Skip to main content
Erschienen in: Metallography, Microstructure, and Analysis 3/2018

26.04.2018 | Technical Article

Effect of Magnesium and Calcium Addition on Carbides Characterizations and Anisotropy Ductile Fracture of Inconel 718

verfasst von: Javad Teimouri, Seyed Rahman Hosseini, Khosro Farmanesh

Erschienen in: Metallography, Microstructure, and Analysis | Ausgabe 3/2018

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

Inconel 718 modified by magnesium and calcium was investigated in order to improve the ductile fracture properties of the alloy. Three different types of Inconel 718 containing 50 ppm Mg, 40 ppm Ca, and no trace elements were prepared by vacuum induction melting processes, rolled, and heat-treated. Tension and impact properties were tested at the room temperature and in the longitudinal and transverse directions. Fractographic and microstructural analyses were done by FESEM examinations. Reduction in area and impact energy was improved by 10–50% in the transverse direction, whereas strength was not changed by adding Ca and Mg. Also, these properties did not show any significant variations in longitudinal specimens. MC-type carbide was formed in solidification and rearranged as stringer during the rolling process, significantly reducing the impact energy of Inconel 718 on transverse samples. Ductile anisotropy was modified as the carbide shape and size were refined in the as-cast microstructure of Mg and Ca alloys.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literatur
1.
Zurück zum Zitat A. Mitchell, Primery carbidea in alloy 718, in Proceedings of the Superalloy 718 and Derivatives, ed. by E.A. Ott, R. Groh, A. Banik, I. Dempster, T.P. Gabb, R. Helmink, X. Liu (Wiley, New York, 2010), pp. 161–167 A. Mitchell, Primery carbidea in alloy 718, in Proceedings of the Superalloy 718 and Derivatives, ed. by E.A. Ott, R. Groh, A. Banik, I. Dempster, T.P. Gabb, R. Helmink, X. Liu (Wiley, New York, 2010), pp. 161–167
2.
Zurück zum Zitat S.-H. Kang, Y. Deguchi, K. Yamamoto, K. Ogi, M. Shirai, Solidification process and behavior of alloying elements in Ni-based superalloy Inconel718. Mater. Trans. 45(8), 2728–2733 (2004)CrossRef S.-H. Kang, Y. Deguchi, K. Yamamoto, K. Ogi, M. Shirai, Solidification process and behavior of alloying elements in Ni-based superalloy Inconel718. Mater. Trans. 45(8), 2728–2733 (2004)CrossRef
3.
Zurück zum Zitat Y. Zhang, Z. Li, P. Nie, Y. Wu, Carbide and nitride precipitation during laser cladding of Inconel 718 alloy coatings. Opt. Laser Technol. 52, 30–36 (2013)CrossRef Y. Zhang, Z. Li, P. Nie, Y. Wu, Carbide and nitride precipitation during laser cladding of Inconel 718 alloy coatings. Opt. Laser Technol. 52, 30–36 (2013)CrossRef
4.
Zurück zum Zitat L. Xiao, M.C. Chaturvedi, D. Chen, Effect of boron and carbon on the fracture toughness of IN 718 superalloy at room temperature and 650°C. J. Mater. Eng. Perform. 14(4), 528–538 (2005)CrossRef L. Xiao, M.C. Chaturvedi, D. Chen, Effect of boron and carbon on the fracture toughness of IN 718 superalloy at room temperature and 650°C. J. Mater. Eng. Perform. 14(4), 528–538 (2005)CrossRef
5.
Zurück zum Zitat W.-J. Zheng, X.-P. Wei, Z.-G. Song, Q.-L. Yong, F. Han, Q.-C. Xie, Effects of carbon content on mechanical properties of Inconel 718 alloy. J. Iron. Steel Res. Int. 22(1), 78–83 (2015)CrossRef W.-J. Zheng, X.-P. Wei, Z.-G. Song, Q.-L. Yong, F. Han, Q.-C. Xie, Effects of carbon content on mechanical properties of Inconel 718 alloy. J. Iron. Steel Res. Int. 22(1), 78–83 (2015)CrossRef
6.
Zurück zum Zitat J. Yang, Q. Zheng, X. Sun, H. Guan, Z. Hu, Relative stability of carbides and their effects on the properties of K465 superalloy. Mater. Sci. Eng. A 429(1), 341–347 (2006)CrossRef J. Yang, Q. Zheng, X. Sun, H. Guan, Z. Hu, Relative stability of carbides and their effects on the properties of K465 superalloy. Mater. Sci. Eng. A 429(1), 341–347 (2006)CrossRef
7.
Zurück zum Zitat C. Joseph, M. Hornqvist, C. Persson, Anisotropy of room temperature ductility in Haynes 282 forgings, in Proceedings of the Superalloy 718 and Derivatives, ed. by E. Ott, A. Banik, X. Liu, I. Dempster, K. Heck, J. Andersson (Wiley, New York, 2014), pp. 601–609 C. Joseph, M. Hornqvist, C. Persson, Anisotropy of room temperature ductility in Haynes 282 forgings, in Proceedings of the Superalloy 718 and Derivatives, ed. by E. Ott, A. Banik, X. Liu, I. Dempster, K. Heck, J. Andersson (Wiley, New York, 2014), pp. 601–609
8.
Zurück zum Zitat K. Mo, G. Lovicu, X. Chen, H.-M. Tung, J.B. Hansen, J.F. Stubbins, Mechanism of plastic deformation of a Ni-based superalloy for VHTR applications. J. Nucl. Mater. 44(1), 695–703 (2013)CrossRef K. Mo, G. Lovicu, X. Chen, H.-M. Tung, J.B. Hansen, J.F. Stubbins, Mechanism of plastic deformation of a Ni-based superalloy for VHTR applications. J. Nucl. Mater. 44(1), 695–703 (2013)CrossRef
9.
Zurück zum Zitat G. Liu, D.K. Rehbein, O. Buck, Anisotropy of the fracture toughness in aged Inconel 718, in Review of Progress in Quantitative Nondestructive Evaluation, ed. by D.O. Thompson, D.E. Chimenti (Plenum Press, New York, 1997), pp. 1451–1457CrossRef G. Liu, D.K. Rehbein, O. Buck, Anisotropy of the fracture toughness in aged Inconel 718, in Review of Progress in Quantitative Nondestructive Evaluation, ed. by D.O. Thompson, D.E. Chimenti (Plenum Press, New York, 1997), pp. 1451–1457CrossRef
10.
Zurück zum Zitat G. Meetham, Trace elements in superalloys—an overview. Metals Technol. 11(1), 414–418 (1984)CrossRef G. Meetham, Trace elements in superalloys—an overview. Metals Technol. 11(1), 414–418 (1984)CrossRef
11.
Zurück zum Zitat K. Banerjee, The role of magnesium in superalloys—a review. Mater. Sci. Appl. 2(9), 1243–1255 (2011) K. Banerjee, The role of magnesium in superalloys—a review. Mater. Sci. Appl. 2(9), 1243–1255 (2011)
12.
Zurück zum Zitat G. Chen, Q. Zhu, D. Wang, X. Xie, Effects of magnesium on niobium segregation and impact toughness in cast alloy 718, in Proceedings of Superalloys 718 and Derivatives, ed. by E.A. Loria (TMS, Pennsylvania, 1989), pp. 545–551 G. Chen, Q. Zhu, D. Wang, X. Xie, Effects of magnesium on niobium segregation and impact toughness in cast alloy 718, in Proceedings of Superalloys 718 and Derivatives, ed. by E.A. Loria (TMS, Pennsylvania, 1989), pp. 545–551
13.
Zurück zum Zitat X. Liu, J. Dong, X. Xie, K.-M. Chang, The appearance of magnesium and its effect on the mechanical properties of Inconel 718 with low sulfur content. Mater. Sci. Eng. A 303(1), 262–266 (2001)CrossRef X. Liu, J. Dong, X. Xie, K.-M. Chang, The appearance of magnesium and its effect on the mechanical properties of Inconel 718 with low sulfur content. Mater. Sci. Eng. A 303(1), 262–266 (2001)CrossRef
14.
Zurück zum Zitat X.-C. Chen, C.-B. Shi, H.-J. Guo, F. Wang, H. Ren, D. Feng, Investigation of oxide inclusions and primary carbonitrides in Inconel 718 superalloy refined through electroslag remelting process. Metall. Mater. Trans. B 43(6), 1596–1607 (2012)CrossRef X.-C. Chen, C.-B. Shi, H.-J. Guo, F. Wang, H. Ren, D. Feng, Investigation of oxide inclusions and primary carbonitrides in Inconel 718 superalloy refined through electroslag remelting process. Metall. Mater. Trans. B 43(6), 1596–1607 (2012)CrossRef
15.
Zurück zum Zitat BS EN 10247 (2007), Micrographic Examination of the Non-metallic Inclusion Content of Steels Using Standard Pictures BS EN 10247 (2007), Micrographic Examination of the Non-metallic Inclusion Content of Steels Using Standard Pictures
16.
Zurück zum Zitat H. Bor, C. Ma, C. Chao, The influence of Mg on creep properties and fracture behaviors of Mar-M247 superalloy under 1255 K/200 MPa. Metall. Mater. Trans. A 31(5), 1365–1373 (2000)CrossRef H. Bor, C. Ma, C. Chao, The influence of Mg on creep properties and fracture behaviors of Mar-M247 superalloy under 1255 K/200 MPa. Metall. Mater. Trans. A 31(5), 1365–1373 (2000)CrossRef
17.
Zurück zum Zitat H. Bor, C. Chao, C. Ma, The influence of magnesium on carbide characteristics and creep behavior of the Mar-M247 superalloy. Scr. Mater. 38(2), 329–335 (1997)CrossRef H. Bor, C. Chao, C. Ma, The influence of magnesium on carbide characteristics and creep behavior of the Mar-M247 superalloy. Scr. Mater. 38(2), 329–335 (1997)CrossRef
18.
Zurück zum Zitat Y. Ono, T. Yuri, H. Sumiyoshi, E. Takeuchi, S. Matsuoka, T. Ogata, High-cycle fatigue properties at cryogenic temperatures in Inconel 718 nickel-based superalloy. Mater. Trans. 45(2), 342–345 (2004)CrossRef Y. Ono, T. Yuri, H. Sumiyoshi, E. Takeuchi, S. Matsuoka, T. Ogata, High-cycle fatigue properties at cryogenic temperatures in Inconel 718 nickel-based superalloy. Mater. Trans. 45(2), 342–345 (2004)CrossRef
19.
Zurück zum Zitat W. Mills, L. Blackburn, Variations in fracture toughness for alloy 718 given a modified heat treatment. J. Eng. Mater. Technol. 112, 116–123 (1990)CrossRef W. Mills, L. Blackburn, Variations in fracture toughness for alloy 718 given a modified heat treatment. J. Eng. Mater. Technol. 112, 116–123 (1990)CrossRef
20.
Zurück zum Zitat J. Zhu, Z. Cheng, H. Ye, The distribution and morphology of trace Mg at a grain boundary in a Ni-base superalloy. Scr. Mater. 23(9), 1537–1542 (1989) J. Zhu, Z. Cheng, H. Ye, The distribution and morphology of trace Mg at a grain boundary in a Ni-base superalloy. Scr. Mater. 23(9), 1537–1542 (1989)
21.
Zurück zum Zitat Dong, J.X., Thompson, R.G., Xie, X.S.: Mult-component intergranular and interfacial segregation in alloy 718 with correlations to stress rupture behavior. In: Loria, E.A. (eds.) Proceedings of the Superalloy 718 and Derivatives, pp. 553–566. The Society, Pennsylvania (1997) Dong, J.X., Thompson, R.G., Xie, X.S.: Mult-component intergranular and interfacial segregation in alloy 718 with correlations to stress rupture behavior. In: Loria, E.A. (eds.) Proceedings of the Superalloy 718 and Derivatives, pp. 553–566. The Society, Pennsylvania (1997)
22.
Zurück zum Zitat A. Bhambri, T. Kattamis, J. Morral, Cast microstructure of Inconel 713C and its dependence on solidification variables. Metall. Trans. B 6(4), 523–537 (1975)CrossRef A. Bhambri, T. Kattamis, J. Morral, Cast microstructure of Inconel 713C and its dependence on solidification variables. Metall. Trans. B 6(4), 523–537 (1975)CrossRef
23.
Zurück zum Zitat B.H. Kear, Effect of uncombined calcium and magnesium on the malleability of nickel alloys, in Proceedings of Superalloys, ed. by J.J. de Barbadillo (Claitors, Baton Rouge, 1976), pp. 95–107 B.H. Kear, Effect of uncombined calcium and magnesium on the malleability of nickel alloys, in Proceedings of Superalloys, ed. by J.J. de Barbadillo (Claitors, Baton Rouge, 1976), pp. 95–107
24.
Zurück zum Zitat J. Dong, X. Xie, R. Thompson, The influence of sulfur on stress-rupture fracture in Inconel 718 superalloys. Metall. Mater. Trans. A 31(9), 2135–2144 (2000)CrossRef J. Dong, X. Xie, R. Thompson, The influence of sulfur on stress-rupture fracture in Inconel 718 superalloys. Metall. Mater. Trans. A 31(9), 2135–2144 (2000)CrossRef
25.
Zurück zum Zitat G. Bernard, P. Riboud, G. Urbain, Investigation of the plasticity of oxide inclusions. Rev. de Metall. 78(5), 421–433 (1981)CrossRef G. Bernard, P. Riboud, G. Urbain, Investigation of the plasticity of oxide inclusions. Rev. de Metall. 78(5), 421–433 (1981)CrossRef
26.
Zurück zum Zitat T. Baker, K. Gave, J. Charles, Inclusion deformation and toughness anisotropy in hot-rolled steels. Metals Technol. 3(1), 183–193 (1976)CrossRef T. Baker, K. Gave, J. Charles, Inclusion deformation and toughness anisotropy in hot-rolled steels. Metals Technol. 3(1), 183–193 (1976)CrossRef
27.
Zurück zum Zitat A. Pineau, A.A. Benzerga, T. Pardoen, Failure of metals I: brittle and ductile fracture. Acta Mater. 107, 424–483 (2016)CrossRef A. Pineau, A.A. Benzerga, T. Pardoen, Failure of metals I: brittle and ductile fracture. Acta Mater. 107, 424–483 (2016)CrossRef
Metadaten
Titel
Effect of Magnesium and Calcium Addition on Carbides Characterizations and Anisotropy Ductile Fracture of Inconel 718
verfasst von
Javad Teimouri
Seyed Rahman Hosseini
Khosro Farmanesh
Publikationsdatum
26.04.2018
Verlag
Springer US
Erschienen in
Metallography, Microstructure, and Analysis / Ausgabe 3/2018
Print ISSN: 2192-9262
Elektronische ISSN: 2192-9270
DOI
https://doi.org/10.1007/s13632-018-0449-y

Weitere Artikel der Ausgabe 3/2018

Metallography, Microstructure, and Analysis 3/2018 Zur Ausgabe

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.