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01-09-2006 | Issue 17/2006

Journal of Materials Science 17/2006

The relationships between microstructure and crystal structure in zincite solid solutions

Journal:
Journal of Materials Science > Issue 17/2006
Authors:
T. Yamashita, R. Hansson, P. C. Hayes

Abstract

Single phase (Zn,Fe)1−xO zincite solid solution samples have been prepared by high temperature equilibration in air and in reducing atmospheres, followed by quenching to room temperature. The Fe2+/Fe3+ concentrations in the samples have been determined using wet chemical and XPS techniques. Iron is found to be present in zincite predominantly in the form of Fe3+ ions. The transition from an equiaxed grain morphology to plate-like zincite crystals is shown to be associated with increasing Fe3+ concentration, increasing elongation in <001> of the hexagonal crystals and increasing anisotropic strain along the c-axis. The plate-like crystals are shown to contain planar defects and zincite polytypes at high iron concentrations.

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