2008 | OriginalPaper | Chapter
Sonochemically Prepared Molybdenum Sulfide
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A sonochemical preparation of high surface area, sub-micron molybdenum sulfide is described.[
1
] A slurry of elemental sulfur and molybdenum hexacarbonyl in isodurene was irradiated with high-intensity ultrasound (20 kHz, ∼ 80 W/cm
2
) under Ar followed by heating under vacuum to remove residual solvent and any unreacted precursor.