Skip to main content
Top
Published in: Applied Composite Materials 3/2019

16-03-2019

Experimental Investigation of the Effect of Pre-Bond Contamination with Fingerprints and Ageing on the Fracture Toughness of Composite Bonded Joints

Authors: E. Moutsompegka, K. Tserpes, M. Noeske, M. Schlag, K. Brune

Published in: Applied Composite Materials | Issue 3/2019

Log in

Activate our intelligent search to find suitable subject content or patents.

search-config
loading …

Abstract

The effect of the pre-bond contamination with fingerprint (FP), both during the production and the application of adhesively bonded patch repairs on composite aircraft parts, and the cumulative effect of fingerprint and hygrothermal ageing on the fracture toughness of carbon fiber reinforced plastic (CFRP) bonded joints are experimentally investigated. To this end, mode I and mode II fracture toughness tests were conducted on FP contaminated coupons and mode II fracture toughness tests on FP contaminated and aged coupons. The artificial FP was supposed to mimic the accidentally applied fingerprints on the CFRP adherent and was applied on the adherent in the size of a human thumb. The two investigated FP formulations consisted of an artificial hand perspiration solution for the production scenario, and of Skydrol hydraulic-oil for the repair scenario. Three levels of contamination with FP were considered for each scenario. The hygrothermal ageing conditions applied until moisture saturation achieved were 70 °C/85% RH. Prior to bonding, the CFRP adherent surfaces were inspected using full-scale monitoring with optically stimulated electron emission (OSEE), an extended nondestructive testing method, in order to analyze the physicochemical variations at the contaminated surface of the adherents before bonding. The ANOVA statistical method was used to assist the evaluation of the results and the deduction or reliable conclusions. The results revealed that the pre-bond FP contamination of the adherents leads to the reduction of the fracture toughness of the CFRP bonded joints. After-bond hygrothermal ageing under the prescribed conditions had no significant influence on the moisture absorption and load carrying capacity of the joint. However, it influenced the bondline integrity as it led to a significant reduction of the fracture toughness of the joint. The effect of the combination of pre-bond contamination and after-bond hygrothermal ageing is more severe than the two separate effects.

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literature
1.
go back to reference da Silva LFM, Öchsner A, Adams RD. Introduction to adhesive bonding technology. In: da Silva LFM, Öchsner A, Adams RD, editor. Handbook of Adhesion Technology 2nd Ed. Springer-Verlag: Heidelberg; 2011. p. 2–3 da Silva LFM, Öchsner A, Adams RD. Introduction to adhesive bonding technology. In: da Silva LFM, Öchsner A, Adams RD, editor. Handbook of Adhesion Technology 2nd Ed. Springer-Verlag: Heidelberg; 2011. p. 2–3
4.
go back to reference Salvato M, De Vito S, Miglietta M, Massera E, Esposito E, Formisano F, Di Francia G. Hydraulic oil fingerprint contamination detection for aircraft CFRP maintenance by electronic nose. ISOCS/IEEE International Symposium on Olfaction and Electronic Nose (ISOEN); 2017 May 28–23; Montreal, QC. https://doi.org/10.1109/ISOEN.2017.7968872 Salvato M, De Vito S, Miglietta M, Massera E, Esposito E, Formisano F, Di Francia G. Hydraulic oil fingerprint contamination detection for aircraft CFRP maintenance by electronic nose. ISOCS/IEEE International Symposium on Olfaction and Electronic Nose (ISOEN); 2017 May 28–23; Montreal, QC. https://​doi.​org/​10.​1109/​ISOEN.​2017.​7968872
5.
go back to reference Creemers F, Geurts KJ, Noeske M. Influence of surface contaminations on the quality and bond strength of structural adhesive joints. Paper presented at: European Adhesion (EURADH) Conference; 2016 September 21–23; University of Strathclyde, Glasgow, UK Creemers F, Geurts KJ, Noeske M. Influence of surface contaminations on the quality and bond strength of structural adhesive joints. Paper presented at: European Adhesion (EURADH) Conference; 2016 September 21–23; University of Strathclyde, Glasgow, UK
6.
go back to reference Gause RL. A noncontacting scanning photoelectron emission technique for bonding surface cleanliness inspection. Paper presented at: fifth annual NASA NDE workshop; 1989; Florida, USA Gause RL. A noncontacting scanning photoelectron emission technique for bonding surface cleanliness inspection. Paper presented at: fifth annual NASA NDE workshop; 1989; Florida, USA
12.
go back to reference Moutsompegka, E., Tserpes, K.I., Polydoropoulou, P., Tornow, C., Schlag, M., Brune, K., Mayer, B., Pantelakis, S.: Experimental study of the effect of pre-bond contamination with de-icing fluid and ageing on the fracture toughness of composite bonded joints. Fatigue Fract. Eng. Mater. Struct. 40(10), 1581–1591 (2017). https://doi.org/10.1111/ffe.12660 CrossRef Moutsompegka, E., Tserpes, K.I., Polydoropoulou, P., Tornow, C., Schlag, M., Brune, K., Mayer, B., Pantelakis, S.: Experimental study of the effect of pre-bond contamination with de-icing fluid and ageing on the fracture toughness of composite bonded joints. Fatigue Fract. Eng. Mater. Struct. 40(10), 1581–1591 (2017). https://​doi.​org/​10.​1111/​ffe.​12660 CrossRef
13.
go back to reference AITM 1–0053 (2006), AITM, Airbus Test Method, Carbon Fibre Reinforced Plastics, Determination of fracture toughness energy of bonded joints, Mode I, Airbus S.A.S, France, 2006 AITM 1–0053 (2006), AITM, Airbus Test Method, Carbon Fibre Reinforced Plastics, Determination of fracture toughness energy of bonded joints, Mode I, Airbus S.A.S, France, 2006
14.
go back to reference ISO 9022-12, Optics, and photonics -- Environmental test methods -- Part 12: Contamination, International Organization for Standardization, 2012 ISO 9022-12, Optics, and photonics -- Environmental test methods -- Part 12: Contamination, International Organization for Standardization, 2012
15.
go back to reference Tornow, C., Schlag, M., Lima Jr., L.C.M., Stübing, D., Hoffmann, M., Noeske, M., Brune, K., Dieckhoff, S.: Quality assurance concepts for adhesive bonding of composite aircraft structures – characterization of adherent surfaces by extended NDT. J. Adhes. Sci. Technol. 29(21), 2281–2294 (2015). https://doi.org/10.1080/01694243.2015.1055062 CrossRef Tornow, C., Schlag, M., Lima Jr., L.C.M., Stübing, D., Hoffmann, M., Noeske, M., Brune, K., Dieckhoff, S.: Quality assurance concepts for adhesive bonding of composite aircraft structures – characterization of adherent surfaces by extended NDT. J. Adhes. Sci. Technol. 29(21), 2281–2294 (2015). https://​doi.​org/​10.​1080/​01694243.​2015.​1055062 CrossRef
17.
go back to reference ASTM D5573–99 (2005), Standard Practice for Classifying Failure Modes in Fiber-Reinforced-Plastic (FRP) Joints, ASTM International, West Conshohocken, PA, 2005, www.astm.org ASTM D5573–99 (2005), Standard Practice for Classifying Failure Modes in Fiber-Reinforced-Plastic (FRP) Joints, ASTM International, West Conshohocken, PA, 2005, www.​astm.​org
19.
go back to reference AITM 1–0006 (1994), AITM, Airbus Industry Test Method, Carbon Fibre Reinforced Plastics, Determination of interlaminar fracture toughness energy, Mode II, Airbus S.A.S, France, 1994 AITM 1–0006 (1994), AITM, Airbus Industry Test Method, Carbon Fibre Reinforced Plastics, Determination of interlaminar fracture toughness energy, Mode II, Airbus S.A.S, France, 1994
20.
go back to reference DIN EN 2823 Aerospace series—fibre reinforced plastics—determination of the effect of exposure to humid atmosphere on physical and mechanical characteristics. European Association of Aerospace Industries (AECMA), German Institute for Characterization (DIN). Brussels, Belgium, 1998 DIN EN 2823 Aerospace series—fibre reinforced plastics—determination of the effect of exposure to humid atmosphere on physical and mechanical characteristics. European Association of Aerospace Industries (AECMA), German Institute for Characterization (DIN). Brussels, Belgium, 1998
Metadata
Title
Experimental Investigation of the Effect of Pre-Bond Contamination with Fingerprints and Ageing on the Fracture Toughness of Composite Bonded Joints
Authors
E. Moutsompegka
K. Tserpes
M. Noeske
M. Schlag
K. Brune
Publication date
16-03-2019
Publisher
Springer Netherlands
Published in
Applied Composite Materials / Issue 3/2019
Print ISSN: 0929-189X
Electronic ISSN: 1573-4897
DOI
https://doi.org/10.1007/s10443-019-09763-9

Other articles of this Issue 3/2019

Applied Composite Materials 3/2019 Go to the issue

Premium Partners