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Arabian Journal for Science and Engineering
Published in: Arabian Journal for Science and Engineering 7/2021

05-01-2021 | Research Article-Chemical Engineering

Butyric Acid Reactive Extraction Using Trioctylamine in 1-Decanol: Response Surface Methodology Parametric Optimization Technique

Authors: Victoria Inyang, David Lokhat

Published in: Arabian Journal for Science and Engineering | Issue 7/2021

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Abstract

The optimization of the reactive extraction of butyric acid from an aqueous stream was effectively carried out using response surface methodology. Three process parameters were studied, viz. initial butyric acid concentration, trioctylamine concentration and temperature, to examine the interactive effects on extraction efficiency and distribution coefficient. A Box-Behnken design comprising of seventeen experimental runs was utilized in the reactive extraction study of butyric acid. Analysis of a second-order polynomial model yielded the following optimal conditions: temperature 301.829 K, initial butyric acid concentration 0.493 kmol/m3, trioctylamine composition 26.417%v/v with the following responses: distribution coefficient = 28.795 and extraction efficiency of 96.666%. Experimental validation of the model was carried out with the predicted process variables, and the responses obtained (distribution coefficient = 27.171, extraction efficiency = 96.450%) were in close conformity to the predicted outcomes. Three-dimensional surface plots obtained from statistical analysis demonstrated that the butyric acid concentration and TOA composition had a more significant and interactive effect than the temperature on the response value in the reactive extraction process.
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Metadata
Title
Butyric Acid Reactive Extraction Using Trioctylamine in 1-Decanol: Response Surface Methodology Parametric Optimization Technique
Authors
Victoria Inyang
David Lokhat
Publication date
05-01-2021
Publisher
Springer Berlin Heidelberg
Published in
Arabian Journal for Science and Engineering / Issue 7/2021
Print ISSN: 2193-567X
Electronic ISSN: 2191-4281
DOI
https://doi.org/10.1007/s13369-020-05255-2

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