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Physics of Metals and Metallography
Published in: Physics of Metals and Metallography 7/2021

01-07-2021 | STRUCTURE, PHASE TRANSFORMATIONS, AND DIFFUSION

Mechanochemical Synthesis of Cu–Al Alloyed Powders and Their Consolidation by Spark Plasma Sintering

Authors: T. F. Grigoreva, S. A. Petrova, S. A. Kovaleva, D. V. Dudina, I. S. Batraev, T. Yu. Kiseleva, S. I. Zholudev, S. V. Vosmerikov, E. T. Devyatkina, T. A. Udalova, S. N. Polyakov, N. Z. Lyakhov

Published in: Physics of Metals and Metallography | Issue 7/2021

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Abstract

The mechanochemically synthesized Cu–20 wt % Al alloys are studied by the X-ray diffraction analysis and scanning electron microscopy. It is shown that, after 20 min of mechanical activation, the single-phase intermetallic compound Cu9Al4 with crystallites ~3 nm in size, low microstrains (~0.03%), and particle size in the range from 0.2–0.4 to 2–4 μm is formed. The morphological characteristics of the solid solution of aluminum in copper, which has been mechanochemically synthesized from the Cu–10 wt % Al alloy, are studied. It is demonstrated that the solid solution is composed of platelike particles 10–50 μm in planar size and 2–10 μm in thickness. The scanning electron and optical microscopy data show that the Cu(Al) solid solution produced by the spark plasma sintering at 700°С are characterized by the low residual porosity (<0.5%). The Vickers hardness is 290 ± 30 HV.
previous article Model of Primary Recrystallization in Pure Copper
next article Effect of Surface Electropulsing Assisted Ultrasonic Impact Treatment on the Microstructure, Phase Composition, and Microhardness of 3D Printed Ti–6Al–4V Alloy

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Metadata
Title
Mechanochemical Synthesis of Cu–Al Alloyed Powders and Their Consolidation by Spark Plasma Sintering
Authors
T. F. Grigoreva
S. A. Petrova
S. A. Kovaleva
D. V. Dudina
I. S. Batraev
T. Yu. Kiseleva
S. I. Zholudev
S. V. Vosmerikov
E. T. Devyatkina
T. A. Udalova
S. N. Polyakov
N. Z. Lyakhov
Publication date
01-07-2021
Publisher
Pleiades Publishing
Published in
Physics of Metals and Metallography / Issue 7/2021
Print ISSN: 0031-918X
Electronic ISSN: 1555-6190
DOI
https://doi.org/10.1134/S0031918X21070024

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