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2018 | OriginalPaper | Chapter

Preparation of 3Y-TZP Nanoceramics by a Modified Two-Step Sintering with Ultrahigh Heating and Cooling Rates

Authors : Feng Chen, Zhiqiao Yan

Published in: Advanced Functional Materials

Publisher: Springer Singapore

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Abstract

3 mol% yttria stabilized tetragonal zirconia polycrystal (3Y-TZP) nanoceramics were prepared separately through traditional two-step sintering (TSS) and a modified TSS, namely rapid-treating TSS (RT-TSS) in which ultrahigh heating and cooling rates during the first step were adopted. The comparison studies showed that in RT-TSS, the first-step sintering temperature required for full densification could be obviously lowered and the grain growth be more effectively suppressed than that in TSS. A nearly fully densified (>98%TD) ceramics with an average grain size of 150 nm was obtained through RT-TSS. While, the ceramics prepared by TSS showed the larger grain size of 180 nm. The results also showed that the suppression of grain growth in RT-TSS didn’t so strongly rely on the ‘frozen’ structure. Supersaturated vacancies generated during the cooling process might play a more important role.

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Metadata
Title
Preparation of 3Y-TZP Nanoceramics by a Modified Two-Step Sintering with Ultrahigh Heating and Cooling Rates
Authors
Feng Chen
Zhiqiao Yan
Copyright Year
2018
Publisher
Springer Singapore
DOI
https://doi.org/10.1007/978-981-13-0110-0_72

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