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01-08-2014

Formation of M_n+1AX_n phases in Ti–Cr–Al–C systems by self-propagating high-temperature synthesis

Authors: Guo-Bing Ying, Xiao-Dong He, Shan-Yi Du, Chun-Cheng Zhu, Yong-Ting Zheng, Yu-Ping Wu, Cheng Wang

Published in: Rare Metals | Issue 4/2014

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Abstract

In this paper, phase composition of the M_n+1AX_n phases by self-propagating high-temperature synthesis (SHS) was determined using Ti, Cr, Al, and carbon black as raw materials. And, phase composition and microstructures of the M_n+1AX_n phases-contained bulk by SHS with the pseudo-hot isostatic pressing (SHS/PHIP) were investigated in Ti–Cr–Al–C systems raw materials. Rietveld XRD refinement was introduced to study the lattice parameters and phase composition of the resultant phases from the SHSed and SHS/PHIPed samples. Ti₂AlC_x, Ti₃AlC_2x, and Cr₂AlC_x by SHS were detected in the Ti–Cr–Al–C systems, as well as the binary carbide of TiC and intermetallics. The mechanical properties of the synthesized bulk samples were determined, exhibiting a high strength and toughness compared with the typical monolithic M_n+1AX_n phase ceramics. It is indicated that the samples prepared by SHS/PHIP are identified to be a strategy for improving the mechanical properties of monolithic M_n+1AX_n phase.

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Title: Formation of M n+1AX n phases in Ti–Cr–Al–C systems by self-propagating high-temperature synthesis
Authors: Guo-Bing Ying
Xiao-Dong He
Shan-Yi Du
Chun-Cheng Zhu
Yong-Ting Zheng
Yu-Ping Wu
Cheng Wang
Publication date: 01-08-2014
Publisher: Nonferrous Metals Society of China
Published in: Rare Metals / Issue 4/2014
Print ISSN: 1001-0521
Electronic ISSN: 1867-7185
DOI: https://doi.org/10.1007/s12598-013-0196-9

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