Skip to main content
Top
Published in: Progress in Additive Manufacturing 4/2019

21-06-2019 | Full Research Article

The validation of the microstructural evolution of selective laser-melted AlSi10Mg on the in-house built machine: energy density studies

Authors: Ntombizodwa R. Mathe, Lerato C. Tshabalala

Published in: Progress in Additive Manufacturing | Issue 4/2019

Log in

Activate our intelligent search to find suitable subject content or patents.

search-config
loading …

Abstract

The additive manufacturing of aluminium alloys has become an area of interest for the aerospace industry due to the high strength-to-weight ratios of the produced components. AlSi10Mg has been explored as an alloy of choice for building aircraft parts such as heat exchangers with internal cooling channels, etc. In this study, metal powders of AlSi10Mg containing spherical particles with good flow ability for selective laser melting were used. Various process parameters were investigated on the in-house selective laser melting system or 3D printer to demonstrate the effect of high energy densities on the microstructure and hardness properties for increasing the consolidation rate. The single track analysis showed that the higher energy densities resulted in deeper penetration depth with wider track widths. The microstructures obtained from built cubes revealed built patterns representative of the laser scans after solidification of the molten powder. X-ray diffraction data analysis presented a substantial shift in the 2θ peak positions at the lowest energy density, indicating possible lattice expansion, known and non-indexed phases, and inherent strains in the material induced during the building process. The electron back-scattered diffraction results also showed a refined grain structures at lower energy densities with the presence of Al, Si, and Mg2Si, and no-indexed phases which could represent possible new phase orientations. The hardness measurements obtained in this study were higher than the conventional procedures due to grain refinement experienced during the fast heating and cooling gradients of this process.

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Appendix
Available only for authorised users
Literature
1.
go back to reference Srivatsan TS, Sudarshan TS (2015) Additive manufacturing: innovations, advances, and applications. CRC Press, Boca RatonCrossRef Srivatsan TS, Sudarshan TS (2015) Additive manufacturing: innovations, advances, and applications. CRC Press, Boca RatonCrossRef
2.
go back to reference Trevisan F et al (2019) Effects of heat treatment on A357 alloy produced by selective laser melting. In: World PM20162017: Hamburg, Germany Trevisan F et al (2019) Effects of heat treatment on A357 alloy produced by selective laser melting. In: World PM20162017: Hamburg, Germany
3.
go back to reference Brenne F et al (2016) Microstructural design of Ni-base alloys for high-temperature applications: impact of heat treatment on microstructure and mechanical properties after selective laser melting. Progress Additive Manuf 1(3):141–151CrossRef Brenne F et al (2016) Microstructural design of Ni-base alloys for high-temperature applications: impact of heat treatment on microstructure and mechanical properties after selective laser melting. Progress Additive Manuf 1(3):141–151CrossRef
4.
go back to reference Criales LE, Özel T (2017) Temperature profile and melt depth in laser powder bed fusion of Ti-6Al-4V titanium alloy. Progress Additive Manuf 2(3):169–177CrossRef Criales LE, Özel T (2017) Temperature profile and melt depth in laser powder bed fusion of Ti-6Al-4V titanium alloy. Progress Additive Manuf 2(3):169–177CrossRef
5.
go back to reference Dilip JJS et al (2017) Influence of processing parameters on the evolution of melt pool, porosity, and microstructures in Ti-6Al-4V alloy parts fabricated by selective laser melting. Progress Additive Manuf 2(3):157–167CrossRef Dilip JJS et al (2017) Influence of processing parameters on the evolution of melt pool, porosity, and microstructures in Ti-6Al-4V alloy parts fabricated by selective laser melting. Progress Additive Manuf 2(3):157–167CrossRef
6.
go back to reference Aboulkhair NT et al (2015) On the formation of AlSi10Mg single tracks and layers in selective laser melting: microstructure and nano-mechanical properties. J Mater Process Technol 230:88–98CrossRef Aboulkhair NT et al (2015) On the formation of AlSi10Mg single tracks and layers in selective laser melting: microstructure and nano-mechanical properties. J Mater Process Technol 230:88–98CrossRef
7.
go back to reference Attar H et al (2014) Selective laser melting of in situ titanium–titanium boride composites: processing, microstructure and mechanical properties. Acta Mater 76:13–22CrossRef Attar H et al (2014) Selective laser melting of in situ titanium–titanium boride composites: processing, microstructure and mechanical properties. Acta Mater 76:13–22CrossRef
8.
go back to reference Bartkowiak K et al (2011) New developments of laser processing aluminium alloys via additive manufacturing technique. Phys Proc 12:393–401CrossRef Bartkowiak K et al (2011) New developments of laser processing aluminium alloys via additive manufacturing technique. Phys Proc 12:393–401CrossRef
9.
go back to reference Kürnsteiner P et al (2017) Massive nanoprecipitation in an Fe-19Ni-xAl maraging steel triggered by the intrinsic heat treatment during laser metal deposition. Acta Mater 129:52–60CrossRef Kürnsteiner P et al (2017) Massive nanoprecipitation in an Fe-19Ni-xAl maraging steel triggered by the intrinsic heat treatment during laser metal deposition. Acta Mater 129:52–60CrossRef
10.
go back to reference Barriobero-Vila P et al (2018) Peritectic titanium alloys for 3D printing. Nat Commun 9(1):3426CrossRef Barriobero-Vila P et al (2018) Peritectic titanium alloys for 3D printing. Nat Commun 9(1):3426CrossRef
11.
go back to reference Brandl E et al (2012) Additive manufactured AlSi10Mg samples using selective laser melting (SLM): microstructure, high cycle fatigue, and fracture behavior. Mater Des 34:159–169CrossRef Brandl E et al (2012) Additive manufactured AlSi10Mg samples using selective laser melting (SLM): microstructure, high cycle fatigue, and fracture behavior. Mater Des 34:159–169CrossRef
12.
go back to reference Pei W et al (2017) The AlSi10Mg samples produced by selective laser melting: single track, densification, microstructure and mechanical behavior. Appl Surface Sci 408:38–50CrossRef Pei W et al (2017) The AlSi10Mg samples produced by selective laser melting: single track, densification, microstructure and mechanical behavior. Appl Surface Sci 408:38–50CrossRef
13.
go back to reference Louvis E, Fox P, Sutcliffe CJ (2011) Selective laser melting of aluminium components. J Mater Process Technol 211(2):275–284CrossRef Louvis E, Fox P, Sutcliffe CJ (2011) Selective laser melting of aluminium components. J Mater Process Technol 211(2):275–284CrossRef
14.
go back to reference Vicario I et al (2015) Development of HPDC Advanced Dies by Casting with Reinforced Tool Steels. Int J Manuf Eng 2015:10 Vicario I et al (2015) Development of HPDC Advanced Dies by Casting with Reinforced Tool Steels. Int J Manuf Eng 2015:10
15.
go back to reference Read N et al (2015) Selective laser melting of AlSi10Mg alloy: process optimisation and mechanical properties development. Mater Design 65:417–424CrossRef Read N et al (2015) Selective laser melting of AlSi10Mg alloy: process optimisation and mechanical properties development. Mater Design 65:417–424CrossRef
16.
go back to reference Prashanth KG et al (2017) Is the energy density a reliable parameter for materials synthesis by selective laser melting? Mater Res Lett 5(6):386–390CrossRef Prashanth KG et al (2017) Is the energy density a reliable parameter for materials synthesis by selective laser melting? Mater Res Lett 5(6):386–390CrossRef
17.
go back to reference Bourell D et al (2017) Evaluation of energy density measures and validation of powder bed fusion of polyamide. CIRp Ann Manuf Technol 66:217–220CrossRef Bourell D et al (2017) Evaluation of energy density measures and validation of powder bed fusion of polyamide. CIRp Ann Manuf Technol 66:217–220CrossRef
18.
go back to reference Gong H, et al (2014) Melt pool characterization for selective laser melting of Ti-6Al-4V pre-alloyed powder. In: 25th Annual international solid freeform fabrication symposium, Austin, Texas Gong H, et al (2014) Melt pool characterization for selective laser melting of Ti-6Al-4V pre-alloyed powder. In: 25th Annual international solid freeform fabrication symposium, Austin, Texas
19.
go back to reference Kempken K et al (2011) Process optimization and microstructural analysis for selective laser melting of AlSi10Mg. In: Solid free from fabrication symposium Kempken K et al (2011) Process optimization and microstructural analysis for selective laser melting of AlSi10Mg. In: Solid free from fabrication symposium
20.
go back to reference Olakanmi EO, Cochrane RF, Dalgarno KW (2015) A review on selective laser sintering/melting (SLS/SLM) of aluminium alloy powders: processing, microstructure, and properties. Prog Mater Sci 74:401–477CrossRef Olakanmi EO, Cochrane RF, Dalgarno KW (2015) A review on selective laser sintering/melting (SLS/SLM) of aluminium alloy powders: processing, microstructure, and properties. Prog Mater Sci 74:401–477CrossRef
21.
go back to reference Spierings AB et al (2016) Powder flowability characterisation methodology for powder-bed-based metal additive manufacturing. Progress Additive Manuf 1(1):9–20CrossRef Spierings AB et al (2016) Powder flowability characterisation methodology for powder-bed-based metal additive manufacturing. Progress Additive Manuf 1(1):9–20CrossRef
22.
go back to reference Markusson L (2017) Powder characterization for additive manufacturing process. Lulea University of Technology, Sweden Markusson L (2017) Powder characterization for additive manufacturing process. Lulea University of Technology, Sweden
23.
go back to reference Tshabalala LC, Mathe NR, Chikwanda H (2017) Characterization of gas atomized Ti-6Al-4V powders for additive manufacturing. In: 4th International conference on titanium powder metallurgy & additive manufacturing, Xi’an, China, Scientific.net Tshabalala LC, Mathe NR, Chikwanda H (2017) Characterization of gas atomized Ti-6Al-4V powders for additive manufacturing. In: 4th International conference on titanium powder metallurgy & additive manufacturing, Xi’an, China, Scientific.net
24.
go back to reference Li XP, O’Donnell KM, Sercombe T (2016) Selective laser melting of Al-12Si alloy: enhanced densification via powder drying. Additive Manuf 10:10–14CrossRef Li XP, O’Donnell KM, Sercombe T (2016) Selective laser melting of Al-12Si alloy: enhanced densification via powder drying. Additive Manuf 10:10–14CrossRef
25.
go back to reference Trevisan F et al (2016) Review on the selective laser melting (SLM) of the AlSi10Mg alloy: process, microstructure, and mechanical properties. Materials 10:76–99CrossRef Trevisan F et al (2016) Review on the selective laser melting (SLM) of the AlSi10Mg alloy: process, microstructure, and mechanical properties. Materials 10:76–99CrossRef
26.
go back to reference Alam MK et al (2018) Predictive modeling and the effect of process parameters on the hardness and bead characteristics for laser-cladded stainless steel. Int J Adv Manuf Technol 94(1):397–413CrossRef Alam MK et al (2018) Predictive modeling and the effect of process parameters on the hardness and bead characteristics for laser-cladded stainless steel. Int J Adv Manuf Technol 94(1):397–413CrossRef
27.
go back to reference Mostaf A et al (2017) Structure, texture and phases in 3D printed IN718 alloy subjected to homogenization and HIP treatments. Metals 7(6):196CrossRef Mostaf A et al (2017) Structure, texture and phases in 3D printed IN718 alloy subjected to homogenization and HIP treatments. Metals 7(6):196CrossRef
28.
go back to reference Thijs L et al (2013) Fine-structured aluminium products with controllable texture by selective laser melting of pre-alloyed AlSi10Mg powder. Acta Mater 61(5):1809–1819CrossRef Thijs L et al (2013) Fine-structured aluminium products with controllable texture by selective laser melting of pre-alloyed AlSi10Mg powder. Acta Mater 61(5):1809–1819CrossRef
29.
go back to reference Wei P et al (2017) The AlSi10Mg samples produced by selective laser melting: single track, densification, microstructure and mechanical behavior. Appl Surface Sci 408:38–50CrossRef Wei P et al (2017) The AlSi10Mg samples produced by selective laser melting: single track, densification, microstructure and mechanical behavior. Appl Surface Sci 408:38–50CrossRef
32.
go back to reference Aboulkhair NT et al (2014) Reducing porosity in AlSi10Mg parts processed by selective laser melting. Additive Manuf 1–4:77–86CrossRef Aboulkhair NT et al (2014) Reducing porosity in AlSi10Mg parts processed by selective laser melting. Additive Manuf 1–4:77–86CrossRef
33.
go back to reference Nahmany M et al (2015) Electron beam welding of AlSi10Mg workpieces produced by selected laser melting additive manufacturing technology. Additive Manuf 8:63–70CrossRef Nahmany M et al (2015) Electron beam welding of AlSi10Mg workpieces produced by selected laser melting additive manufacturing technology. Additive Manuf 8:63–70CrossRef
34.
go back to reference Takata N et al (2017) Change in microstructure of selectively laser melted AlSi10Mg alloy with heat treatments. Mater Sci Eng A 704:218–228CrossRef Takata N et al (2017) Change in microstructure of selectively laser melted AlSi10Mg alloy with heat treatments. Mater Sci Eng A 704:218–228CrossRef
35.
go back to reference Li W et al (2016) Effect of heat treatment on AlSi10Mg alloy fabricated by selective laser melting: microstructure evolution, mechanical properties and fracture mechanism. Mater Sci Eng A 663:116–125CrossRef Li W et al (2016) Effect of heat treatment on AlSi10Mg alloy fabricated by selective laser melting: microstructure evolution, mechanical properties and fracture mechanism. Mater Sci Eng A 663:116–125CrossRef
36.
go back to reference Yan C et al (2015) Microstructure and mechanical properties of aluminium alloy cellular lattice structures manufactured by direct metal laser sintering. Mater Sci Eng A 628:238–246CrossRef Yan C et al (2015) Microstructure and mechanical properties of aluminium alloy cellular lattice structures manufactured by direct metal laser sintering. Mater Sci Eng A 628:238–246CrossRef
37.
go back to reference Liu J (2015) Phase transformations and stress evolution during laser beam welding and post heat treatment of TiAl-alloys, in Helmholtz-Zentrum Geesthacht Report 2015. Technischen Universität Hamburg, Hamburg, p 104 Liu J (2015) Phase transformations and stress evolution during laser beam welding and post heat treatment of TiAl-alloys, in Helmholtz-Zentrum Geesthacht Report 2015. Technischen Universität Hamburg, Hamburg, p 104
38.
go back to reference Wu J et al (2016) Microstructure and strength of selectively laser melted AlSi10Mg. Acta Mater 117:311–320CrossRef Wu J et al (2016) Microstructure and strength of selectively laser melted AlSi10Mg. Acta Mater 117:311–320CrossRef
39.
go back to reference Chen B et al (2017) Strength and strain hardening of a selective laser melted AlSi10Mg alloy. Scripta Mater 141:45–49CrossRef Chen B et al (2017) Strength and strain hardening of a selective laser melted AlSi10Mg alloy. Scripta Mater 141:45–49CrossRef
40.
go back to reference Wang HQ, Sun WL, Xing YQ (2013) Microstructure analysis on 6061 aluminum alloy after casting and diffuses annealing process. Phys Proc 50:68–75CrossRef Wang HQ, Sun WL, Xing YQ (2013) Microstructure analysis on 6061 aluminum alloy after casting and diffuses annealing process. Phys Proc 50:68–75CrossRef
41.
go back to reference Shafieizad A et al (2015) The Mg2Si phase evolution during thermomechanical processing of in situ aluminum matrix macro-composite. Mater Sci Eng A 664:310–317CrossRef Shafieizad A et al (2015) The Mg2Si phase evolution during thermomechanical processing of in situ aluminum matrix macro-composite. Mater Sci Eng A 664:310–317CrossRef
42.
go back to reference Bahl S et al (2017) Elucidating microstructural evolution and strengthening mechanisms in nanocrystalline surface induced by surface mechanical attrition treatment of stainless steel. Acta Mater 122:138–151CrossRef Bahl S et al (2017) Elucidating microstructural evolution and strengthening mechanisms in nanocrystalline surface induced by surface mechanical attrition treatment of stainless steel. Acta Mater 122:138–151CrossRef
43.
go back to reference Tian Y et al (2016) Ductility sensitivity to stacking fault energy and grain size in Cu–Al alloys. Mater Res Lett 4(2):112–117CrossRef Tian Y et al (2016) Ductility sensitivity to stacking fault energy and grain size in Cu–Al alloys. Mater Res Lett 4(2):112–117CrossRef
44.
go back to reference Wright SI et al (2015) Introduction and comparison of new EBSD post-processing methodologies. Ultramicroscopy 159(1):81–94CrossRef Wright SI et al (2015) Introduction and comparison of new EBSD post-processing methodologies. Ultramicroscopy 159(1):81–94CrossRef
45.
go back to reference Rosenthal I, Stern A, Frage N (2014) Microstructure and mechanical properties of AlSi10Mg parts produced by the laser beam additive manufacturing (AM) technology. Metallogr Microstruct Anal 3(6):448–453CrossRef Rosenthal I, Stern A, Frage N (2014) Microstructure and mechanical properties of AlSi10Mg parts produced by the laser beam additive manufacturing (AM) technology. Metallogr Microstruct Anal 3(6):448–453CrossRef
46.
go back to reference Buchbinder D et al (2011) High power selective laser melting (HP SLM) of aluminum parts. Phys Proc 12:271–278CrossRef Buchbinder D et al (2011) High power selective laser melting (HP SLM) of aluminum parts. Phys Proc 12:271–278CrossRef
Metadata
Title
The validation of the microstructural evolution of selective laser-melted AlSi10Mg on the in-house built machine: energy density studies
Authors
Ntombizodwa R. Mathe
Lerato C. Tshabalala
Publication date
21-06-2019
Publisher
Springer International Publishing
Published in
Progress in Additive Manufacturing / Issue 4/2019
Print ISSN: 2363-9512
Electronic ISSN: 2363-9520
DOI
https://doi.org/10.1007/s40964-019-00086-6

Other articles of this Issue 4/2019

Progress in Additive Manufacturing 4/2019 Go to the issue

Premium Partners