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Journal of Sol-Gel Science and Technology

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01-09-2014 | Original Paper

Sol–gel synthesis of calcium hydroxyapatite thin films on quartz substrate using dip-coating and spin-coating techniques

Authors: Milda Malakauskaite-Petruleviciene, Zivile Stankeviciute, Aldona Beganskiene, Aivaras Kareiva

Published in: Journal of Sol-Gel Science and Technology | Issue 3/2014

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Abstract

Sol–gel synthesis route was suggested to prepare calcium hydroxyapatite (Ca₁₀(PO₄)₆(OH)₂, CHA) thin films on quartz substrates. CHA thin films were obtained using dip-coating and spin-coating techniques by coating the substrates 1, 5, 15 and 30 times. In the sol–gel process, the ethylenediaminetetraacetic acid and 1,2-ethandiol as complexing agents were used. Moreover, triethanolamine and polyvinyl alcohol were used as gel network forming materials. After each coating procedure the films were annealed at 1,000 °C. The results obtained from dip-coating and spin-coating techniques were compared in this study. It was demonstrated, that the formation of calcium hydroxyapatite depends on dipping (or spinning) time and annealing duration.

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Title: Sol–gel synthesis of calcium hydroxyapatite thin films on quartz substrate using dip-coating and spin-coating techniques
Authors: Milda Malakauskaite-Petruleviciene
Zivile Stankeviciute
Aldona Beganskiene
Aivaras Kareiva
Publication date: 01-09-2014
Publisher: Springer US
Published in: Journal of Sol-Gel Science and Technology / Issue 3/2014
Print ISSN: 0928-0707
Electronic ISSN: 1573-4846
DOI: https://doi.org/10.1007/s10971-014-3394-5

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