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2020 | OriginalPaper | Chapter

Characterisation of Green Nanomaterials

Authors : T. Anukiruthika, S. Priyanka, J. A. Moses, C. Anandharamakrishnan

Published in: Green Nanomaterials

Publisher: Springer Singapore

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Abstract

Green synthesis of nanoparticles is becoming popular due to its sustainability, eco-friendly and inexpensive approach. Production of submicron-sized particles from the biogenic sources is referred as green-mediated synthesis. Different kinds of green metal nanoparticles available are Ag, Au, Cu, Cd, Pt, Pd, Fe, and other metal oxides include ZnO, CeO₂, TiO_2, ZrO₂, In₂O₃, Cu₂O and CuO, PbS, Fe₃O₄. These nanoparticles are characterised for its surface morphology and its compositional structure. The common techniques employed for characterisation of metal and metal oxide nanoparticles include UV-visible absorption spectroscopy, X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, energy dispersive spectroscopy (EDAX), atomic force microscopy (AFM), scanning electron microscope (SEM), transmission electron microscope (TEM), etc. The main characteristics that determine the properties and functionality of green nanomaterials are particle size, size distribution, crystallinity, specific surface area, surface morphology and elemental composition. Characterisation of green nanoparticles is significant to study about the nature, behaviour and functional properties of synthesised green nanoparticles (NPs). These NPs are well known for its antimicrobial and antioxidant effects as they have potential applications in food processing as in food packaging, food quality analysis and food/drug delivery systems. In order to find potential applications of green nanomaterials, characterisation of these nanoparticles is significant. This chapter essentially focusses on various characterisation techniques for the green-synthesised nanomaterials.

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Agarwal N, Nair MS, Mazumder A (2018) Characterization of nanomaterials using nuclear magnetic resonance spectroscopy. In: Characterization of nanomaterials. Elsevier Ltd. https://doi.org/10.1016/B978-0-08-101973-3.00003-1

Ahmad A, Mukherjee P, Mandal D, Senapati S, Khan MI, Kumar R, Sastry M (2003) Extracellular biosynthesis of silver nanoparticles using the fungus Fusarium oxysporum composite metal particles, and the atom to metal. Colloids Surf B: Biointerfaces 28:313–318

Ahmed KBA, Kalla D, Uppuluri KB, Anbazhagan V (2014) Green synthesis of silver and gold nanoparticles employing levan, a biopolymer from Acetobacter xylinum NCIM 2526, as a reducing agent and capping agent. Carbohyd Polym 112:539–545. https://doi.org/10.1016/j.carbpol.2014.06.033CrossRef

Alam TM, Jenkins JE (2012) HR-MAS NMR spectroscopy in material science. Intech Open 2:64. https://doi.org/10.5772/32009CrossRef

Anake WU, Ana GR, Benson NU (2016) Study of surface morphology, elemental composition and sources of airborne fine particulate matter in Agbara industrial estate, Nigeria. Int J Appl Environ Sci 11(4):881–890

Ando J, Yano T, Fujita K, Kawata S (2013) Metal nanoparticles for nano-imaging and nano-analysis. Phys Chem Chem Phys 15(33):13713–13722. https://doi.org/10.1039/c3cp51806jCrossRef

Arokiyaraj S, Vincent S, Saravanan M, Oh YK, Kim KH (2016) Green synthesis of silver nanoparticles using Rheum palmatum root extract and their antibacterial activity against Staphylococcus aureus and Pseudomonas aeruginosa. 1401 (March). https://doi.org/10.3109/21691401.2016.1160403

Arunachalam KD, Annamalai SK, Hari S (2013) One-step green synthesis and characterization of leaf extract-mediated biocompatible silver and gold nanoparticles from Memecylon umbellatum. Int J Nanomedicine 8:1307–1315CrossRef

Asfaram A, Ghaedi M, Goudarzi A (2015) Solid-phase extraction for the determination of. New J Chem 39:9813–9823. https://doi.org/10.1039/C5NJ01730KCrossRef

Asou HM, Al-antary M, Awwad AM (2018) Environmental nanotechnology, monitoring & management green route for synthesis hematite (α-Fe₂O₃) nanoparticles: toxicity e ffect on the green peach aphid. Myzus persicae (Sulzer) 9:107–111. https://doi.org/10.1016/j.enmm.2018.01.004CrossRef

Bai RG, Sabouni R, Husseini G (2018) Green Nanotechnology—A Road Map to Safer Nanomaterials. In: Applications of Nanomaterials, Elsevier Ltd. https://doi.org/10.1016/B978-0-08-101971-9.00006-5

Bandyopadhyay S (2013) Advanced analytical techniques for the measurement of nanomaterials in food and agricultural samples: a review 1, 30(3): 118–125. https://doi.org/10.1089/ees.2012.0325

Bhattacherjee A, Ghosh T, Datta A (2018) Green synthesis and characterisation of antioxidant-tagged gold nanoparticle (X-GNP) and studies on its potent antimicrobial activity. J Exp Nanosci 13(1):50–61. https://doi.org/10.1080/17458080.2017.1407042CrossRef

Biao L, Tan S, Meng Q, Gao J, Zhang X, Liu Z, Fu Y (2018) Green synthesis, characterization and application of proanthocyanidins-functionalized gold nanoparticles. Nanomaterials 8(1):53. https://doi.org/10.3390/nano8010053CrossRef

Bishnoi A, Kumar S, Joshi N (2017) Wide-angle X-ray diffraction (WXRD): technique for characterization of nanomaterials and polymer nanocomposites. In: Microscopy Methods in Nanomaterials Characterization, Elsevier, pp 313–337

Bunaciu AA, UdriŞTioiu EG, Aboul-Enein HY (2015) X-ray diffraction: instrumentation and applications. Crit Rev Anal Chem 45(4):289–299CrossRef

Chen M, Wang X, Yu YH, Pei ZL, Bai XD, Sun C, Wen LS (2000) X-ray photoelectron spectroscopy and auger electron spectroscopy studies of Al-doped ZnO films. Appl Surf Sci 158(1):134–140. https://doi.org/10.1016/S0169-4332(99)00601-7CrossRef

Cheng F, Su C, Yang Y, Yeh C (2005) Characterization of aqueous dispersions of Fe₃O₄ nanoparticles and their biomedical applications 26: 729–738. https://doi.org/10.1016/j.biomaterials.2004.03.016

Costa S, Borowiak-Palen E, Kruszynska M, Bachmatiuk A, Kalenczuk R (2008) Characterization of carbon nanotubes by Raman spectroscopy. Mater Sci Poland 26(2):433–441

Crozier A, Jaganath IB, Clifford MN, Crozier A, Jaganath B, Clifford MN (2009) Dietary phenolics: chemistry, bioavailability and effects on health. 26(8). https://doi.org/10.1039/b802662a

Davar F, Fereshteh Z, Salavati-niasari M (2009) Nanoparticles Ni and NiO: synthesis, characterization and magnetic properties 476:797–801. https://doi.org/10.1016/j.jallcom.2008.09.121

David L, Moldovan B, Vulcu A, Olenic L, Perde-schrepler M, Fischer-fodor E, Adriana G (2014) Green synthesis, characterization and anti-inflammatory activity of silver nanoparticles using European black elderberry fruits extract. Colloids Surfaces B Biointerfaces. https://doi.org/10.1016/j.colsurfb.2014.08.018

De Oliveira O, Marystela F, de Lima Leite F, Da Róz AL (2017) Nanocharacterization Techniques. Matthew Deans. https://doi.org/10.1016/B978-0-323-49778-7.00001-1CrossRef

Devience SJ, Pham LM, Lovchinsky I, Sushkov AO, Bar-gill N, Belthangady C, Walsworth RL (2015) Nanoscale NMR spectroscopy and imaging of multiple nuclear species. Nature Nanotechnol, 2–7. https://doi.org/10.1038/nnano.2014.313

Dipankar C, Murugan S (2012) Colloids and Surfaces B: Biointerfaces The green synthesis, characterization and evaluation of the biological activities of silver nanoparticles synthesized from Iresine herbstii leaf aqueous extracts. Colloids Surf B 98:112–119. https://doi.org/10.1016/j.colsurfb.2012.04.006CrossRef

Dixon R (2005). Proanthocyanidins—a final frontier in

Djuris AB, Leung YH, Ng AMC, Xu XY, Lee PK, Degger N, Wu RS (2014) Toxicity of metal oxide nanoparticles: mechanisms, characterization, and avoiding experimental artefacts. pp 1–19. https://doi.org/10.1002/smll.201303947

Faix O (1992) Fourier transform infrared spectroscopy. Methods Lignin Chem pp 83–109. https://doi.org/10.1007/978-3-642-74065-7_16

Ferri FA, Perreira-da-Silva MDA, Marega E (2012) Atomic force microscopy-imaging, measuring and manipulating surfaces at the atomic scale. In: Bellitto V (ed) InTech, p 268

Gangadoo S, Chapman J (2015) Nanoparticle and biomaterial characterisation techniques, 30. https://doi.org/10.1179/1753555714Y.0000000201

García-Betancourt ML, Rahier H, Van Assche G (2018)Physicochemical characterization of nanomaterials: polymorph, composition, wettability, and thermal stability. In: Emerging applications of nanoparticles and architecture nanostructures, Elsevier Inc. https://doi.org/10.1016/B978-0-323-51254-1.00009-9

Gogoi N, Jayasekhar P, Mahanta C, Bora U (2015) Green synthesis and characterization of silver nanoparticles using alcoholic fl ower extract of Nyctanthes arbortristis and in vitro investigation of their antibacterial and cytotoxic activities. Mater Sci Eng C 46:463–469. https://doi.org/10.1016/j.msec.2014.10.069CrossRef

Goldstein JI, Newbury DE, Michael JR, Ritchie NW, Scott JH, Joy DC (2017) Scanning electron microscopy and X-ray microanalysis, Springer

Gopi D, Kanimozhi K, Bhuvaneshwari N, Indira J, Kavitha L (2014) Novel banana peel pectin mediated green route for the synthesis of hydroxyapatite nanoparticles and their spectral characterization. Spectrochim Acta Part A Mol Biomol Spectrosc 118:589–597. https://doi.org/10.1016/j.saa.2013.09.034CrossRef

Goyal RK (2017) Nanomaterials and nanocomposites: synthesis, properties, characterization techniques, and applications, CRC Press

Hafner B (2006) Energy dispersive spectroscopy on the SEM: a primer. In: Characterization Facility, University of Minnesota, pp 1–26

Hall JB, Dobrovolskaia MA, Patri AK, McNeil SE (2007) Characterization of nanoparticles for therapeutics

Henning S, Adhikari R (2017) Scanning electron microscopy, ESEM, and X-ray microanalysis. In: Microscopy Methods in Nanomaterials Characterization, Elsevier, pp. 1–30

Hollander JM, Jolly WL (1970) X-ray photoelectron spectroscopy. Acc Chem Res 3(6):193–200CrossRef

https://en.Wikipedia.org/wiki/Ultraviolet%E2%80%93visible_spectroscopy

https://en.wikipedia.org/wiki/X-ray_photoelectron_spectroscopy#/media/File:System2.gif

Hussain I, Singh NB, Singh A, Singh H, Singh SC (2016) Green synthesis of nanoparticles and its potential application. Biotech Lett 38(4):545–560. https://doi.org/10.1007/s10529-015-2026-7CrossRef

Hyllested JÆ, Palanco ME, Hagen N, Mogensen KB (2015) Green preparation and spectroscopic characterization of plasmonic silver nanoparticles using fruits as reducing agents, pp 293–299. https://doi.org/10.3762/bjnano.6.27

Instruments N (1999) Energy-dispersive x-ray microanalysis an introduction. Noran Instruments Inc., Middleton

Jaggi N, Vij DR (2006) Fourier transform infrared, pp 411–450

Jain A, Ranjan S, Dasgupta N, Ramalingam C (2018) Nanomaterials in food and agriculture: an overview on their safety concerns and regulatory issues. Crit Rev Food Sci Nutr 58(2):297–317. https://doi.org/10.1080/10408398.2016.1160363CrossRef

Jiang X, Jiang J, Jin Y, Wang E, Dong S (2005). Effect of colloidal gold size on the conformational changes of adsorbed cytochrome c: probing by circular dichroism, UV—Visible, and Infrared Spectroscopy, pp 46–53

Johal MS (2012) Understanding nanomaterials, CRC Press

Kale RD, Jagtap P (2018) Biogenic synthesis of silver nanoparticles using Citrus Limon leaves and its structural investigation, pp 11–20. https://doi.org/10.1007/978-981-10-7122-5_2

Khan AU, Malik N, Khan M, Hwan M (2017) Fungi-assisted silver nanoparticle synthesis and their applications. Bioprocess Biosyst Eng. https://doi.org/10.1007/s00449-017-1846-3CrossRef

Khan MK, Wang QY, Fitzpatrick ME (2016) Atomic force microscopy (AFM) for materials characterization. In: Materials Characterization Using Nondestructive Evaluation (NDE) Methods, Elsevier, pp 1–16

Khan M, Albalawi GH, Shaik MR, Khan M, Adil SF, Kuniyil M, Alkhathlan HZ, Al-Warthan A, Siddiqui MRH (2017) Miswak mediated green synthesized palladium nanoparticles as effective catalysts for the Suzuki coupling reactions in aqueous media. J Saudi Chem Soc 21(4):450–457. https://doi.org/10.1039/b615357g.

Khan ZUH, Khan A, Chen YM, Shah NS, Khan AU, Muhammad N, Wan P (2018) Enhanced antimicrobial, anti-oxidant applications of green synthesized AgNPs- an acute chronic toxicity study of phenolic azo dyes & study of materials surface using X-ray photoelectron spectroscopy. J Photochem Photobiol B 180:208–217. https://doi.org/10.1016/j.jphotobiol.2018.02.015CrossRef

Khitrov GA, Strouse GF (2003) ZnS nanomaterial characterization by MALDI-TOF mass spectrometry 10: 10465–10469

Kneipp J, Kneipp H, Wittig B, Kneipp K (2010) Novel optical nanosensors for probing and imaging live cells. Nanomed Nanotechnol Biol Med 6(2): 214–226. https://doi.org/10.1016/j.nano.2009.07.009

Kong J, Yu S (2007) Fourier transform infrared spectroscopic analysis of protein secondary structures protein FTIR data analysis and band assign 39(20745001):549–559. https://doi.org/10.1111/j.1745-7270.2007.00320.xCrossRef

Konno H (2016) X-ray Photoelectron Spectroscopy. In: Materials Science and Engineering of Carbon, Tsinghua University Press Limited. https://doi.org/10.1016/B978-0-12-805256-3.00008-8

Kouvaris P, Delimitis A, Zaspalis V, Papadopoulos D, Tsipas SA, Michailidis N (2012) Green synthesis and characterization of silver nanoparticles produced using Arbutus Unedo leaf extract. Mater Lett 76:18–20. https://doi.org/10.1016/j.matlet.2012.02.025CrossRef

Kumar J, Thomas KG (2011) Nanorod edges and dimer junctions

Kumar U, Ankamwar B, Karmakar S, Halder A (2018) Science direct green synthesis of silver nanoparticles using the plant extract of Shikakai and Reetha. Mater Today Proc 5(1):2321–2329. https://doi.org/10.1016/j.matpr.2017.09.236CrossRef

Li X, Zhang W (2007) Sequestration of metal cations with Zerovalent Iron nanoparticles: a study with high resolution X-ray Photoelectron Spectroscopy (HR-XPS). J Phys Chem C Saudi Chem Soc 111(19): 6939–6946. https://doi.org/10.1021/jp0702189. https://doi.org/10.1016/j.jscs.2016.03.008

Lee SH, Heng Desmond, Ng WK, Chan H-K, Tan RBH (2011) Nano spray drying: a novel method for preparing protein nanoparticles for protein therapy. Int J Pharm 403(1–2):192–200CrossRef

Lin PC, Lin S, Wang PC, Sridhar R (2014) Techniques for physicochemical characterization of nanomaterials. Biotechnol Adv 32(4):711–726. https://doi.org/10.1016/j.biotechadv.2013.11.006CrossRef

Liu S, Wang Y (2010) Application of AFM in microbiology: a review. Scanning 32(2):61–73CrossRef

Liu S, Wang Y (2011) A review of the application of atomic force microscopy (AFM) in food science and technology. In: Advances in food and nutrition research, Elsevier, pp 201–240

Liu J, Jiang P, He C, Jiang X, Lu L (2018) Preparation and characterization of Ag @ C composites with hexagon silver core and controllable carbon shell for surface-enhanced Raman scattering, pp 3443–3454. https://doi.org/10.1007/s10853-017-1801-3

López-Sanz S, Fariñas NR, Vargas RS, Martín-Doimeadios RDCR, Ríos Á (2017) Methodology for monitoring gold nanoparticles and dissolved gold species in culture medium and cells used for nanotoxicity tests by liquid chromatography hyphenated to inductively coupled plasma-mass spectrometry. Talanta 164:451–457. https://doi.org/10.1016/j.talanta.2016.11.060

Luo F, Yang D, Chen Z, Megharaj M, Naidu R (2016) One-step green synthesis of bimetallic Fe/Pd nanoparticles used to degrade Orange II. J Hazard Mater 303:145–153CrossRef

Lupoi JS, Singh S, Simmons BA, Henry RJ (2014) Assessment of Lignocellulosic biomass using analytical spectroscopy: an evolution to high-throughput techniques. Bioenergy Res 7(1):1–23. https://doi.org/10.1007/s12155-013-9352-1CrossRef

Ma M, Zhang Y, Yu W, Shen H, Zhang H, Gu N (2003) Preparation and characterization of magnetite nanoparticles coated by amino silane 212:219–226

Marbella LE, Millstone JE (2015) NMR techniques for noble metal nanoparticles. https://doi.org/10.1021/cm504809c

Mayeen A, Shaji LK, Nair AK, Kalarikkal N (2018) Morphological characterization of nanomaterials. In: Characterization of Nanomaterials, Elsevier, pp 335–364

Medina-Ramirez I, Bashir S, Luo Z, Liu JL (2009) Green synthesis and characterization of polymer-stabilized silver nanoparticles. Colloids Surf B 73(2):185–191. https://doi.org/10.1016/j.colsurfb.2009.05.015CrossRef

Miguel L, Rivera R, Silva LP (2018) https://doi.org/10.1016/j.matchemphys.2018.05.068 (Accepted Manuscript)

Michler GH (2008) Electron microscopy of polymers, Springer Science & Business Media

Mishra RK, Zachariah AK, Thomas S (2017) Energy-dispersive X-ray spectroscopy techniques for nanomaterial. In: Microscopy Methods in Nanomaterials Characterization, Elsevier, pp 383–405

Mukherjee P, Roy M, Mandal BP, Dey GK, Mukherjee PK, Ghatak J, Kale SP (2008) Green synthesis of highly stabilized nanocrystalline silver particles by a non-pathogenic and agriculturally important fungus T. asperellum, p 075103. https://doi.org/10.1088/0957-4484/19/7/075103

Muñetón D, Santillán JMJ, Arce VB, Fernández MB , Raap V, Muraca D, Sca LB (2018) Materials characterization a simple and “green” technique to synthesize long-term stability colloidal Ag nanoparticles: Fs laser ablation in a biocompatible aqueous medium, vol 140, pp 320–332. https://doi.org/10.1016/j.matchar.2018.04.021

Nagajyothi PC, Pandurangan M, Veerappan M, Kim DH, Sreekanth TVM, Shim J (2017) Green synthesis, characterization and anticancer activity of yttrium oxide nanoparticles. Mater Lett. https://doi.org/10.1016/j.matlet.2017.12.081CrossRef

Pesila NS, Kathleen JS, Searson PC (2003) Relationship between absorbance spectra and particle size distributions for quantum-sized nanocrystals, pp 10412–10415. https://doi.org/10.1021/jp0303218

Pace HE, Rogers NJ, Jarolimek C, Coleman VA, Higgins CP, Ranville JF (2011) Determining transport efficiency for the purpose of counting and sizing nanoparticles via single particle inductively coupled plasma mass spectrometry, pp 9361–9369

Patel NH (2015). Basic principle, working and instrumentation of experimental techniques

Paterson E, Swaffield R (1994) X-ray photoelectron spectroscopy

Plachtova P, Med Z, Zbo R, Varma RS, Maršálek B (2018) Iron and iron oxide nanoparticles synthesized using green tea extract: differences in ecotoxicological profile and ability to degrade malachite green. https://doi.org/10.1021/acssuschemeng.8b00986

Pleul D, Simon F (2008) X ray photoelectron spectroscopy. Polymer Surf Interfaces, pp 71–89. https://doi.org/10.1007/978-3-540-73864-0

Popovic ZV, Mitrovic ZD, Scepanoviv M, Brojčinm M, Askrabic S (2011) Raman scattering on nanomaterials and nanostructures, 74(1): 62–74. https://doi.org/10.1002/andp.201000094

Rana S, Philip J, Raj B (2010) Micelle based synthesis of cobalt ferrite nanoparticles and its characterization using Fourier transform infrared transmission spectrometry and thermogravimetry. Mater Chem Phys 124(1):264–269. https://doi.org/10.1016/j.matchemphys.2010.06.029CrossRef

Rao YS, Kotakadi VS, Prasad TNVKV, Reddy AV, Gopal DS (2013) Green synthesis and spectral characterization of silver nanoparticles from Lakshmi tulasi (Ocimum sanctum) leaf extract. Spectrochim Acta Part A: Mol Biomol Spectrosc 103:156–159

Ritheshraj D, Prasanth S, Vineeshkumar TV, Sudarsanakumar C (2015) Sens Actuators B Chem. https://doi.org/10.1016/j.snb.2015.10.106CrossRef

Roming M, Feldmann C, Avadhut YS (2008) Characterization of noncrystalline nanomaterials: NMR of Zinc Phosphate as a case study. Chem Mater 4:5787–5795CrossRef

Rosbero TMS, Camacho DH (2017) Green preparation and characterization of tentacle-like silver/ copper. Biochem Pharm. https://doi.org/10.1016/j.jece.2017.05.009CrossRef

Roushani M, Mavaei M, Rajabi HR (2015) Graphene quantum dots as novel and green nano-materials for the visible-light-driven photocatalytic degradation of cationic dye, Elsevier B.V. https://doi.org/10.1016/j.molcata.2015.08.011

Salame PH, Pawade VB, Bhanvase BA (2018) Characterization tools and techniques for nanomaterials. In: Nanomaterials for green energy, Elsevier, pp 83–111

Sarmento B, Ferreira D, Veiga F, Ribeiro A (2006) Characterization of insulin-loaded alginate nanoparticles produced by ionotropic pre-gelation through DSC and FTIR studies. Carbohydr Polym 66(1):1–7

Sathyavathi R, Krishna MB, Rao SV, Saritha R, Rao DN (2010) Biosynthesis of silver nanoparticles using Coriandrum Sativum leaf extract and their application in nonlinear optics. Adv Sci Lett 3(2):1–6. https://doi.org/10.1166/asl.2010.1099CrossRef

Saxena A, Tripathi RM, Singh RP (2010) Biological synthesis of silver nanoparticles by using onion (Allium cepa) extract and their antibacterial activity. Digest J Nanomaterials Biostructures 5(2):427–432

Schmidt B, Loeschner K, Hadrup N, Mortensen A, Sloth JJ, Koch CB, Larsen EH (2011) Quantitative characterization of gold nanoparticles by field-flow fractionation coupled online with light scattering detection and inductively coupled plasma mass spectrometry. Anal Chem 83:2461–2468CrossRef

Shameli K, Ahmad MB, Jazayeri SD, Sedaghat S, Shabanzadeh P, Jahangirian H, Abdollahi Y (2012) Synthesis and characterization of polyethylene glycol mediated silver nanoparticles by the green method. Int J Mol Sci 13(6):6639–6650. https://doi.org/10.3390/ijms13066639CrossRef

Shrivastava S, Bera T, Roy A, Singh G, Ramachandrarao P, Dash D (2007) Characterization of enhanced antibacterial effects of novel silver nanoparticles. Nanotechnology 18(22):225103.

Singhal G, Bhavesh R (2011) Biosynthesis of silver nanoparticles using Ocimum sanctum (Tulsi) leaf extract and screening its antimicrobial activity, 2981–2988. https://doi.org/10.1007/s11051-010-0193-y

Song Y, Bhushan B (2007) Finite-element vibration analysis of tapping-mode atomic force microscopy in liquid. Ultramicroscopy 107(10–11):1095–1104CrossRef

Song JY, Jang H, Kim BS (2009) Biological synthesis of gold nanoparticles using Magnolia kobus and Diopyros kaki leaf extracts. Process Biochem 44:1133–1138. https://doi.org/10.1016/j.procbio.2009.06.005CrossRef

Stuart B (2005) Infrared spectroscopy 1(1): 1–20

Subramanian A, Rodriguez-Saona L (2009) Fourier Transform Infrared (FTIR) spectroscopy. In: Sun DW (ed) Infrared spectroscopy for food quality analysis and control. Academic Press, pp 145–178.

Suganya KSU, Govindaraju K, Kumar VG, Dhas TS, Karthick V, Singaravelu G, Elanchezhiyan M (2015) Blue green alga mediated synthesis of gold nanoparticles and its antibacterial efficacy against Gram positive organisms. Mater Sci Eng, C 47:351–356. https://doi.org/10.1016/j.msec.2014.11.043CrossRef

Sun Q, Cai X, Li J, Zheng M, Chen Z, Yu C (2014) Colloids and surfaces a: physicochemical and engineering aspects green synthesis of silver nanoparticles using tea leaf extract and evaluation of their stability and antibacterial activity. Colloids Surf A Physicochem Eng Aspects 444:226–231. https://doi.org/10.1016/j.colsurfa.2013.12.065CrossRef

Suzuki E (2002) High-resolution scanning electron microscopy of immunogold-labelled cells by the use of thin plasma coating of osmium. J Microsc 208(3):153–157CrossRef

Tanaka K, Waki H, Ido Y, Akita S, Yoshida Y (1988) Protein and polymer analyses up to mlz 100 000 by laser ionization time-of-flight mass spectrometry. Rapid Commun Mass Spectrom 2(8):151–153CrossRef

Taylor P, Tiede K, Boxall ABA, Tear SP, Lewis J, David H, Hassellöv M (2008) Food additives & contaminants: part a detection and characterization of engineered nanoparticles in food and the environment, pp 37–41. https://doi.org/10.1080/02652030802007553. Oct 2012

Thovhogi N, Diallo A, Gurib-fakim A, Maaza M (2015) Nanoparticles green synthesis by Hibiscus Sabdariffa flower extract: main physical properties. J Alloys Compd 647:392–396. https://doi.org/10.1016/j.jallcom.2015.06.076CrossRef

Tiede K, Boxall ABA, Tear SP, Lewis J, David H, Hassellöv M (2008) Detection and characterization of engineered nanoparticles in food and the environment. Food Addit Contam 25(7):795–821CrossRef

Tripathi DK et al (2018) Nanomaterials in plants, algae, and microorganisms: concepts and controversies, vol 1. https://doi.org/10.1016/C2016-0-00176-6

Ulug B, Haluk Turkdemir M, Cicek A, Mete A (2015) Role of irradiation in the green synthesis of silver nanoparticles mediated by fig (Ficus carica) leaf extract. Spectrochim Acta Part A Mol Biomol Spectrosc 135:153–161. https://doi.org/10.1016/j.saa.2014.06.142CrossRef

Veisi H, Azizi S, Mohammadi P (2017) Green synthesis of the silver nanoparticles mediated by Thymbra spicata extract and its application as a heterogeneous and recyclable nanocatalyst for catalytic reduction of a variety of dyes in water. J Cleaner Prod. https://doi.org/10.1016/j.jclepro.2017.09.265CrossRef

Walther T (2017) Transmission electron microscopy of nanostructures. In: Microscopy Methods in Nanomaterials Characterization, Elsevier, pp 105–134

Wang ZL (1999) Transmission electron microscopy and spectroscopy of nanoparticles. Charact Nanophase Mater 3:37–80CrossRef

Wang Y, Irudayaraj J, Irudayaraj J (2012) Surface-enhanced Raman spectroscopy at single-molecule scale and its implications in biology

Weckhuysen BM (2004) Ultraviolet-visible spectroscopy, pp 255–270

Weng X, Guo M, Luo F, Chen Z (2017) One-step green synthesis of bimetallic Fe/Ni nanoparticles by eucalyptus leaf extract: Biomolecules identification, characterization and catalytic activity. Chem Eng J 308:904–911. https://doi.org/10.1016/j.cej.2016.09.134CrossRef

Williams DB, Carter CB (2009) The transmission electron microscope. In: Transmission electron microscopy: a textbook for materials science, Springer, Boston, MA, US, pp 3–22

Yamaura M, Camilo RL, Sampaio LC, Macêdo MA, Nakamura M, Toma HE (2004) Preparation and characterization of (3-aminopropyl)triethoxysilane-coated magnetite nanoparticles. J Magn Magn Mater 279(2–3):210–217. https://doi.org/10.1016/j.jmmm.2004.01.094CrossRef

Yang Z, Xing Z, Xu J, Liu X, Lei Y (2018) A new synthetic strategy of Ag-TiO₂ Nanocomposites based on Ligand-to-Metal charge transfer under visible light irradiation: characterizations and photocatalytic activity. Phys Status Solidi (A) 215(14):1800026. https://doi.org/10.1002/pssa.201800026CrossRef

Yu J, Wang H, Zhan J, Huang W (2017) Review of recent UV-Vis and infrared spectroscopy researches on wine detection and discrimination. https://doi.org/10.1080/05704928.2017.1352511

Yuvakkumar R, Suresh J, Nathanael AJ, Sundrarajan M, Hong SI (2014) Novel green synthetic strategy to prepare ZnO nanocrystals using rambutan (Nephelium lappaceum L.) peel extract and its antibacterial applications. Mater Sci Eng, C 41:17–27. https://doi.org/10.1016/j.msec.2014.04.025CrossRef

Zhang J, Higashi K, Limwikrant W, Moribe K, Yamamoto K (2012) Molecular-level characterization of probucol nanocrystal in water by in situ solid-state NMR spectroscopy. Int J Pharm 423(2):571–576. https://doi.org/10.1016/j.ijpharm.2011.11.028CrossRef

Zhang Y, Yu W, Pei L, Lai K, Rasco BA, Huang Y (2015) Rapid analysis of malachite green and leucomalachite green in fish muscles with surface-enhanced resonance Raman scattering. Food Chem 169:80–84. https://doi.org/10.1016/j.foodchem.2014.07.129CrossRef

Title: Characterisation of Green Nanomaterials
Authors: T. Anukiruthika
S. Priyanka
J. A. Moses
C. Anandharamakrishnan
Publisher: Springer Singapore
Book: Green Nanomaterials
Print ISBN: 978-981-15-3559-8

Electronic ISBN: 978-981-15-3560-4

Copyright Year: 2020
DOI: https://doi.org/10.1007/978-981-15-3560-4_3

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