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2017 | OriginalPaper | Chapter

Study of the Internal Structure of Isotropic Pyrolytic Graphite by Broadband Ultrasonic Spectroscopy

Authors : Anton S. Bychkov, Elena B. Cherepetskaya, Adam Konvalinka, Alexander A. Karabutov, Alexander Kravcov, V. A. Makarov, Elena A. Mironova, Nikolay A. Morozov

Published in: Durability of Critical Infrastructure, Monitoring and Testing

Publisher: Springer Singapore

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Abstract

As material for structural components, isotropic pyrolytic graphite (IPG) is widely used in such objects of critical infrastructure as nuclear fission reactors. There is the possibility of using IPG as a facing material for experimental thermonuclear facilities; this is currently being explored. Also, IPG is used as a sealing and anti-friction material in the aerospace industry. It is shown that X-ray tomography is not very suitable for studying the internal structure of IPG produced by chemical vapor deposition because its density is much the same as that of heterogeneities encountered in IPG, such as carbon black inclusions and anisotropic pyrographite crystallites. Broadband ultrasonic spectroscopy has been used to detect pores and carbon deposited layers in IPG samples, 2D images of the internal structure produced.

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Literature
1.
go back to reference Pierson, H.O.: Handbook of Carbon, Graphite, Diamond and Fullerenes. Noyes Publication, Park Ridge (1993) Pierson, H.O.: Handbook of Carbon, Graphite, Diamond and Fullerenes. Noyes Publication, Park Ridge (1993)
2.
go back to reference Choe, J., Lim, J.W., Kim, M., Kim, J., Lee, D.G.: Durability of graphite coated carbon composite bipolar plates for vanadium redox flow batteries. Compos. Struct. 134, 106–113 (2015)CrossRef Choe, J., Lim, J.W., Kim, M., Kim, J., Lee, D.G.: Durability of graphite coated carbon composite bipolar plates for vanadium redox flow batteries. Compos. Struct. 134, 106–113 (2015)CrossRef
3.
go back to reference Pageot, J., Rouzaud, J.N., Ahmad, M.A., Deldicque, D., Gadiou, R., Dentzer, J., et al.: Milled graphite as a pertinent analogue of French UNGG reactor graphite waste for a CO2 gasification-based treatment. Carbon 86, 174–187 (2015)CrossRef Pageot, J., Rouzaud, J.N., Ahmad, M.A., Deldicque, D., Gadiou, R., Dentzer, J., et al.: Milled graphite as a pertinent analogue of French UNGG reactor graphite waste for a CO2 gasification-based treatment. Carbon 86, 174–187 (2015)CrossRef
4.
go back to reference Leiro, J.A., Heinonen, M.H., Laiho, T., Batirev, I.G.: Core-level XPS spectra of fullerene, highly oriented pyrolitic graphite, and glassy carbon. J. Electr. Spectrosc. Relat. Phenom. 128, 205–213 (2003)CrossRef Leiro, J.A., Heinonen, M.H., Laiho, T., Batirev, I.G.: Core-level XPS spectra of fullerene, highly oriented pyrolitic graphite, and glassy carbon. J. Electr. Spectrosc. Relat. Phenom. 128, 205–213 (2003)CrossRef
5.
go back to reference Maslova, O.A., Ammar, M.-R., Guimbretiere, G., Rouzaud, J.-N., Simon, P.: Determination of crystallite size in polished graphitized carbon by Raman spectroscopy. Phys. Rev. B 86, 134205 (2012)CrossRef Maslova, O.A., Ammar, M.-R., Guimbretiere, G., Rouzaud, J.-N., Simon, P.: Determination of crystallite size in polished graphitized carbon by Raman spectroscopy. Phys. Rev. B 86, 134205 (2012)CrossRef
6.
go back to reference Salver-Disma, F., Tarascon, J.-M., Clinard, C., Rouzaud, J.-N.: Transmission electron microscopy studies on carbon materials prepared by mechanical milling. Carbon 37, 1941–1959 (1999)CrossRef Salver-Disma, F., Tarascon, J.-M., Clinard, C., Rouzaud, J.-N.: Transmission electron microscopy studies on carbon materials prepared by mechanical milling. Carbon 37, 1941–1959 (1999)CrossRef
7.
go back to reference Wirth, R.: Focused ion beam (FIB) combined with SEM and TEM: advanced analytical tools for studies of chemical composition, microstructure and crystal structure in geomaterials on a nanometer scale, Chem. Geol. 261 (2009) 217. Chem. Geol. 261, 217229 (2009)CrossRef Wirth, R.: Focused ion beam (FIB) combined with SEM and TEM: advanced analytical tools for studies of chemical composition, microstructure and crystal structure in geomaterials on a nanometer scale, Chem. Geol. 261 (2009) 217. Chem. Geol. 261, 217229 (2009)CrossRef
8.
go back to reference Le Guillou, M., Rouzaud, J.N., Deldicque, D., Toulhoat, N., Pipon, Y., Moncoffre, N.: Structural and nanostructural behavior of deuterium implanted Highly Ordered Pyrolytic Graphite investigated by combined High Resolution Transmission Electron Microscopy Scanning Electron Microscopy and Raman microspectrometry. Carbon 94, 277–284 (2015)CrossRef Le Guillou, M., Rouzaud, J.N., Deldicque, D., Toulhoat, N., Pipon, Y., Moncoffre, N.: Structural and nanostructural behavior of deuterium implanted Highly Ordered Pyrolytic Graphite investigated by combined High Resolution Transmission Electron Microscopy Scanning Electron Microscopy and Raman microspectrometry. Carbon 94, 277–284 (2015)CrossRef
Metadata
Title
Study of the Internal Structure of Isotropic Pyrolytic Graphite by Broadband Ultrasonic Spectroscopy
Authors
Anton S. Bychkov
Elena B. Cherepetskaya
Adam Konvalinka
Alexander A. Karabutov
Alexander Kravcov
V. A. Makarov
Elena A. Mironova
Nikolay A. Morozov
Copyright Year
2017
Publisher
Springer Singapore
DOI
https://doi.org/10.1007/978-981-10-3247-9_1

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