic Processes of Zeolites Synthesized by the Hydrothermal Method

verfasst von : Patricia H. Y. Cordeiro, Heveline Enzweiler, Luiz Jardel Visioli, Cássio Henrique Zandonai, João Lourenço Castagnari Willimann Pimenta, Gimerson Weigert Subtil

Erschienen in: Emerging Research in Science and Engineering Based on Advanced Experimental and Computational Strategies

Verlag: Springer International Publishing

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Abstract

The zeolites are aluminosilicates with perfectly crystalline structure based on tetrahedral arrangements of silicon and aluminum. These materials present great potential for application in catalytic, adsorption and ion exchange processes. In addition, the zeolite crystallinity results in a highly stable material, with very organized micropores and network of channels. Zeolites have been widely used in chemical processes as heterogeneous catalysts, both in the research and development stage of technology and in applications already established in industry, such as the catalytic cracking of petroleum. The synthesis of this material occurs through the hydrothermal method, which consists on the steps of gel synthesis, crystallization at autogenous pressure, separation of the precipitated material and subsequent heat treatment to remove the structure directing agents. During preparation of the synthesis gel, the composition of the material to be generated can be changed, by varying the Si/Al ratio (important parameter for zeolites) or by incorporating other metals into the crystalline structure, for example. It is also possible to vary the amount of synthesis water, which changes the solubility of the medium and also the autogenous pressure in the subsequent phase. In the crystallization step, the time and temperature in which nucleation and crystal growth occurs can be manipulated, altering the size of the crystallites formed. Finally, in the heat treatment step, the textural properties and the crystallinity can be altered by modifying the temperature, heating rate and calcination time. The possibility of altering the physical-chemical properties of the zeolites makes them very versatile materials for application in catalysis, making it possible to obtain materials with characteristics close to the ideal for specific processes. In this sense, zeolitic materials have been used as catalysts with acidic activity (property generated in the material structure itself), as supports for certain active phases in chemical reactions and even as active supports in photochemical reactions. Therefore, the aim of this chapter is to discuss the synthesis of zeolites through the hydrothermal method, with a focus on the manipulation of the synthesis conditions and their consequences on the physicochemical properties and the implications for the applications in different catalytic processes.

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Zion Research : Zeolite (Natural and Synthetic) Market for Catalysts, adsorbents, Detergent Builders and Other Applications, Global Industry Perspective, Comprehensive Analysis, Size, Share, Growth, Segment, Trends and Forecast 2020. Acessado em 01 de setembro de 2019 (2015). https://www.marketresearchstore.com/news/global-zeolite-market-140

Titel: Design and Applications in Catalytic Processes of Zeolites Synthesized by the Hydrothermal Method
verfasst von: Patricia H. Y. Cordeiro
Heveline Enzweiler
Luiz Jardel Visioli
Cássio Henrique Zandonai
João Lourenço Castagnari Willimann Pimenta
Gimerson Weigert Subtil
Verlag: Springer International Publishing
Buch: Emerging Research in Science and Engineering Based on Advanced Experimental and Computational Strategies
Print ISBN: 978-3-030-31402-6

Electronic ISBN: 978-3-030-31403-3

Copyright-Jahr: 2020
DOI: https://doi.org/10.1007/978-3-030-31403-3_14

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