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Published in: Metallurgical and Materials Transactions B 2/2016

27-01-2016

Effect of Particle Size of Titanium and Nickel on the Synthesis of NiTi by TE-SHS

Authors: Pavel Novák, Tomáš Veselý, Ivo Marek, Petr Dvořák, Vladimír Vojtěch, Pavel Salvetr, Miroslav Karlík, Petr Haušild, Jaromír Kopeček

Published in: Metallurgical and Materials Transactions B | Issue 2/2016

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Abstract

In this work, the influence of the particle size of nickel and titanium on the synthesis of NiTi shape memory alloy by self-propagating high-temperature synthesis (SHS) was investigated. It was found that coarse titanium and nickel powders undergo only a limited SHS reaction. On the other hand, too fine powders support the low-temperature diffusional formation of NiTi intermetallics at 773 K to 1073 K (500 °C to 800 °C) which could then suppress the SHS reaction. The optimum powder fraction of both nickel and titanium to achieve the most intensive SHS reaction is 25 to 45 µm. The influence of the particle size of both nickel and titanium on the reaction mechanism is discussed in terms of the microstructure evolution, phase, and chemical composition changes and thermal effects determined by differential thermal analysis.

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Metadata
Title
Effect of Particle Size of Titanium and Nickel on the Synthesis of NiTi by TE-SHS
Authors
Pavel Novák
Tomáš Veselý
Ivo Marek
Petr Dvořák
Vladimír Vojtěch
Pavel Salvetr
Miroslav Karlík
Petr Haušild
Jaromír Kopeček
Publication date
27-01-2016
Publisher
Springer US
Published in
Metallurgical and Materials Transactions B / Issue 2/2016
Print ISSN: 1073-5615
Electronic ISSN: 1543-1916
DOI
https://doi.org/10.1007/s11663-016-0589-x

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