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Published in: Cellulose 13/2021

21-07-2021 | Original Research

Layer-by-layer assembly of cationic guar gum, cellulose nanocrystals and hydroxypropyl methylcellulose based multilayered composite films

Authors: Arun Saini, Deepak Sharma, Yuanyuan Xia, Aman Saini, Xiangyu You, Ying Su, Lihong Chen, Chandravati Yadav, Xinping Li

Published in: Cellulose | Issue 13/2021

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Abstract

Eco-friendly sustainable materials provide an appealing template to replace contemporary synthetic-nonrenewable resource-based materials while maintaining the acceptable material properties to meet the performance requirements. Here, a layer-by-layer (LBL) self-assembly technique was used for fabricating multilayer composite films using all bio-based polymers/polysaccharides, i.e. cationic guar gum (CGg), carboxylated cellulose nanocrystals (cCNCs) and hydroxypropyl methylcellulose (HPMC). A five layered composite film was fabricated by depositing polymeric layers as follows: CGg→cCNCs→HPMC→cCNCs→CGg. The structural analysis of (CGg/cCNCs/HPMC)5 L multilayered composite films indicated the existence of electrostatic interaction as well as H-bonding between polymeric layers that resulted in homogenous, dense and compact film surface with improved smoothness and strength properties. As compared to pure CGg film, the (CGg/cCNCs/HPMC)5 L multilayered composite films showed improved tensile strength (84.8 % increment) and modulus (29.19 % improvement). Importantly, the deposition of HPMC layer contributed in achieving multilayer composite films with more flexible behavior (46.55 % improvement in elongation at break). Furthermore, owing to the high transparency (89.5 % transmittance), appreciable gas and oil barrier performance and resistance to various solvents (e.g. acetone, THF and DMAc), these multilayer films are promising candidates for various applications including renewable/sustainable packaging materials.

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Appendix
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Metadata
Title
Layer-by-layer assembly of cationic guar gum, cellulose nanocrystals and hydroxypropyl methylcellulose based multilayered composite films
Authors
Arun Saini
Deepak Sharma
Yuanyuan Xia
Aman Saini
Xiangyu You
Ying Su
Lihong Chen
Chandravati Yadav
Xinping Li
Publication date
21-07-2021
Publisher
Springer Netherlands
Published in
Cellulose / Issue 13/2021
Print ISSN: 0969-0239
Electronic ISSN: 1572-882X
DOI
https://doi.org/10.1007/s10570-021-04064-6

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