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2018 | OriginalPaper | Chapter

5. The Conjugate Thermolysis—Thermal Polymerization of Metal Chelate Monomers and Thermolysis of Polymers Formed In Situ

Authors : Igor E. Uflyand, Gulzhian I. Dzhardimalieva

Published in: Nanomaterials Preparation by Thermolysis of Metal Chelates

Publisher: Springer International Publishing

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Abstract

A common drawback of practically all methods for obtaining metal–polymer nanocomposite materials with “core–shell” structure is the multistage of process, on the one hand, and the formation of polydispersed systems with a wide distribution of particle size, on the other hand. Traditional approaches are rather laborious and include the stage of formation of macromolecular complexes, metal ions reduction reaction to form nano-sized particles, separation of the phase of chemically unbound components.

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previous chapter Thermolysis of Polymeric Metal Chelates
next chapter Thermolysis of Metal Chelates in Polymer Matrices
Footnotes
1
It is believed that E(CH2CHCOOH) (g) = 461.5 kJ mol−1.
 
2
Estimates of the thermal effects were carried out for a gas-phase reaction using the following data and assumptions: \( E\left( {{\text{CH}}_{ 2} {\text{CHCOOH }}\left( {\text{g}} \right)} \right)\, = \,E\left( {\text{MeCOOH}} \right) \, = \, 461.5{\text{ kJ mol}}^{ - 1}, \)\( \Delta H_{f}^{o} \left( {{\text{CH}}_{ 2} {\text{CHCOOH }}\left( {\text{l}} \right)} \right) \, = - 384.6{\text{ kJ mol}}^{ - 1} \), \( \Delta H_{\text{ev}} \left( {{\text{CH}}_{ 2} {\text{CHCOOH }}\left( {\text{l}} \right)} \right) \, = \, 545.6{\text{ kJ mol}}^{ - 1} \), \( \Delta H_{f}^{o} \left( {{\text{CH}}_{ 2} {\text{CHCOOH }}\left( {\text{g}} \right)} \right) \, = \, 96.2{\text{ kJ mol}}^{ - 1} \), \( \Delta H_{f}^{o} \left( {{\text{CH}}_{ 2} {\text{CH }}\left( {\text{g}} \right)} \right) \approx 271.7{\text{ kJ mol}}^{ - 1} \),\( \Delta H_{{f^{\prime}}}^{o} \left( {{\text{C}}_{ 2} {\text{H}}_{ 4} \left( {\text{g}} \right)} \right) \, = \, 52.3{\text{ kJ mol}}^{ - 1} ,\Delta H_{f}^{o} \left( {{\text{CO}}_{ 2} \left( {\text{g}} \right)} \right) \, = - 393{\text{ kJ mol}}^{ - 1} \).
 
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Metadata
Title
The Conjugate Thermolysis—Thermal Polymerization of Metal Chelate Monomers and Thermolysis of Polymers Formed In Situ
Authors
Igor E. Uflyand
Gulzhian I. Dzhardimalieva
Copyright Year
2018
Book
Nanomaterials Preparation by Thermolysis of Metal Chelates

Print ISBN: 978-3-319-93404-4

Electronic ISBN: 978-3-319-93405-1

Copyright Year: 2018

DOI
https://doi.org/10.1007/978-3-319-93405-1_5

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