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16-12-2022 | Technical Article

Direct Laser-Deposited IN718 Alloy: Effect of Heat Treatment Route on Microstructural Evolution and Mechanical Properties

Authors: Prayag Burad, Chaitanya Gullipalli, Nikhil Thawari, T. V. K. Gupta

Published in: Journal of Materials Engineering and Performance | Issue 19/2023

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Abstract

The laser-based additive manufacturing techniques are widely used for the refurbishment of worn-out components. The post-processing treatments on additive manufactured parts will improve the material properties and meet the functional requirements. In this study, the multilayered deposition of Inconel 718, a nickel-based alloy is performed using fiber-coupled diode laser with 4 kW maximum output and 5.5 mm spot diameter of direct laser deposition technique. The fabricated samples were subjected to two different stages of heat treatment namely (i) solution-treated and (ii) solution-treated plus direct aged, aiming to study both stages of microstructural and mechanical properties of the deposit. Microstructural observations are carried out using SEM with EDS and microhardness measurements through Vickers indentation method. Further, the influence of different stages of heat treatment on microstructure formation is investigated individually for all multilayered samples. The heat treatment results show that, at different stages, the morphology and hardness differ irrespective of the number of layers. In addition, solution treatment with direct aging reveals precipitation of γ′ (Ni3Ti) and γ′′ (Ni3Nb) phases in the Ni-γ matrix. Further, a 40 to 50% increment in microhardness was obtained and the two-stage heat treatment process has given better results.

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Literature
1.
go back to reference N. Guo and M.C. Leu, Additive Manufacturing: Technology, Applications and Research Needs, Front. Mech. Eng., 2013, 8(3), p 215–243.CrossRef N. Guo and M.C. Leu, Additive Manufacturing: Technology, Applications and Research Needs, Front. Mech. Eng., 2013, 8(3), p 215–243.CrossRef
2.
go back to reference J.C. Ion, Chapter 12-Cladding. In Laser Processing of Engineering Materials Ed. Butterworth-Heinemann: Oxford, 2005, 296–326. J.C. Ion, Chapter 12-Cladding. In Laser Processing of Engineering Materials Ed. Butterworth-Heinemann: Oxford, 2005, 296–326.
3.
go back to reference E. Toyserkani, A.K. Stephen, and F. Corbin, Laser Cladding, 1st ed. CRC Press, Boca Raton, 2004.CrossRef E. Toyserkani, A.K. Stephen, and F. Corbin, Laser Cladding, 1st ed. CRC Press, Boca Raton, 2004.CrossRef
4.
go back to reference J.R. Davis, ASM Specialty Handbook: Nickel, Cobalt, and Their Alloys, ASM International: 2007. J.R. Davis, ASM Specialty Handbook: Nickel, Cobalt, and Their Alloys, ASM International: 2007.
5.
go back to reference C.P. Paul and A.N. Jinoop, Additive Manufacturing, Mc Graw Hill, 2021. C.P. Paul and A.N. Jinoop, Additive Manufacturing, Mc Graw Hill, 2021.
7.
10.
go back to reference C. Gullipalli, N. Thawari, P. Burad, and T.V.K. Gupta, Influence of Normalized Enthalpy on Inconel 718 Morphology in Direct Metal Deposition, Proc. Inst. Mech. Eng. Part E J. Process Mech. Eng., 2022. C. Gullipalli, N. Thawari, P. Burad, and T.V.K. Gupta, Influence of Normalized Enthalpy on Inconel 718 Morphology in Direct Metal Deposition, Proc. Inst. Mech. Eng. Part E J. Process Mech. Eng., 2022.
13.
go back to reference N. Thawari, C. Gullipalli, J.K. Katiyar, and T.V.K. Gupta, In-Process Monitoring of Distortion and Temperature in Multi-Layer Laser Cladding of Stellite 6 and Inconel 718 Alloys, Proc. Inst. Mech. Eng. Part B J. Eng. Manuf., 2022. N. Thawari, C. Gullipalli, J.K. Katiyar, and T.V.K. Gupta, In-Process Monitoring of Distortion and Temperature in Multi-Layer Laser Cladding of Stellite 6 and Inconel 718 Alloys, Proc. Inst. Mech. Eng. Part B J. Eng. Manuf., 2022.
16.
go back to reference J.F. Radavich, The Physical Metallurgy of Cast and Wrought Alloy 718, Superalloy, 2012, 718, p 229–240. J.F. Radavich, The Physical Metallurgy of Cast and Wrought Alloy 718, Superalloy, 2012, 718, p 229–240.
18.
go back to reference C. Radhakrishna, K.P. Rao, and S. Srinivas, Laves Phase in Superalloy 718 Weld Metals, J. Mater. Sci. Lett., 1995, 14(24), p 1810–1812.CrossRef C. Radhakrishna, K.P. Rao, and S. Srinivas, Laves Phase in Superalloy 718 Weld Metals, J. Mater. Sci. Lett., 1995, 14(24), p 1810–1812.CrossRef
19.
go back to reference P. Burad, G. Chaitanya, N. Thawari, J. Bhatt, and T.V.K. Gupta, Characterization of Additive Manufactured Inconel 718 Alloy Using Laser Cladding, Key Eng. Mater., 2021, 882 KEM, p 3–10. P. Burad, G. Chaitanya, N. Thawari, J. Bhatt, and T.V.K. Gupta, Characterization of Additive Manufactured Inconel 718 Alloy Using Laser Cladding, Key Eng. Mater., 2021, 882 KEM, p 3–10.
20.
go back to reference H. Qi, M. Azer, and A. Ritter, Studies of Standard Heat Treatment Effects on Microstructure and Mechanical Properties of Laser Net Shape Manufactured, n.d., 2. H. Qi, M. Azer, and A. Ritter, Studies of Standard Heat Treatment Effects on Microstructure and Mechanical Properties of Laser Net Shape Manufactured, n.d., 2.
21.
go back to reference Y. Zhang, Z. Li, P. Nie, and Y. Wu, Effect of Cooling Rate on the Microstructure of Laser-Remelted INCONEL 718 Coating, Metall. Mater. Trans. A Phys. Metall. Mater. Sci., 2013, 44(12), p 5513–5521.CrossRef Y. Zhang, Z. Li, P. Nie, and Y. Wu, Effect of Cooling Rate on the Microstructure of Laser-Remelted INCONEL 718 Coating, Metall. Mater. Trans. A Phys. Metall. Mater. Sci., 2013, 44(12), p 5513–5521.CrossRef
22.
go back to reference E. Chlebus, K. Gruber, B. Kuźnicka, J. Kurzac, and T. Kurzynowski, Effect of Heat Treatment on the Microstructure and Mechanical Properties of Inconel 718 Processed by Selective Laser Melting, Mater. Sci. Eng. A, 2015, 639, p 647–655.CrossRef E. Chlebus, K. Gruber, B. Kuźnicka, J. Kurzac, and T. Kurzynowski, Effect of Heat Treatment on the Microstructure and Mechanical Properties of Inconel 718 Processed by Selective Laser Melting, Mater. Sci. Eng. A, 2015, 639, p 647–655.CrossRef
23.
go back to reference E. Bassini, G. Marchese, and A. Aversa, Tailoring of the Microstructure of Laser Powder Bed Fused Inconel 718 Using Solution Annealing and Aging Treatments, Metals (Basel), 2021, 11(6), p 921.CrossRef E. Bassini, G. Marchese, and A. Aversa, Tailoring of the Microstructure of Laser Powder Bed Fused Inconel 718 Using Solution Annealing and Aging Treatments, Metals (Basel), 2021, 11(6), p 921.CrossRef
24.
go back to reference D. Deng, Additively Manufactured Inconel 718: Microstructures and Mechanical Properties, Linköping University Electronic Press, 2018.CrossRef D. Deng, Additively Manufactured Inconel 718: Microstructures and Mechanical Properties, Linköping University Electronic Press, 2018.CrossRef
26.
go back to reference A. Sadek, Optimization of the Post Heat Treatment of Additively Manufactured IN718, 31st ASM Heat Treat. Soc. Conf. Expo. Heat Treat 2021 - Ext. Abstr., 2021, 2(5), p 23–29. A. Sadek, Optimization of the Post Heat Treatment of Additively Manufactured IN718, 31st ASM Heat Treat. Soc. Conf. Expo. Heat Treat 2021 - Ext. Abstr., 2021, 2(5), p 23–29.
28.
go back to reference E.M. Fayed, M. Saadati, D. Shahriari, V. Brailovski, M. Jahazi, and M. Medraj, Effect of Homogenization and Solution Treatments Time on the Elevated-Temperature Mechanical Behavior of Inconel 718 Fabricated by Laser Powder Bed Fusion, Sci. Rep., 2021, 11(1), p 1–17. https://doi.org/10.1038/s41598-021-81618-5. (Nature Publishing Group UK)CrossRef E.M. Fayed, M. Saadati, D. Shahriari, V. Brailovski, M. Jahazi, and M. Medraj, Effect of Homogenization and Solution Treatments Time on the Elevated-Temperature Mechanical Behavior of Inconel 718 Fabricated by Laser Powder Bed Fusion, Sci. Rep., 2021, 11(1), p 1–17. https://​doi.​org/​10.​1038/​s41598-021-81618-5. (Nature Publishing Group UK)CrossRef
29.
go back to reference E.M. Fayed, D. Shahriari, M. Saadati, V. Brailovski, M. Jahazi, and M. Medraj, Influence of Homogenization and Solution Treatments Time on the Microstructure and Hardness of Inconel 718 Fabricated by Laser Powder Bed Fusion Process, Materials (Basel), 2020, 13(11), p 2574.CrossRef E.M. Fayed, D. Shahriari, M. Saadati, V. Brailovski, M. Jahazi, and M. Medraj, Influence of Homogenization and Solution Treatments Time on the Microstructure and Hardness of Inconel 718 Fabricated by Laser Powder Bed Fusion Process, Materials (Basel), 2020, 13(11), p 2574.CrossRef
30.
go back to reference D. Kong, C. Dong, X. Ni, L. Zhang, C. Man, J. Yao, Y. Ji, Y. Ying, K. Xiao, X. Cheng, and X. Li, High-Throughput Fabrication of Nickel-Based Alloys with Different Nb Contents via a Dual-Feed Additive Manufacturing System: Effect of Nb Content on Microstructural and Mechanical Properties, J. Alloys Compd., 2019, 785, p 826–837. https://doi.org/10.1016/j.jallcom.2019.01.263. (Elsevier B.V)CrossRef D. Kong, C. Dong, X. Ni, L. Zhang, C. Man, J. Yao, Y. Ji, Y. Ying, K. Xiao, X. Cheng, and X. Li, High-Throughput Fabrication of Nickel-Based Alloys with Different Nb Contents via a Dual-Feed Additive Manufacturing System: Effect of Nb Content on Microstructural and Mechanical Properties, J. Alloys Compd., 2019, 785, p 826–837. https://​doi.​org/​10.​1016/​j.​jallcom.​2019.​01.​263. (Elsevier B.V)CrossRef
31.
34.
go back to reference M. Calandri, D. Manfredi, F. Calignano, E.P. Ambrosio, S. Biamino, R. Lupoi, and D. Ugues, Solution Treatment Study of Inconel 718 Produced by SLM Additive Technique in View of the Oxidation Resistance, Adv. Eng. Mater., 2018, 20(11), p 1–16.CrossRef M. Calandri, D. Manfredi, F. Calignano, E.P. Ambrosio, S. Biamino, R. Lupoi, and D. Ugues, Solution Treatment Study of Inconel 718 Produced by SLM Additive Technique in View of the Oxidation Resistance, Adv. Eng. Mater., 2018, 20(11), p 1–16.CrossRef
36.
go back to reference E. Broitman, Indentation Hardness Measurements at Macro-, Micro-, and Nanoscale: A Critical Overview, Tribol. Lett., 2017, 65(1), p 1–18. (Springer US)CrossRef E. Broitman, Indentation Hardness Measurements at Macro-, Micro-, and Nanoscale: A Critical Overview, Tribol. Lett., 2017, 65(1), p 1–18. (Springer US)CrossRef
37.
go back to reference A. Devaux, L. Nazé, R. Molins, A. Pineau, A. Organista, J.Y. Guédou, J.F. Uginet, and P. Héritier, Gamma Double Prime Precipitation Kinetic in Alloy 718, Mater. Sci. Eng. A, 2008, 486(1–2), p 117–122.CrossRef A. Devaux, L. Nazé, R. Molins, A. Pineau, A. Organista, J.Y. Guédou, J.F. Uginet, and P. Héritier, Gamma Double Prime Precipitation Kinetic in Alloy 718, Mater. Sci. Eng. A, 2008, 486(1–2), p 117–122.CrossRef
Metadata
Title
Direct Laser-Deposited IN718 Alloy: Effect of Heat Treatment Route on Microstructural Evolution and Mechanical Properties
Authors
Prayag Burad
Chaitanya Gullipalli
Nikhil Thawari
T. V. K. Gupta
Publication date
16-12-2022
Publisher
Springer US
Published in
Journal of Materials Engineering and Performance / Issue 19/2023
Print ISSN: 1059-9495
Electronic ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-022-07744-x

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