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Journal of Materials Engineering and Performance
Published in: Journal of Materials Engineering and Performance 3/2019

14-02-2019

Evolution of Crystallographic Structure of M23C6 Carbide Under Thermal Aging of P91 Steel

Authors: Arūnas Baltušnikas, Albertas Grybėnas, Rita Kriūkienė, Irena Lukošiūtė, Vidas Makarevičius

Published in: Journal of Materials Engineering and Performance | Issue 3/2019

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Abstract

The structural changes of P91 steel after different heat treatment and M23C6 lattice expansion are well described by JMA kinetics law; however, the role of molybdenum on the M23C6 lattice expansion is not clearly revealed. The aim of the present work is to investigate the solubility of molybdenum in M23C6 lattice when iron or chromium atoms are replaced by molybdenum and to examine the effect of crystallographic structure changes on the mechanical properties of thermal aged P91 steel. Rietveld analysis of electrochemically extracted residues from the as-received and thermally aged at 600, 650 and 700 °C steel revealed that it is possible to measure and evaluate quantitatively the fraction of 8c crystallographic site occupation by molybdenum atoms of the M23C6 lattice. It was shown that the value of the site occupation factor plotted in natural logarithmic scale increases linearly and obeys Johnson–Mehl–Avrami kinetic law, giving Avrami exponent navg = 0.3356 and activation energy E = 272 kJ/mol. Hardness measurements of the aged samples indicate that the deterioration of properties is closely coherent to the growth of crystallite size.
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Metadata
Title
Evolution of Crystallographic Structure of M23C6 Carbide Under Thermal Aging of P91 Steel
Authors
Arūnas Baltušnikas
Albertas Grybėnas
Rita Kriūkienė
Irena Lukošiūtė
Vidas Makarevičius
Publication date
14-02-2019
Publisher
Springer US
Published in
Journal of Materials Engineering and Performance / Issue 3/2019
Print ISSN: 1059-9495
Electronic ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-019-03935-1

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