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2014 | OriginalPaper | Chapter

7. Green Sample Preparation Focusing on Organic Analytes in Complex Matrices

Authors : Vânia Gomes Zuin, Cíntia Alessandra Matiucci Pereira

Published in: Green Chromatographic Techniques

Publisher: Springer Netherlands

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Abstract

This chapter will describe some of the main separation techniques, considered environmentally correct, with special emphasis on sample preparation. To illustrate aspects of green analytical chemistry, techniques for sample preparation and hyphenation capable of miniaturization will be presented, which reduce, replace or eliminate the use of hazardous organic solvents focusing on organic analytes in complex matrices, mainly based on supercritical fluid extraction, membranes, solid phase extraction, matrix solid phase dispersion as well as sorptive extraction techniques, including some examples of their uses.

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Anastas PT (1999) Green chemistry and the role of analytical methodology development. Crit Rev Anal Chem 29(3):167–175

Anastas PTW, Warner JC (1998) Green chemistry: theory and practice. Oxford University Press, New York

Aguinaga N, Campillo N, Vinas P, Hernandez-Cordoba M (2009) Solid-phase microextraction coupled to gas chromatography-mass spectrometry for the analysis of famoxadone in wines, fruits, and vegetables. Spectrosc Lett 42(6–7):320–326. doi:Pii 917313600, 10.1080/00387010903178723

Alonso M, Cerdan L, Godayol A, Antico E, Sanchez JM (2011) Headspace needle-trap analysis of priority volatile organic compounds from aqueous samples: Application to the analysis of natural and waste waters. J Chromatogr A 1218(45):8131–8139. doi:10.1016/j.chroma.2011.09.042

Barriada-Pereira M, Serodio P, Gonzalez-Castro MJ, Nogueira JMF (2010) Determination of organochlorine pesticides in vegetable matrices by stir bar sorptive extraction with liquid desorption and large volume injection-gas chromatography-mass spectrometry towards compliance with European Union directives. J Chromatogr A 1217(1):119–126. doi:10.1016/j.chroma.2009.10.076

Barker SA (2007) Matrix solid phase dispersion (MSPD). J Biochem Biophys Methods 70(2):151–162. doi:10.1016/j.jbbm.2006.06.005

Basheer C, Vetrichelvan M, Valiyaveettil S, Lee HK (2007) On-site polymer-coated hollow fiber membrane microextraction and gas chromatography-mass spectrometry of polychlorinated biphenyls and polybrominated diphenyl ethers. J Chromatogr A 1139(2):157–164. doi:10.1016/j.chroma.2006.11.008

Bicchi C, Iori C, Rubiolo P, Sandra P (2002) Headspace sorptive extraction (HSSE), stir bar sorptive extraction (SBSE), and solid phase microextraction (SPME) applied to the analysis of roasted arabica coffee and coffee brew. J Agr Food Chem 50(3):449–459. doi:10.1021/Jf010877x

Bicchi C, Cordero C, Iori C, Rubiolo P, Sandra P, Yariwake JH, Zuin VG (2003) SBSE-GC-ECD/FPD in the analysis of pesticide residues in Passiflora alata Dryander herbal teas. J Agric Food Chem 51(1):27–33. doi:10.1021/jf020630f

Bicchi C, Cordero C, Liberto E, Rubiolo P, Sgorbini B (2004) Automated headspace solid-phase dynamic extraction to analyse the volatile fraction of food matrices. J Chromatogr A 1024(1–2):217–226. doi:10.1016/j.choma.2003.10.009

Bicchi C, Cordero C, Liberto E, Rubiolo P, Sgorbini B, David F, Sandra P (2005) Dual-phase twisters: a new approach to headspace sorptive extraction and stir bar sorptive extraction. J Chromatogr A 1094(1–2):9–16. doi:10.1016/j.chroma.2005.07.099

Blasco C, Fernandez M, Pico Y, Font G (2004) Comparison of solid-phase microextraction and stir bar sorptive extraction for determining six organophosphorus insecticides in honey by liquid chromatography-mass spectrometry. J Chromatogr A 1030(1–2):77–85. doi:10.1016/j.chroma.2003.11.037

Bogialli S, Di Corcia A (2007) Matrix solid-phase dispersion as a valuable tool for extracting contaminants from foodstuffs. J Biochem Biophys Methods 70(2):163–179. doi:10.1016/j.jbbm.2006.07.007

Bourdat-Deschamps M, Daudin JJ, Barriuso E (2007) An experimental design approach to optimise the determination of polycyclic aromatic hydrocarbons from rainfall water using stir bar sorptive extraction and high performance liquid chromatography-fluorescence detection. J Chromatogr A 1167(2):143–153. doi:10.1016/j.chroma.2007.08.025

Bruheim I, Lord H, Pawliszyn J (2003) Comments on “Helical sorbent for fast sorption and desorption in solid-phase microextraction-gas chromatographic analysis”. Anal Chem 75(15):3946–3949. doi:10.1021/Ac0264271

Burkhardt D, Mosandl A (2003) Biogenetic studies in Syringa vulgaris L.: bioconversion of O-18(H-2)-labeled precursors into lilac aldehydes and lilac alcohols. J Agric Food Chem 51(25):7391–7395. doi:10.1021/Jf0304674

Calvano CD, Jensen ON, Zambonin CG (2009) Selective extraction of phospholipids from dairy products by micro-solid phase extraction based on titanium dioxide microcolumns followed by MALDI-TOF-MS analysis. Anal Bioanal Chem 394(5):1453–1461. doi:10.1007/s00216–009-2812-y

Calvano CD, Aresta A, Zambonin CG (2010) Detection of hazelnut oil in extra-virgin olive oil by analysis of polar components by micro-solid phase extraction based on hydrophilic liquid chromatography and MALDI-ToF mass spectrometry. J Mass Spectrom 45(9):981–988. doi:10.1002/Jms.1753

Campillo N, Penalver R, Lopez-Garcia I, Hernandez-Cordoba M (2009) Headspace solid-phase microextraction for the determination of volatile organic sulphur and selenium compounds in beers, wines and spirits using gas chromatography and atomic emission detection. Journal of Chromatography A 1216(39):6735–6740. doi:10.1016/j.chroma.2009.08.019

Capriotti AL, Cavaliere C, Giansanti P, Gubbiotti R, Samperi R, Lagana A (2010) Recent developments in matrix solid-phase dispersion extraction. J Chromatogr A 1217(16):2521–2532. doi:10.1016/j.chroma.2010.01.030

Chen SJ, Cheng FC, Jen JF (2010) On-line microdialysis coupled solid-phase extraction to decrease matrix interference in the HPLC analysis of urinary ketamine and its metabolites. J Sep Sci 33(13):2010–2016. doi:10.1002/jssc.201000002

Cheng CY, Wang YC, Ding WH (2011) Determination of triclosan in aqueous samples using solid-phase extraction followed by on-line derivatization gas chromatography-mass spectrometry. Anal Sci 27(2):197–202

Covaci A, Mashiya JG, Molope I, Tshiame I, Molatlhegi R, Ngobeni P (2010) Miniaturized method based on matrix solid-phase dispersion for the rapid screening of 36 pesticides in agricultural food commodities. Anal Lett 43(7–8):1400–1410. doi:10.1080/00032710903518807

Cunha SS, Fernandes JO, Oliveira MBPP (2006) Quantification of free and esterified sterols in Portuguese olive oils by solid-phase extraction and gas chromatography-mass spectrometry. J Chromatogr A 1128(1–2):220–227. doi:10.1016/j.chroma.2006.06.039

De LGuardiaM, Garrigues S (2011) Challenges in green analytical chemistry. RSC Publishing, Cambridge

De Villiers A, Vanhoenacker G, Lynen F, Sandra P (2004) Stir bar sorptive extraction-liquid desorption applied to the analysis of hop-derived bitter acids in beer by micellar electrokinetic chromatography. Electrophoresis 25(4–5):664–669. doi:10.1002/elps.200305758

Duan C, Shen Z, Wu D, Guan Y (2011) Recent developments in solid-phase microextraction for on-site sampling and sample preparation. TrAC Trends Anal Chem 30(10):1568–1574

Eom IY, Tugulea AM, Pawliszyn J (2008) Development and application of needle trap devices. J Chromatogr A 1196:3–9. doi:10.1016/j.chroma.2008.02.090

Fan WL, Shen HY, Xu Y (2011) Quantification of volatile compounds in Chinese soy sauce aroma type liquor by stir bar sorptive extraction and gas chromatography-mass spectrometry. J Sci Food Agr 91(7):1187–1198. doi:10.1002/Jsfa.4294

Franc C, David F, Revel G de (2009) Multi-residue off-flavour profiling in wine using stir bar sorptive extraction-thermal desorption-gas chromatography-mass spectrometry. J Chromatogr A 1216(15):3318–3327. doi:10.1016/j.chroma.2009.01.103

Garcia-Lopez M, Canosa P, Rodriguez I (2008) Trends and recent applications of matrix solid-phase dispersion. Anal Bioanal Chem 391(3):963–974. doi:10.1007/s00216-008-1898-y

Gilbert-Lopez B, Garcia-Reyes JF, Lozano A, Fernandez-Alba AR, Molina-Diaz A (2010) Large-scale pesticide testing in olives by liquid chromatography-electrospray tandem mass spectrometry using two sample preparation methods based on matrix solid-phase dispersion and QuEChERS. J Chromatogr A 1217(39):6022–6035. doi:S0021-9673(10)00998-2 [pii], 10.1016/j.chroma.2010.07:062

Gonzalez-Marino I, Quintana JB, Rodriguez I, Schrader S, Moeder M (2011) Fully automated determination of parabens, triclosan and methyl triclosan in wastewater by microextraction by packed sorbents and gas chromatography-mass spectrometry. Anal Chim Acta 684(1–2):59–66. doi:10.1016/j.aca.2010.10.049

Gonzalez-Ruiz V, Olives AI, Martin MA (2011) SPE/RP-HPLC using C1 columns: an environmentally friendly alternative to conventional reverse-phase separations for quantitation of beta-carboline alkaloids in human serum samples. Anal Bioanal Chem 400(2):395–401. doi:10.1007/s00216-010-4562-2

Greenwood R, Mills GA, Roig B (2007) Introduction to emerging tools and their use in water monitoring. Trac-Trends Anal Chem 26(4):263–267. doi:10.1016/j.trac.2006.12.006

Guerrero ED, Bastante MJC, Mejias RC, Marin RN, Barroso CG (2011) Characterization and differentiation of Sherry Brandies using their aromatic profile. J Agr Food Chem 59(6):2410–2415. doi:10.1021/Jf104409n

Hampel D, Mosandl A, Wust M (2005) Biosynthesis of mono- and sesquiterpenes in carrot roots and leaves (Daucus carota L.): metabolic cross talk of cytosolic mevalonate and plastidial methylerythritol phosphate pathways. Phytochemistry 66(3):305–311. doi:10.1016/j.phytochem.2004.12.010

Hsu CL, Ding WH (2009) Determination of low-molecular-weight dicarboxylic acids in atmospheric aerosols by injection-port derivatization and gas chromatography-mass spectrometry. Talanta 80(2):1025–1028. doi:10.1016/j.talanta.2009.07.047

http://www.nemi.gov/

http://www.epa.gov/sw-846/pdfs/3510c.pdf

http://www.epa.gov/sw-846/pdfs/3540c.pdf

Hylton K, Mitra S (2007) Automated, on-line membrane extraction. J Chromatogr A 1152(1–2):199–214. doi:10.1016/j.chroma.2006.12.047

Hyotylainen T, Riekkola ML (2005) Solid-phase extraction or liquid chromatography coupled on-line with gas chromatography in the analysis of biological samples. J Chromatogr B Analyt Technol Biomed Life Sci 817(1):13–21. doi:S1570023204003964 [pii], 10.1016/j.jchromb.2004.04:033

Iparraguirre A, Prieto A, Navarro P, Olivares M, Fernandez LA, Zuloaga O (2011) Optimisation of stir bar sorptive extraction and in-tube derivatisation-thermal desorption-gas chromatography-mass spectrometry for the determination of several endocrine disruptor compounds in environmental water samples. Anal Bioanal Chem 401(1):339–352. doi:10.1007/s00216-011-5074-4

Insa S, Antico E, Ferreira V (2005) Highly selective solid-phase extraction and large volume injection for the robust gas chromatography-mass spectrometric analysis of TCA and TBA in wines. J Chromatogr A 1089(1–2):235–242. doi:10.1016/j.chroma.2005.06.061

Ishizaki A, Saito K, Hanioka N, Narimatsu S, Kataoka H (2010) Determination of polycyclic aromatic hydrocarbons in food samples by automated on-line in-tube solid-phase microextraction coupled with high-performance liquid chromatography-fluorescence detection. J Chromatogr A 1217(35):5555–5563. doi:S0021–9673(10)00868-X [pii], 10.1016/j.chroma.2010.06:068

Jakubowska N, Polkowska Z, Namiesnik J, Przyjazny A (2005) Analytical applications of membrane extraction for biomedical and environmental liquid sample preparation. Crit Rev Anal Chem 35(3):217–235. doi:10.1080/10408340500304032

Juan-Garcia A, Manes J, Font G, Pico Y (2004) Evaluation of solid-phase extraction and stir-bar sorptive extraction for the determination of fungicide residues at low-mu g kg(-1) levels in grapes by liquid chromatography-mass spectrometry. J Chromatogr A 1050(2):119–127. doi:10.1016/j.chroma.2004.08.026

Jochmann MA, Kmiecik MP, Schmidt TC (2006) Solid-phase dynamic extraction for the enrichment of polar volatile organic compounds from water. J Chromatogr A 1115(1–2):208–216. doi:10.1016/j.chroma.2006.02.061

Kanimozhi S, Basheer C, Narasimhan K, Liu L, Koh S, Xue F, Choolani M, Lee HK (2011) Application of porous membrane protected micro-solid-phase-extraction combined with gas chromatography-mass spectrometry for the determination of estrogens in ovarian cyst fluid samples. Anal Chim Acta 687(1):56–60. doi:10.1016/j.aca.2010.12.007

Kaljurand M, Koel M (2011) Recent advancements on greening analytical separation. Cri Rev Anal Chem 41(1):2–20. doi:Pii 933412012, 10.1080/10408347.2011.539420

Kawaguchi M, Ishii Y, Sakui N, Okanouchi N, Ito R, Inoue K, Saito K, Nakazawa H (2004) Stir bar sorptive extraction with in situ derivatization and thermal desorption-gas chromatography-mass spectrometry in the multi-shot mode for determination of estrogens in river water samples. J Chromatogr A 1049(1–2):1–8. doi:10.1016/j.chroma.2004.08.013

Keith LH, Gron LU, Young JL (2007) Green analytical methodologies. Chem Rev 107(6):2695–2708. doi:10.1021/Cr068359e

Klein DR, Flannelly DF, Schultz MM (2010) Quantitative determination of triclocarban in wastewater effluent by stir bar sorptive extraction and liquid desorption-liquid chromatography-tandem mass spectrometry. J Chromatogr A 1217(11):1742–1747. doi:10.1016/j.chroma.2010.01.028

Kloskowski A, Chrzanowski W, Pilarczyk M, Namiesnik J (2007) Modern techniques of sample preparation for determination of organic analytes by gas chromatography. Crit Rev Anal Chem 37(1):15–38. doi:10.1080/10408340600976663

Kouzayha A, Al Iskandarani M, Mokh S, Rabaa AR, Budzinski H, Jaber F (2011) Optimization of a solid-phase extraction method using centrifugation for the determination of 16 polycyclic aromatic hydrocarbons in water. J Agric Food Chem 59(14):7592–7600. doi:10.1021/Jf200123v

Koel M, Kaljurand M (2006) Application of the principles of green chemistry in analytical chemistry. Pure Appl Chem 78(11):1993–2002. doi:10.1351/pac200678111993

Kreck M, Scharrer A, Bilke S, Mosandl A (2002) Enantioselective analysis of monoterpene compounds in essential oils by stir bar sorptive extraction (SBSE)-enantio-MDGC-MS. Flavour Frag J 17(1):32–40

Kreck M, Puschel S, Wust M, Mosandl A (2003) Biogenetic studies in syringa vulgaris L.: synthesis and bioconversion of deuterium-labeled precursors into lilac aldehydes and lilac alcohols. J Agric Food Chem 51(2):463–469

Kristenson EM, Ramos L, Brinkman UAT (2006) Recent advances in matrix solid-phase dispersion. Trac-Trends Anal Chem 25(2):96–111

Kronholm J, Hartonen K, Riekkola ML (2007) Analytical extractions with water at elevated temperatures and pressures. Trac-Trends Anal Chem 26(5):396–412. doi:10.1016/j.trac.2007.03.004

Majors RE (1991) An overview of sample preparation. Lc Gc-Mag Sep Sci 9(1):16–18

Melo LP, Queiroz RH, Queiroz ME (2011) Automated determination of rifampicin in plasma samples by in-tube solid-phase microextraction coupled with liquid chromatography. J Chromatogr B Analyt Technol Biomed Life Sci 879(24):2454–2458. doi:S1570-0232(11)00438-7 [pii], 10.1016/j.jchromb.2011.06:041

Mieth M, Kischkel S, Schubert JK, Hein D, Miekisch W (2009) Multibed needle trap devices for on site sampling and preconcentration of volatile breath biomarkers. Anal Chem 81(14):5851–5857. doi:10.1021/Ac9009269

Moeder M, Bauer C, Popp P, Pinxteren M van, Reemtsma T (2012) Determination of pesticide residues in wine by membrane-assisted solvent extraction and high-performance liquid chromatography-tandem mass spectrometry. Anal Bioanal Chem 403(6):1731–1741. doi:10.1007/s00216-012-5956-0

Morlock G, Kopacz S (2008) Fast and precise SBSE-HPTLC/FLD method for quantification of six polycyclic aromatic hydrocarbons frequently found in water. J Liq Chromatogr R T 31(13):1925–1942. doi:10.1080/10826070802194856

Musshoff F, Lachenmeier DW, Kroener L, Madea B (2002) Automated headspace solid-phase dynamic extraction for the determination of amphetamines and synthetic designer drugs in hair samples. J Chromatogr A 958(1–2):231–238

Namiesnik J (2001) Green analytical chemistry—some remarks. J Sep Sci 24(2):151–153

do Nascimento I, Schossler P, Freitas LS, Melecchi MIS, Vale MGR, Caramao EB (2004) Selective extraction of benzoic acid from landfill leachate by solid-phase extraction and ion-exchange chromatography. J Chromatogr A 1027(1–2):167–170. doi:10.1016/j.chroma.2003.10.044

Navarro M, Pico Y, Marin R, Manes J (2002) Application of matrix solid-phase dispersion to the determination of a new generation of fungicides in fruits and vegetables. J Chromatogr A 968(1–2):201–209

Nevado JJB, Penalvo GC, Dorado RMR (2005) Method development and validation for the separation and determination of omeprazole enantiomers in pharmaceutical preparations by capillary electrophoresis. Anal Chim Acta 533(2):127–133. doi:10.1016/j.aca.2004.11.018

Ochiai N, Sasamoto K, Kanda H, Yamagami T, David F, Tienpont B, Sandra P (2005) Optimization of a multi-residue screening method for the determination of 85 pesticides in selected food matrices by stir bar sorptive extraction and thermal desorption GC-MS. J Sep Sci 28(9–10):1083–1092. doi:10.1002/jssc.200500017

Ochiai N, Sasamoto K, Kanda H, Nakamura S (2006) Fast screening of pesticide multiresidues in aqueous samples by dual stir bar sorptive extraction-thermal desorption-low thermal mass gas chromatography-mass spectrometry. Journal of Chromatography A 1130(1):83–90. doi:10.1016/j.chroma.2006.06.032

Ochiai N, Sasamoto K, Kanda H, Pfannkoch E (2008) Sequential stir bar sorptive extraction for uniform enrichment of trace amounts of organic pollutants in water samples. J Chromatogr A 1200(1):72–79. doi:10.1016/j.chroma.2008.05.069

Olbe L, Carlsson E, Lindberg P (2003) A proton-pump inhibitor expedition: the case histories of omeprazole and esomeprazole. Nat Rev Drug Discov 2(2):132–139. doi:10.1038/Nrd1010

Papadopoulos N, Gikas E, Zalidis G, Tsarbopoulos A (2009) Simultaneous Determination of herbicide terbuthylazine and its major hydroxy and dealkylated metabolites in typha latifolia L. Wetland plant using SPE and HPLC-DAD. J Liq Chromatogr R T 32(20):2975–2992. doi:Pii 916846758, 10.1080/10826070903320566

Pico Y, Fernandez M, Ruiz MJ, Font G (2007) Current trends in solid-phase-based extraction techniques for the determination of pesticides in food and environment. J Biochem Biophys Methods 70(2):117–131. doi:10.1016/j.jbbm.2006.10.010

Poole CF (2003) New trends in solid-phase extraction. Trac-Trend Anal Chem 22(6):362–373. doi:10.1016/S0165-9936(03)00605-8

Ponnusamy VK, Jen JF (2011) A novel graphene nanosheets coated stainless steel fiber for microwave assisted headspace solid phase microextraction of organochlorine pesticides in aqueous samples followed by gas chromatography with electron capture detection. J Chromatogr A 1218(39):6861–6868. doi:10.1016/j.chroma.2011.08.019

Popp P, Bauer C, Hauser B, Keil P, Wennrich L (2003) Extraction of polycyclic aromatic hydrocarbons and organochlorine compounds from water: a comparison between solid-phase microextraction and stir bar sorptive extraction. J Sep Sci 26(9–10):961–967. doi:10.1002/jssc.200301398

Prieto A, Basauri O, Rodil R, Usobiaga A, Fernandez LA, Etxebarria N, Zuloaga O (2010) Stir-bar sorptive extraction: a view on method optimisation, novel applications, limitations and potential solutions. J Chromatogr A 1217(16):2642–2666. doi:10.1016/j.chroma.2009.12.051

Qi DJ, Kang XJ, Chen LQ, Zhang YY, Wei HM, Gu ZZ (2008) Electrospun polymer nanofibers as a solid-phase extraction sorbent for the determination of trace pollutants in environmental water. Anal Bioanal Chem 390(3):929–938. doi:10.1007/s00216-007-1747-4

Ramos L (2012) Critical overview of selected contemporary sample preparation techniques. J Chromatogr A 1221:84–98. doi:10.1016/j.chroma.2011.11.011

Ramos L, Ramos JJ, Brinkman UA (2005) Miniaturization in sample treatment for environmental analysis. Anal Bioanal Chem 381(1):119–140. doi:10.1007/s00216-004-2906-5

Raynie DE (2004) Modern extraction techniques. Anal Chem 76(16):4659–4664. doi:10.1021/Ac040117w

Ridgway K, Lalljie SPD, Smith RM (2007) Sample preparation techniques for the determination of trace residues and contaminants in foods. J Chromatogr A 1153(1–2):36–53. doi:10.1016/j.chroma.2007.01.134

Ridgway K, Lalljie SPD, Smith RM (2010) An alternative method for analysis of food taints using stir bar sorptive extraction. Anal Chim Acta 677(1):29–36. doi:10.1016/j.aca.2010.01.049

Rodil R, Moeder M (2008) Stir bar sorptive extraction coupled to thermodesorption-gas chromatography-mass spectrometry for the determination of insect repelling substances in water samples. J Chromatogr A 1178(1–2):9–16. doi:S0021-9673(07)02003-1 [pii], 10.1016/j.chroma.2007.11:051

Rodrigues SA, Caldas SS, Primel EG (2010) A simple; efficient and environmentally friendly method for the extraction of pesticides from onion by matrix solid-phase dispersion with liquid chromatography-tandem mass spectrometric detection. Anal Chim Acta 678(1):82–89. doi:10.1016/j.aca.2010.08.026

do Rosario PMA, Nogueira JMF (2006) Combining stir bar sorptive extraction and MEKC for the determination of polynuclear aromatic hydrocarbons in environmental and biological matrices. Electrophoresis 27(23):4694–4702. doi:10.1002/elps.200600210

Rubert J, Soler C, Manes J (2011) Evaluation of matrix solid-phase dispersion (MSPD) extraction for multi-mycotoxin determination in different flours using LC-MS/MS. Talanta 85(1):206–215. doi:10.1016/j.talanta.2011.03.046

Sanchez-Rojas F, Bosch-Ojeda C, Cano-Pavon JM (2009) A review of stir bar sorptive extraction. Chromatographia 69:S79–S94. doi:10.1365/s10337-008-0687-2

Saito K, Yagi K, Ishizaki A, Kataoka H (2010) Determination of anabolic steroids in human urine by automated in-tube solid-phase microextraction coupled with liquid chromatography-mass spectrometry. J Pharm Biomed Anal 52(5):727–733. doi:S0731-7085(10)00113-5 [pii], 10.1016/j.jpba.2010.02:027

Sandra P, Tienpont B, Vercammen J, Tredoux A, Sandra T, David F (2001) Stir bar sorptive extraction applied to the determination of dicarboximide fungicides in wine. J Chromatogr A 928(1):117–126

Sandra P, Tienpont B, David F (2003) Multi-residue screening of pesticides in vegetables, fruits and baby food by stir bar sorptive extraction-thermal desorption-capillary gas chromatography-mass spectrometry. J Chromatogr A 1000(1–2):299–309. doi:10.1016/S0021-9673(03)00508-9

Sasamoto K, Ochiai N, Kanda H (2007) Dual low thermal mass gas chromatography-mass spectrometry for fast dual-column separation of pesticides in complex sample. Talanta 72(5):1637–1643. doi:10.1016/j.talanta.2007.03.020

Serodio P, Nogueira JMF (2006) Considerations on ultra-trace analysis of phthalates in drinking water. Water Res 40(13):2572–2582. doi:10.1016/j.watres.2006.05.002

Sewenig S, Bullinger D, Hener U, Mosandl A (2005) Comprehensive authentication of (E)-alpha(beta)-ionone from raspberries, using constant flow MDGC-C/P-IRMS and Enantio-MDGC-MS. J Agric Food Chem 53(4):838–844. doi:10.1021/Jf040356k

Tan BLL, Hawker DW, Muller JF, Tremblay LA, Chapman HF (2008) Stir bar sorptive extraction and trace analysis of selected endocrine disruptors in water, biosolids and sludge samples by thermal desorption with gas chromatography-mass spectrometry. Water Res 42(1–2):404–412. doi:10.1016/j.watres.2007.07.032

Tholl D, Boland W, Hansel A, Loreto F, Rose US, Schnitzler JP (2006) Practical approaches to plant volatile analysis. Plant J 45(4):540–560. doi:TPJ2612 [pii], 10.1111/j.1365-313X.2005.02612.x

Tobiszewski M, Mechlinska A, Zygmunt B, Namiesnik J (2009) Green analytical chemistry in sample preparation for determination of trace organic pollutants. Trac-Trend Anal Chem 28(8):943–951. doi:10.1016/j.trac.2009.06.001

Tobiszewski M, Mechlinska A, Namiesnik J (2010) Green analytical chemistry-theory and practice. Chem Soc Rev 39(8):2869–2878. doi:10.1039/B926439f

Trevisan MGP, Poppi RJ (2006) Química analítica de processos. Química Nova 29(5):1065–1071

Turner C (2006) Overview of modern extraction techniques for food and agricultural samples. Acs Sym Ser 926:3–19

Vinas P, Campillo N, Martinez-Castillo N, Hernandez-Cordoba M (2009) Solid-phase microextraction on-fiber derivatization for the analysis of some polyphenols in wine and grapes using gas chromatography-mass spectrometry. J Chromatogr A 1216(9):1279–1284. doi:10.1016/j.chroma.2008.12.058

Vinas P, Campillo N, Martinez-Castillo N, Hernandez-Cordoba M (2010) Comparison of two derivatization-based methods for solid-phase microextraction-gas chromatography-mass spectrometric determination of bisphenol A, bisphenol S and biphenol migrated from food cans. Anal Bioanal Chem 397(1):115–125. doi:10.1007/s00216-010-3464-7

Wille SM, Lambert WE (2007) Recent developments in extraction procedures relevant to analytical toxicology. Anal Bioanal Chem 388(7):1381–1391. doi:10.1007/s00216-007-1294-z

Wilson ID, Brinkman UAT (2007) Hype and hypernation: multiple hyphenation of column liquid chromatography and spectroscopy. Trac-Trends Anal Chem 26(9):847–854. doi:10.1016/j.trac.2007.07.007

Wu F, Lu WP, Chen JH, Liu W, Zhang L (2010) Single-walled carbon nanotubes coated fibers for solid-phase microextraction and gas chromatography-mass spectrometric determination of pesticides in Tea samples. Talanta 82(3):1038–1043. doi:10.1016/j.talanta.2010.06.016

Yang TJ, Tsai FJ, Chen CY, Yang TCC, Lee MR (2010) Determination of additives in cosmetics by supercritical fluid extraction on-line headspace solid-phase microextraction combined with gas chromatography-mass spectrometry. Anal Chim Acta 668(2):188–194. doi:10.1016/j.aca.2010.04.001

Yamaguchi C, Lee WY (2010) A cost effective, sensitive, and environmentally friendly sample preparation method for determination of polycyclic aromatic hydrocarbons in solid samples. J Chromatogr A 1217(44):6816–6823. doi:10.1016/j.chroma.2010.08.055

Yu YQ, Gilar M, Kaska J, Gebler JC (2005) A rapid sample preparation method for mass spectrometric characterization of N-linked glycans. Rapid Commun Mass Spectrom 19(16):2331–2336. doi:10.1002/Rcm.2067

Zuin VG, Lopes AL, Yariwake JH, Augusto F (2004) Application of a novel sol-gel polydimethylsiloxane-poly(vinyl alcohol) solid-phase microextraction fiber for gas chromatographic determination of pesticide residues in herbal infusions. J Chromatogr A 1056(1–2):21–26. doi:10.1016/j.chroma.2004.07.074

Zuin VG, Montero L, Bauer C, Popp P (2005) Stir bar sorptive extraction and high-performance liquid chromatography-fluorescence detection for the determination of polycyclic aromatic hydrocarbons in Mate teas. J Chromatogr A 1091(1–2):2–10

Zuin VG, Schellin M, Montero L, Yariwake JH, Augusto F, Popp P (2006) Comparison of stir bar sorptive extraction and membrane-assisted solvent extraction as enrichment techniques for the determination of pesticide and benzo[a]pyrene residues in Brazilian sugarcane juice. J Chromatogr A 1114(2):180–187. doi:10.1016/j.chroma.2006.03.035

Zygmunt B, Jastrzebska A, Namiesnik J (2001) Solid phase microextraction—a convenient tool for the determination of organic pollutants in environmental matrices. Crit Rev Anal Chem 31(1):1–18

Title: Green Sample Preparation Focusing on Organic Analytes in Complex Matrices
Authors: Vânia Gomes Zuin
Cíntia Alessandra Matiucci Pereira
Publisher: Springer Netherlands
Book: Green Chromatographic Techniques
Print ISBN: 978-94-007-7734-7

Electronic ISBN: 978-94-007-7735-4

Copyright Year: 2014
DOI: https://doi.org/10.1007/978-94-007-7735-4_7

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