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Computational Investigation of Chatter for Face Mill Tool on VMC Using Different Shim Material with Experimental Validation Read chapter Read first chapter

2022 | OriginalPaper | Chapter

Synthesis and Morphological Study of Ethylene Diamine-Based Nickel Oxide Flower-Like Nanostructure

Authors : Deepika Tawar, Kamlesh Goyre, Diksha Choudhary, Kali Charan Sabat, Archana Singh

Published in: Advancement in Materials, Manufacturing and Energy Engineering, Vol. I

Publisher: Springer Singapore

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Abstract

Metal coordination complex has been used to synthesize nanostructures with defined morphologies. Nickel hydroxide complex is a coordination complex crystalline material whose structure depends on the adopted method of preparation. The previous investigations have confirmed different structures of Ni(OH)2. In the current study, we demonstrate a synthesis process for the development of β-Ni(OH)2 flower-like nanostructure using Ni(II) metal inorganic complexes by one-pot hydrothermal method. Using a mixture of –en (ethylene diamine) ligand and metal salt as a precursor to synthesize nickel hydroxide, many agglomerated structures were obtained. Using predefined [Ni(en)3]2+ complex, a very well-defined flower-like structure with no agglomeration was found. The prepared samples were characterized with X-ray powder diffraction, scanning electron microscopy, and dynamic light scattering techniques. It was found that the use of pre-synthesized metal inorganic complexes and the reaction temperature are the influencing factor for the development of the flowers.

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previous chapter Metal-Inorganic Nickel Complexes-Derived Nanostructured Nickel Oxide as an Efficient Water Oxidation Catalyst
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Metadata
Title
Synthesis and Morphological Study of Ethylene Diamine-Based Nickel Oxide Flower-Like Nanostructure
Authors
Deepika Tawar
Kamlesh Goyre
Diksha Choudhary
Kali Charan Sabat
Archana Singh
Copyright Year
2022
Publisher
Springer Singapore
Book
Advancement in Materials, Manufacturing and Energy Engineering, Vol. I

Print ISBN: 978-981-16-5370-4

Electronic ISBN: 978-981-16-5371-1

Copyright Year: 2022

DOI
https://doi.org/10.1007/978-981-16-5371-1_43

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