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Wood Science and Technology

Hydroxyl accessibility in wood by deuterium exchange and ATR-FTIR spectroscopy: methodological uncertainties

  • 13-05-2017
  • Original
Published in:
Authors
Asghar Tarmian
Ingo Burgert
Emil Engelund Thybring
Published in
Wood Science and Technology | Issue 4/2017

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Abstract

The accessibility of wood hydroxyls to water is commonly studied by infrared spectroscopy after deuteration where water-interacting hydroxyls have their H exchanged for D. In this study, the hydroxyl accessibility is determined with ATR-FTIR spectroscopy after deuteration of specimens with liquid D2O. Several factors are examined to reveal the uncertainties involved in the accessibility determination. Despite the fact that specimens were able to interact with water vapour after deuteration and drying, producing a freshly cut surface just before measurement limited the effect of re-exchange of hydroxyls and gave for most batches reproducible results.

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previous article Transition characteristics of a carbonized wood cell wall investigated by scanning thermal microscopy (SThM)
next article Hydroalcoholic extracts from the bark of Quercus suber L. (Cork): optimization of extraction conditions, chemical composition and antioxidant potential
Title
Hydroxyl accessibility in wood by deuterium exchange and ATR-FTIR spectroscopy: methodological uncertainties
Authors
Asghar Tarmian
Ingo Burgert
Emil Engelund Thybring
Publication date
13-05-2017
Publisher
Springer Berlin Heidelberg
Published in
Wood Science and Technology / Issue 4/2017
Print ISSN: 0043-7719
Electronic ISSN: 1432-5225
DOI
https://doi.org/10.1007/s00226-017-0922-9
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