nach oben

Arabian Journal for Science and Engineering

Erschienen in:

22.01.2020 | Research Article-Chemistry

Determination of Trace Level Perchlorate in Seawater Using Dispersive Solid-Phase Extraction and Co-precipitation Extraction with Layered Double Hydroxides Followed by Ion Chromatography Analysis

verfasst von: Amayreh Mousa, Chanbasha Basheer, Mohanad Abdullah, Abdulrahman Al-Arfaj

Erschienen in: Arabian Journal for Science and Engineering | Ausgabe 6/2020

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config

KI-gestützte Suche

Aus

Abstract

In this manuscript, three-layered double hydroxides (LDH-CO₃²⁻, LDH-NO₃⁻, and LDH-Cl⁻) were synthesized and utilized as efficient sorbents for the extraction of perchlorate in water samples. Two different microextraction methods, namely dispersive solid-phase extraction (D-SPE) and co-precipitation extraction (Co-PE), were developed. Then performances of these methods were compared with previously reported in the literature. Analyses were performed using the ion chromatography (IC). The experimental conditions that affect the enrichment factor of the target analyte from the aqueous sample were investigated and optimized. The results showed (pH = 6) are the optimum for both methods. The Co-PE results demonstrated shorted extraction time (10 min) when compared to (20 min) D-SPE. After optimizing both methods, excellent linearity for the analyte in the range from 0.2 to 10 μg/L with coefficients of determination (r²) from 0.992 to 0.997 is obtained. The limits of detection were calculated based on a signal-to-noise (S/N) ratio of 3: For Co-PE, it was 0.04 μg/L, and for D-SPE, it was 0.06 μg/L. The limits of quantitation were calculated based on S/N of 10 and were 0.12 and 0.19 μg/L, respectively. Methods percentage relative standard deviations (n = 3), 2 for Co-PE and 2.2% for D-SPE were obtained. The relative recoveries (mean ± standard deviation, n = 3) of perchlorate from 5 µg/L spiked real seawater samples for the two extraction techniques D-SPE and Co-PE were between (89.5 and 102.3 ± 2–6.1%) and (86 to 99.8 ± 1.7–5.8%), respectively. The two extraction methods, coupled with IC, were used to the determination of perchlorate concentration in seawater samples from the different locations in Saudi Arabia. Overall, the D-SPE process demonstrated better analytical capability when compared to Co-SPE and other reported methods.

Vorheriger Artikel New Green Adsorbent for Capturing Carbon Dioxide by Choline Chloride:Urea-Confined Nanoporous Silica

Nächster Artikel Low-Cost Route for Preparing Carbon–Silica Composite Mesoporous Material from Coal Gasification Slag: Synthesis, Characterization and Application in Purifying Dye Wastewater

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

über 102.000 Bücher
über 537 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Finance + Banking
Management + Führung
Marketing + Vertrieb
Maschinenbau + Werkstoffe
Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

über 67.000 Bücher
über 390 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Maschinenbau + Werkstoffe

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Vogt, H.; Balej, J.; Bennett, J.E.; Wintzer, P.; Sheikh, S.A.; Gallone, P.; Pelin, K.: Chlorine Oxides and Chlorine Oxygen Acids, Ullmann’s Encyclopedia of Industrial Chemistry. Wiley-VCH, Weinheim (2002). https://doi.org/10.1002/14356007.a06_483.pub2 CrossRef

Feifei, C.; Jessy, J.; Patrick, O.; Benjamin, C.; Xavier, M.; Daniel, H.; Alain, D.; Nicolas, D.; Vincent, B.; Pierre, P.: Sources and behavior of perchlorate ions (ClO₄⁻) in chalk aquifer of Champagne–Ardenne, France: preliminary results. Proc. IAHS 379, 113–117 (2018). https://doi.org/10.5194/piahs-379-113-2018 CrossRef

Patrizia, I.; Oriana, M.; Rossella, T.; Maurizio, V.; Antonio, P.: Determination of perchlorate in bottled water from Italy. Water 5(2), 767–779 (2013). https://doi.org/10.3390/w5020767 CrossRef

Backus, S.M.; Klawuun, P.; Brown, S.; D’sa, I.; Sharp, S.; Surette, C.; Williams, D.J.: Determination of perchlorate in selected surface waters in the Great Lakes Basin by HPLC/MS/MS. Chemosphere 61(6), 834–843 (2005). https://doi.org/10.1016/j.chemosphere.2005.04.054 CrossRef

Draft Toxicological Profile for Perchlorates, prepared by Syracuse Research Corporation (Contact Vo. 200-2004-09793), for U.S. Department of Health and Human Services, Public Health Service, Agency for Toxic Substances and Disease Registry, September 2005

Rocio, A.R.; Zhiyun, J.; Jiping, Z.; Yong, L.F.: Application of pressure-assisted electrokinetic injection-tandem mass spectrometry in the determination of perchlorate in water and soil samples. Anal. Sci. 28(3), 231–236 (2012). https://doi.org/10.2116/analsci.28.231 CrossRef

Ozge, C.; Ben, B.; Liza, V.B.; Yigit, E.; Deniz, U.; Murat, A.; Abdurrahman, C.; Mustafa, S.; Ibrahim, U.; Aysel, O.: Perchlorate exposure through water and milk in Istanbul. Bull. Environ. Contam. Toxicol. 79, 439–445 (2016). https://doi.org/10.1007/s00128-016-1889-1 CrossRef

Sungur, S.; Kemal, S.M.: Ion chromatographic determination of perchlorate in foods consumed in Hatay region. Food Chem. 126(1), 326–331 (2011). https://doi.org/10.1016/j.foodchem.2010.10.068 CrossRef

Seiler, M.A.; Jensen, D.; Neist, U.; Deister, U.K.; Schmitz, F.: Determination of trace perchlorate in water: a simplified method for the identification of potential interferences. Environ Sci. Eur. 29, 1–9 (2017). https://doi.org/10.1186/s12302-017-0128-7) CrossRef

10.

Tian, K.; Dasgupta, P.K.; Anderson, T.A.: Determination of trace perchlorate in high-salinity water samples by ion chromatography with on-line preconcentration and preelution. Anal. Chem. 75(3), 701–706 (2003). https://doi.org/10.1021/ac026268l CrossRef

11.

Edward, T.U.: Perchlorate as an environmental contaminant. Environ. Sci. Pollut. Res. 9(3), 187–192 (2002). https://doi.org/10.1007/BF02987487 MathSciNetCrossRef

12.

Jianlin, Xu; Yanguang, S.; Booki, M.; Lisa, S.; Bruce, E.L.: Microbial degradation of perchlorate: principles and applications. Environ. Eng. Sci. 20(5), 405–422 (2004). https://doi.org/10.1089/109287503768335904 CrossRef

13.

Raul, C.; Paulina, P.; David, P.; Mauricio, E.: Capture and accumulation of perchlorate in lettuce. Effect of genotype, temperature, perchlorate concentration, and competition with anions. Chemosphere 111, 195–200 (2014). https://doi.org/10.1016/j.chemosphere.2014.03.027 CrossRef

14.

Karjalainen, T.: European Union-funded research on endocrine disrupters and underlying policy. In: Congenital Diseases and the Environment (Environmental Science and Technology Library), pp. 379–406. Springer (2007). https://link.springer.com/content/pdf/10.1007%2F1-4020-4831-9_17.pdf

15.

U.S. Environmental Protection Agency (USEPA), Announcement of the Draft Drinking Water Contaminant Candidate List Notice, EPA Number 815Z97003m (1997) 52193

16.

Leung, A.M.; Pearce, E.N.; Braverman, L.E.: Environmental perchlorate exposure: potential adverse thyroid effects. Curr. Opin. Endocrinol. Diabetes Obes. 21(5), 372–376 (2014)CrossRef

17.

Magnuson, M.L.; Urbansky, E.T.; Kelty, C.A.: Determination of perchlorate at trace levels in drinking water by ion-pair extraction with electrospray ionization mass spectrometry. Anal. Chem. 72(1), 25–29 (2000). https://doi.org/10.1021/ac9909204 CrossRef

18.

Carolyn, J.K.; Harry, R.B.; Rolf, H.: Analysis of perchlorate in groundwater by electrospray ionization mass spectrometry/mass spectrometry. Environ. Sci. Technol. 34(9), 1862–1864 (2000)CrossRef

19.

Wagner, H.P.; Pepich, B.V.; Pohl, C.; Later, D.; Joyce, R.; Srinivasan, K.; Thomas, D.; Woodruff, A.; Deborba, B.; Munch, D.J.: US Environmental Protection Agency Method 314.1, an automated sample preconcentration/matrix elimination suppressed conductivity method for the analysis of trace levels (0.50 μg/L) of perchlorate in drinking water. J. Chromatogr. A 1118(1), 85–93 (2006)CrossRef

20.

Li, Y.; George, E.J.: Analysis of perchlorate in water by reversed-phase LC/ESI-MS/MS using an internal standard technique. Anal. Chem. 77(14), 4453–4458 (2005). https://doi.org/10.1021/ac0500986 CrossRef

21.

Shane, A.S.; Brett, J.V.; David, J.R.: Trace analysis of bromate, chlorate, iodate, and perchlorate in natural and bottled waters. Environ. Sci. Technol. 39(12), 4586–4593 (2005). https://doi.org/10.1021/es047935q CrossRef

22.

Shi, Y.; Zhang, P.; Wang, Y.; Shi, J.; Cai, Y.; Mou, S.; Jiang, G.: Perchlorate in sewage sludge, rice, bottled water and milk collected from different areas in China. Environ. Int. 33(7), 955–962 (2007). https://doi.org/10.1016/j.envint.2007.05.007 CrossRef

23.

Elefteria, P.; Nicolas, K.: Developments in liquid-phase microextraction. TrAC Trends Anal. Chem. 22(9), 565–574 (2003). https://doi.org/10.1016/S0165-9936(03)01007-0 CrossRef

24.

Stig, P.N.; Knut, E.R.: Liquid-phase microextraction with porous hollow fibers, a miniaturized and highly flexible format for liquid–liquid extraction. J. Chromatogr. A 1184(1–2), 132–142 (2008). https://doi.org/10.1016/j.chroma.2007.08.088 CrossRef

25.

Barri, T.; Jonsson, J.A.: Advances and developments in membrane extraction for gas chromatography: techniques and applications. J. Chromatogr. A 1186(1–2), 16–38 (2008). https://doi.org/10.1016/j.chroma.2008.02.002 CrossRef

26.

Rasmussen, K.E.; Pedersen-Bjergaard, S.; Krogh, M.; Ugland, H.G.; Gronhaug, T.: Development of a simple in-vial liquid-phase microextraction device for drug analysis compatible with capillary gas chromatography, capillary electrophoresis and high-performance liquid chromatography. J. Chromatogr. A 873(1), 3–11 (2000). https://doi.org/10.1016/s0021-9673(99)01163-2 CrossRef

27.

Zhao, L.; Lee, H.K.: Liquid-phase microextraction combined with hollow fiber as a sample preparation technique prior to gas chromatography/mass spectrometry. Anal. Chem. 74(11), 2486–2492 (2002). https://doi.org/10.1021/ac011124c CrossRef

28.

Kirk, A.B.; Martinelango, P.K.; Tian, K.; Dutta, A.; Smith, E.E.; Dasgupta, P.K.: Perchlorate and iodide in dairy and breast milk. Environ. Sci. Technol. 39(7), 2011–2017 (2015). https://doi.org/10.1021/es048118t CrossRef

29.

Dyke, J.V.; Ito, K.; Obitsu, T.; Hisamatsu, Y.; Dasgupta, P.K.; Blount, B.C.: Perchlorate in dairy milk. Comparison of Japan versus the United States. Environ. Sci. Technol. 41(1), 88–92 (2007). https://doi.org/10.1021/es061429e CrossRef

30.

Li, Q.; Yu, Y.J.; Wang, F.F.; Chen, S.W.; Yin, Y.; Lin, H.P.; Che, F.; Sun, P.; Qin, J.; Liu, J.; Wang, H.M.: Urinary perchlorate exposure and risk in women of reproductive age in a fireworks production area of China. Arch. Environ. Contam. Toxicol. 67(1), 42–49 (2014). https://doi.org/10.1007/s00244-014-0042-6 CrossRef

31.

U.S. Environmental Protection Agency (USEPA): Method 331.0 Determination of Perchlorate in Drinking Water by Liquid Chromatography Electrospray Ionization Mass Spectrometry, Revision 1.0.; USEPA: Cincinnati, OH, USA (2005)

32.

Yan, L.; Hezhi, S.; Lim, Z.; Fengjian, L.; Xinzhong, Z.; Zongmao, C.: Quantitative determination and contamination pattern of perchlorate in tea by ultra performance liquid chromatography and tandem mass spectrometry. Food Chem. 274, 180–186 (2019). https://doi.org/10.1016/j.foodchem.2018.07.113 CrossRef

33.

Urbansky, E.T.: Quantitation of perchlorate ion: practices and advances applied to the analysis of common matrices. Crit. Rev. Anal. Chem. 30(4), 311–343 (2000). https://doi.org/10.1080/10408340008984163 CrossRef

34.

Corr, J.J.; Anacleto, J.F.: Analysis of inorganic species by capillary electrophoresis–mass spectrometry and ion exchange chromatography–mass spectrometry using an ion spray source. Anal. Chem. 68(13), 2155–2163 (1996). https://doi.org/10.1021/ac951053f CrossRef

35.

Chen, H.C.; Chen, W.T.; Ding, W.H.: Determination of perchlorate in river by ion-pair hollow-fiber liquid-phase microextraction coupled with electrospray ionization tandem mass spectrometry. Talanta 79(2), 442–445 (2009). https://doi.org/10.1016/j.talanta.2009.04.002 CrossRef

36.

Maxime, L.; Yuanyuan, L.; Fanny, V.; Pierre, P.; Laurent, J.M.; Elodie, B.; Valerie, G.; Antoine, T.; Manuel, P.; Jean, B.B.; Pascale, R.; Sophie, L.C.: Tuning the nature of the anion in hydrated layered double hydroxides for H₂ production under ionizing radiation. ACS Appl. Nano Mater. 1(9), 5246–5257 (2018). https://doi.org/10.1021/acsanm.8b01240 CrossRef

37.

Sajid, M.; Basheer, C.: Layered double hydroxides: emerging sorbent materials for analytical extractions. TrAC Trends Anal. Chem. 75, 174–182 (2016). https://doi.org/10.1016/j.trac.2015.06.010 CrossRef

38.

Geetanjali, M.; Barsha, D.; Sony, P.: Layered double hydroxides: a brief review from fundamentals to application as evolving biomaterials. Appl. Clay Sci. 153, 172–186 (2018)CrossRef

39.

Tang, S.; Lee, H.K.: Application of dissolvable layered double hydroxides as sorbent in dispersive solid-phase extraction and extraction by co-precipitation for the determination of aromatic acid anions. Anal. Chem. 85, 7426–7433 (2013)CrossRef

40.

Yang, Y.Q.; Gao, N.Y.; Chu, W.H.; Zhang, Y.J.; Ma, Y.: Adsorption of perchlorate from aqueous solution by the calcination product of Mg/(Al–Fe) hydrotalcite-like compounds. J. Hazard. Mater. 209–210, 318–325 (2012). https://doi.org/10.1016/j.jhazmat.2012.01.026 CrossRef

41.

Feng, L.; Xue, D.: Application Layered Double Hydroxides, pp. 193–223. Springer, Berlin (2005)

42.

Shappur, V.; Adeogun, A.I.; Ramesh, B.B.: Magnetic core layered double hydroxide over halloysite as a robust adsorbent for the treatment of dye-contaminated wastewater: a clean approach for industrial applications. Desalin. Water Treat. 138, 379–388 (2019). https://doi.org/10.5004/dwt.2019.23334) CrossRef

43.

Vicente, R.: Characterisation of layered double hydroxides and their decomposition products. Mater. Chem. Phys. 75(1–3), 19–25 (2002). https://doi.org/10.1016/S0254-0584(02)00024-X CrossRef

44.

Bruna, F.; Pavlovic, I.; Barriga, C.; Cornejo, J.; Ulibarri, M.: Adsorption of pesticides carbetamide and metamitron on organohydrotalcite. Appl. Clay Sci. 33(2), 116–124 (2006)CrossRef

45.

Hii, T.M.; Basheer, C.; Lee, H.K.: Commercial polymeric fiber as sorbent for solid-phase microextraction combined with high-performance liquid chromatography for the determination of polycyclic aromatic hydrocarbons in water. J. Chromatogr. A 1216(44), 7520–7526 (2009)CrossRef

46.

Abdolmohammad, H.; Rezvani, Z.; Sadeghi, G.H.; Zorufi, E.: Layered double hydroxides: a novel nano-sorbent for solid-phase extraction. Anal. Chim. Acta 685(2), 212–219 (2011). https://doi.org/10.1016/j.aca.2010.11.035 CrossRef

47.

El-Aribi, H.; Le, B.Y.J.; Antonsen, S.; Sakuma, T.: Analysis of perchlorate in foods and beverages by ion chromatography coupled with tandem mass spectrometry (IC–ESI–MS/MS). Anal. Chim. Acta 567(1), 39–47 (2006). https://doi.org/10.1016/j.aca.2006.03.012 CrossRef

48.

Ye, L.; You, H.; Yao, J.; Kang, X.; Tang, L.: Seasonal variation and factors influencing perchlorate in water, snow, soil and corns in Northeastern China. Chemosphere 90(10), 2493–2498 (2013). https://doi.org/10.1016/j.chemosphere.2012.10.058 CrossRef

Titel: Determination of Trace Level Perchlorate in Seawater Using Dispersive Solid-Phase Extraction and Co-precipitation Extraction with Layered Double Hydroxides Followed by Ion Chromatography Analysis
verfasst von: Amayreh Mousa
Chanbasha Basheer
Mohanad Abdullah
Abdulrahman Al-Arfaj
Publikationsdatum: 22.01.2020
Verlag: Springer Berlin Heidelberg
Erschienen in: Arabian Journal for Science and Engineering / Ausgabe 6/2020
Print ISSN: 2193-567X
Elektronische ISSN: 2191-4281
DOI: https://doi.org/10.1007/s13369-020-04342-8

Premium Partner

Marktübersichten

Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.

Zur Marktübersicht

Springer Professional

Abstract

Bitte loggen Sie sich ein, um Zugang zu Ihrer Lizenz zu erhalten.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Springer Professional "Technik"

Weitere Artikel der Ausgabe 6/2020

Synthesis and Mechanical Properties of Zirconia–Yttria Matrices/Alumina Short Fibre Composites

DFT and Kinetic Evaluation of Chloromethane Removal Using Cost-Effective Activated Carbon

Evaluation of Antibacterial Activity of Macroalgae Extracts as Adjunctive Therapy in Neonates Sepsis Induced by Klebsiella pneumoniae

Anti-inflammatory Activity and Chemical Characterisation of Opuntia ficus-indica Seed Oil Cultivated in Saudi Arabia

First Principle Insight into the Structural, Optoelectronic, Half Metallic, and Mechanical Properties of Cubic Perovskite NdInO3

Abnormal Formation Pressure in the Sulaiman Province, Pakistan: An Insight into Factor Affecting Reservoirs in a Compressional Strike-Slip Region

Premium Partner

Marktübersichten