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01-09-2006 | Issue 17/2006

Journal of Materials Science 17/2006

Synthesis and characterization of molybdenum disulfide micro-sized solid spheres

Journal:
Journal of Materials Science > Issue 17/2006
Authors:
Danmei Wu, Xiaodong Zhou, Xun Fu, Huaqiang Shi, Debao Wang, Zhengshui Hu

Abstract

Mono-dispersed molybdenum disulfide solid spheres with the diameter of 0.5–2 μm have been successfully synthesized by a solvothermal method with a homemade quaternary ammonium salt of 2-undecyl-1-dithioureido-ethyl-imidazoline (SUDEI) as surfactant. The obtained solid spheres are characterized by transmission electron microscopy (TEM), scanning electron microscopy (SEM), X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS), respectively. The influences of reaction conditions are discussed while a mechanism is proposed to explain the formation of the peculiar morphology.

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