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Erschienen in: Journal of Materials Engineering and Performance 7/2017

21.06.2017

Effect of Surface Roughness of an Electropolished Aluminum Substrate on the Thickness, Morphology, and Hardness of Aluminum Oxide Coatings Formed During Anodization in Oxalic Acid

verfasst von: R. K. Choudhary, K. P. Sreeshma, P. Mishra

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 7/2017

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Abstract

Aluminum specimens were electropolished to five different roughness profiles and anodized in 10% oxalic acid under identical conditions in order to study the effect of surface topography on the thickness, morphology, chemical composition and hardness of the anodic aluminum oxide coatings formed. Field emission scanning electron microscopy showed that the anodic coating grown on a substrate having an average roughness of 250 nm was dense, whereas the microstructure became more porous with increasing the substrate roughness. The thickness of the coating was found to be a parabolic function of substrate roughness. Energy-dispersive x-ray analysis of coatings revealed a continuous increase in O/Al ratio with increasing substrate roughness suggesting increased incorporation of anions during oxide growth and also a tendency toward the formation of stoichiometric Al2O3. Coatings with higher O/Al ratio displayed improved hardness values.

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Metadaten
Titel
Effect of Surface Roughness of an Electropolished Aluminum Substrate on the Thickness, Morphology, and Hardness of Aluminum Oxide Coatings Formed During Anodization in Oxalic Acid
verfasst von
R. K. Choudhary
K. P. Sreeshma
P. Mishra
Publikationsdatum
21.06.2017
Verlag
Springer US
Erschienen in
Journal of Materials Engineering and Performance / Ausgabe 7/2017
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-017-2798-0

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