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2020 | OriginalPaper | Chapter

Base Transesterification of Ineffectual Soybean Oil Using Lab Scale Synthesized CaO Catalyst

Authors : Rakesh Singh Ningthoujam, Ronaldo Singh Naorem, Denin Singh Langpokpam, Thokchom Subhaschandra Singh, Tikendra Nath Verma

Published in: Advances in Applied Mechanical Engineering

Publisher: Springer Singapore

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Abstract

The present study involves the transesterification of ineffectual soybean oil using synthesized calcinated (duck eggshell) calcium oxide (CaO) as heterogeneous base catalyst. The catalyst was first prepared by exposing at a muffle furnace for about 180 min 800 °C and then characterized using X-ray diffraction (XRD), Fourier transform infrared spectrometry (FT-IR), scanning electron microscopy (SEM) and energy-dispersive x-ray spectroscopy (EDX). There is characterization of uncooked, ineffectual and transesterified ineffectual soybean oil using FT-IR spectrometry. The yield was obtained to be 94.55% when transesterified at 3% (wt%) catalyst loading, 10:1 alcohol to oil ratio, a reaction temperature of 70 °C and a reaction time of 60 min. The methyl ester underwent gas chromatography–mass spectrometer (GC-MS) test to check the contents of the yield oil. It was found that the cheap and ready to be discarded ineffectual soybean oil can be effectively used for producing biodiesel.

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Metadata
Title
Base Transesterification of Ineffectual Soybean Oil Using Lab Scale Synthesized CaO Catalyst
Authors
Rakesh Singh Ningthoujam
Ronaldo Singh Naorem
Denin Singh Langpokpam
Thokchom Subhaschandra Singh
Tikendra Nath Verma
Copyright Year
2020
Publisher
Springer Singapore
Book
Advances in Applied Mechanical Engineering

Print ISBN: 978-981-15-1200-1

Electronic ISBN: 978-981-15-1201-8

Copyright Year: 2020

DOI
https://doi.org/10.1007/978-981-15-1201-8_79

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