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Journal of Sol-Gel Science and Technology
Published in: Journal of Sol-Gel Science and Technology 2/2019

05-06-2019 | Original Paper: Nano-structured materials (particles, fibers, colloids, composites, etc.)

Effect of the synthesis method and calcination temperature on the formation of Ni–NiO nanocomposites

Authors: R. B. da Silva, R. A. Pinto, J. M. Soares, A. Franco Jr., M. A. Correa, F. Bohn, J. A. P. da Costa

Published in: Journal of Sol-Gel Science and Technology | Issue 2/2019

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Abstract

We investigate the structural, morphological, chemical, and magnetic properties of Ni–NiO nanocomposites synthesized through two distinct routes, sol–gel and coprecipitation, followed by calcination. By considering several techniques we show that the resulting nanocomposites, as well as their properties, are strongly dependent on both, synthesis method and calcination temperature. Hence, we explore the possibility of tailoring the physical properties of the nanocomposite by modifying production parameters. The results place the employed routes as a simple, low-cost candidate to the production of Ni–NiO nanocomposites, especially nickel oxide.
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Metadata
Title
Effect of the synthesis method and calcination temperature on the formation of Ni–NiO nanocomposites
Authors
R. B. da Silva
R. A. Pinto
J. M. Soares
A. Franco Jr.
M. A. Correa
F. Bohn
J. A. P. da Costa
Publication date
05-06-2019
Publisher
Springer US
Published in
Journal of Sol-Gel Science and Technology / Issue 2/2019
Print ISSN: 0928-0707
Electronic ISSN: 1573-4846
DOI
https://doi.org/10.1007/s10971-019-05038-8

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