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2019 | OriginalPaper | Chapter

Thermal and Mechanical Characteristics of Dual Cure Self-etching, Self-adhesive Resin Based Cement

Authors : Aleksandra Mitrovic, Nenad Mitrovic, Aleksandar Maslarevic, Vuk Adzic, Dejana Popovic, Milos Milosevic, Dusan Antonovic

Published in: Experimental and Numerical Investigations in Materials Science and Engineering

Publisher: Springer International Publishing

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Abstract

One of the main objectives in research and development of resin based cements (RBCs) is to enhance their clinical longevity and ease of use. In spite of the undeniable technological advances introduced in the last few decades, the polymerization shrinkage i.e. strain that accompanies the chain-growth polymerization of dimethacrylate monomers remains one of the major concerns for the clinical performance of composite restorations. Also, RBCs can produce a considerable amount of heat, due to the light energy from the curing lights and exothermic reaction of polymerization.

The purpose of this study was to determine the temperature changes during the photo-polymerization using thermocouples and to measure strain field of the self-etching, self-adhesive RBC, Maxcem Elite (Kerr, Orange, CA, USA) (ø5 × 1 mm - Group I and ø5 × 2 mm - Group II) using experimental technique, 3D Digital Image Correlation (DIC) method. Digital images were recorded immediately after photo-polymerization of the samples with a LED-curing unit for 20 s, according to manufacturer’s recommendation. Vickers microhardness was determined after photo-polymerization and after 24 h. Temperature curves for both groups indicated similar patterns but the peak temperature of Group II was significantly higher compared to peak temperature of Group I. DIC showed that peripheral zone of the samples had the highest strain values in both groups. Group I indicated significantly higher values of hardness. All the results were material-dependent and probably correlated to the composition of each material, which is not fully disclosed by the manufacturers.

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Kitzmüller, K., Graf, A., Watts, D., Schedle, A.: Setting kinetics and shrinkage of self-adhesive resin cements depend on cure-mode and temperature. Dent. Mater. 27, 544–551 (2011). https://doi.org/10.1016/j.dental.2011.02.004CrossRef

Vrochari, A.D., Eliades, G., Hellwig, E., Wrbas, K.T.: Curing efficiency of four self-etching, self-adhesive resin cements. Dent. Mater. 25, 1104–1108 (2009). https://doi.org/10.1016/j.dental.2009.02.015CrossRef

Van Ende, A., Van de Casteele, E., Depypere, M., De Munck, J., Li, X., Maesc, F., Wevers, M., Van Meerbeek, B.: 3D volumetric displacement and strain analysis of composite polymerization. Dent. Mater. 31, 453–461 (2015). https://doi.org/10.1016/j.dental.2015.01.018CrossRef

Zorzina, J., Maiera, E., Harrea, S., Feyb, T., Belli, R., Lohbauer, U., Petschelt, A., Taschner, A.: Bulk-fill resin composites: polymerization properties and extended light curing. Dent. Mater. 31, 293–301 (2015). https://doi.org/10.1016/j.dental.2014.12.010CrossRef

Li, J., Fok, A.S., Satterthwaite, J., Watts, D.C.: Measurement of the full-field polymerization shrinkage and depth of cure of dental composites using digital image correlation. Dent. Mater. 25, 582–588 (2009). https://doi.org/10.1016/j.dental.2008.11.001CrossRef

Miletic, V., Manojlovic, D., Milosevic, M., Mitrovic, N., Stankovic, T.S., Maneski, T.: Analysis of local shrinkage patterns of self-adhering and flowable composites using 3D digital image correlation. Quintessence Int. J. Pract. Dentist. Engl. Ed. 42, 797–804 (2011)

Fang Chen, T.Y., Sheng Huang, P., Fen, C.S.: Modeling dental composite shrinkage by digital image correlation and finite element methods. Opt. Lasers Eng. 61, 23–30 (2014). https://doi.org/10.1016/j.optlaseng.2014.04.006CrossRef

Cadenaro, M., Navarra, C.O., Antoniolli, F., Mazzoni, A., Di Lenarda, R., Rueggeberg, F.A., Breschi, L.: The effect of curing mode on extent of polymerization and microhardness of dual-cured, self-adhesive resin cements. Am. J. Dent. 23, 14–18 (2010)

Giráldez, I., Ceballos, L., Garrido, M.A., Rodríguez, J.: Early hardness of self-adhesive resin cements cured under indirect resin composite restorations. Jo. Esthet. Restor. Dent. 23, 116–124 (2011). https://doi.org/10.1111/j.1708-8240.2011.00408.xCrossRef

10.

Kim, R.J., Son, S.A., Hwang, J.Y., Lee, I.B., Seo, D.G.: Comparison of photopolymerization temperature increases in internal and external positions of composite and tooth cavities in real time: incremental fillings of microhybrid composite vs. bulk filling of bulk fill composite. J. Dent. 43, 1093–1098 (2015). https://doi.org/10.1016/j.jdent.2015.07.003CrossRef

11.

da Silva, E.M., Penelas, A.G., Simão, M.S., Filho, J.D., Posku, L.T., Guimarães, J.G.: Influence of the degree of dentine mineralization on pulp chamber temperature increase during resin-based composite (RBC) light-activation. J. Dent. 38, 336–342 (2010). https://doi.org/10.1016/j.jdent.2009.12.007CrossRef

12.

Michalakis, K., Pissiotis, A., Hirayama, H., Kang, K., Kafantaris, N.: Comparison of temperature increase in the pulp chamber during the polymerization of materials used for the direct fabrication of provisional restorations. J. Prosthet. Dent. 96, 418–423 (2006). https://doi.org/10.1016/j.prosdent.2006.10.005CrossRef

13.

Ramoglu, S.I., Karamehmetoglu, H., Sari, T., Usumez, S.: Temperature rise caused in the pulp chamber under simulated intrapulpal microcirculation with different light-curing modes. Angle Orthod. 85, 381–385 (2015). https://doi.org/10.2319/030814-164.1CrossRef

14.

Hannig, M., Bott, B.: In-vitro pulp chamber temperature rise during composite resin polymerization with various light-curing sources. Dent. Mater. 15, 275–281 (1999). https://doi.org/10.1016/S0109-5641(99)00047-0CrossRef

15.

McCabe, J.F.: Cure performance of light-activated composites by differential thermal analysis (DTA). Dent. Mater. 1, 231–234 (1985). https://doi.org/10.1016/S0109-5641(85)80048-8CrossRef

16.

Vaidyanathan, J., Vaidyanathan, T.K., Wang, Y., Viswanadhan, T.: Thermoanalytical characterization of visible light cure dental composites. J. Oral Rehabil. 19, 49–64 (1992). https://doi.org/10.1111/j.1365-2842.1992.tb01590.xCrossRef

17.

Vaidyanathan, J., Vaidyanathan, T.K.: Computer-controlled differential scanning calorimetry of dental composites. IEEE Trans. Biomed. Eng. 38, 319–325 (1991). https://doi.org/10.1109/10.133224CrossRef

18.

Al-Qudah, A.A., Mitchell, C.A., Biagioni, P.A., Hussey, D.L.: Thermographic investigation of contemporary resin-containing dental materials. J. Dent. 33, 593–602 (2005). https://doi.org/10.1016/j.jdent.2005.01.010CrossRef

19.

Al-Qudah, A.A., Mitchell, C.A., Biagioni, P.A., Hussey, D.L.: Effect of composite shade, increment thickness and curing light on temperature rise during photocuring. J. Dent. 35, 238–245 (2007). https://doi.org/10.1016/j.jdent.2006.07.012CrossRef

20.

Stewardson, D.A., Shortall, A.C., Harrington, E., Lumley, P.J.: Thermal changes and cure depths associated with a high intensity light activation unit. J. Dent. 32, 643–651 (2004). https://doi.org/10.1016/j.jdent.2004.06.007CrossRef

21.

Shortall, A., El-Mahy, W., Stewardson, D., Addison, O., Palin, W.: Initial fracture resistance and curing temperature rise of ten contemporary resin-based composites with increasing radiant exposure. J. Dent. 41, 455–463 (2013). https://doi.org/10.1016/j.jdent.2013.02.002CrossRef

22.

Hofmann, N., Hugo, B., Klaiber, B.: Effect of irradiation type (LED or QTH) on photo-activated composite shrinkage strain kinetics, temperature rise, and hardness. Eur. J. Oral Sci. 11, 471–479 (2002). https://doi.org/10.1034/j.1600-0722.2002.21359.xCrossRef

23.

Leprince, J., Devaux, J., Mullier, T., Vreven, J., Leloup, G.: Pulpal-temperature rise and polymerization efficiency of LED curing lights. Oper. Dent. 35, 220–230 (2010). https://doi.org/10.2341/09-203-lCrossRef

24.

Alnazzawi, A., Watts, D.C.: Simultaneous determination of polymerization shrinkage, exotherm and thermal expansion coefficient for dental resin-composites. Dent. Mater. 28, 1240–1249 (2012). https://doi.org/10.1016/j.dental.2012.09.004CrossRef

25.

Mamourian, M., Esfahani, A.J., Ayani, B.M.: Experimental and scale up study of the flame spread over the PMMA sheets. Therm. Sci. 13, 79–88 (2009). https://doi.org/10.2298/TSCI0901079MCrossRef

26.

Zhao, Z., Huang, H.M., Wang, Q., Ji, S.: Effects of pressure and temperature on thermal contact resistance between different materials. Therm. Sci. 19, 1369–1372 (2015). https://doi.org/10.2298/tsci1504369zCrossRef

27.

Asmussen, E., Peutzfeldt, A.: Temperature rise induced by some light emitting diode and quartz-tungsten-halogen curing units. Eur. J. Oral Sci. 113, 96–98 (2005). https://doi.org/10.1111/j.1600-0722.2004.00181.xCrossRef

28.

Hofmann, N., Markert, T., Hugo, B., Klaiber, B.: Effect of high intensity vs. soft-start halogen irradiation on light-cured resin-based composites. Part I. Temperature rise and polymerization shrinkage. Am. J. Dent. 16, 421–430 (2003)

29.

Daronch, M., Rueggeberg, F.A., Hall, G., De Goes, M.F.: Effect of composite temperature on in vitro intrapulpal temperature rise. Dent. Mater. 23, 1283–1288 (2007). https://doi.org/10.1016/j.dental.2006.11.024CrossRef

30.

Knežević, A., Tarle, Z., Meniga, A., Sutalo, J., Pichler, G.: Influence of light intensity from different curing units upon composite temperature rise. J. Oral Rehabil. 32, 362–367 (2005). https://doi.org/10.1111/j.1365-2842.2004.01418.xCrossRef

31.

Armellin, E., Bovesecchi, G., Coppa, P., Pasquantonio, G., Cerroni, L.: LED curing lights and temperature changes in different tooth sites. Biomed. Res. Int. 2016, 1–10 (2016). https://doi.org/10.1155/2016/1894672CrossRef

32.

Vallittu, P.K.: Peak temperatures of some prosthetic acrylates on polymerization. J. Oral Rehabil. 23, 776–781 (1996). https://doi.org/10.1046/j.1365-2842.1996.00430.xCrossRef

33.

Kim, S.H., Watts, D.C.: Exotherm behavior of the polymer-based provisional crown and fixed partial denture materials. Dent. Mater. 20, 383–387 (2004). https://doi.org/10.1016/j.dental.2003.11.001CrossRef

34.

Braga, R.R., Ballester, R.Y., Ferracane, J.L.: Factors involved in the development of polymerization shrinkage stress in resin-composites: a systematic review. Dent. Mater. 21, 962–970 (2005). https://doi.org/10.1016/j.dental.2005.04.018CrossRef

35.

Labella, R., Lambrechts, P., Van Meerbeek, B., Vanherle, G.: Polymerization shrinkage and elasticity of flowable composites and filled adhesives. Dent. Mater. 15, 128–137 (1999). https://doi.org/10.1016/S0109-5641(99)00022-6CrossRef

36.

Miletic, V., Peric, D., Milosevic, M., Manojlovic, D., Mitrovic, N.: Local deformation fields and marginal integrity of sculptable bulk-fill, low-shrinkage and conventional composites. Dent. Mater. 32, 1441–1451 (2016). https://doi.org/10.1016/j.dental.2016.09.011CrossRef

37.

Manojlovic, D., Dramićanin, M.D., Milosevic, M., Zeković, I., Cvijović-Alagić, I., Mitrovic, N., Miletic, V.: Effects of a low-shrinkage methacrylate monomer and monoacylphosphine oxide photoinitiator on curing efficiency and mechanical properties of experimental resin-based composites. Mater. Sci. Eng. C 58, 487–494 (2016). https://doi.org/10.1016/j.msec.2015.08.054CrossRef

38.

Milosevic, M., Miletic, V., Mitrovic, N., Manojlovic, D., Savic Stankovic, T., Maneski, T.: Measurement of local deformation fields in dental composites using 3D optical system. Chem. Listy 105, s751–s753 (2011)

39.

Mitrović, A., Tanasić, V.I., Mitrović, N., Milošević, M., Tihaček-Šojić, L., Antonović, D.: Strain determination of self-adhesive resin cement using 3D Digital Image Correlation method. Arh. Celok. Lek, Srp (2018). https://doi.org/10.2298/sarh170530176mCrossRef

40.

Kaisarly, D., Gezawi, M.E.: Polymerization shrinkage assessment of dental resin composites: a literature review. Odontology 104, 257–270 (2016). https://doi.org/10.1007/s10266-016-0264-3CrossRef

41.

Arrais, C.A., Rueggeberg, F.A., Waller, J.L., de Goes, M.F., Giannini, M.: Effect of curing mode on the polymerization characteristics of dual-cured resin cement systems. J. Dent. 36, 418–426 (2008). https://doi.org/10.1016/j.jdent.2008.02.014CrossRef

42.

Kleverlaan, C.J., Feilzer, A.J.: Polymerization shrinkage and contraction stress of dental resin composites. Dent. Mater. 21, 1150–1157 (2005). https://doi.org/10.1016/j.dental.2005.02.004CrossRef

43.

Spinell, T., Schedle, A., Watts, D.C.: Polymerization shrinkage kinetics of dimethacrylate resin-cements. Dent. Mater. 25, 1058–1066 (2009). https://doi.org/10.1016/j.dental.2009.04.008CrossRef

44.

Martinsen, M., El-Hajjar, R.F., Berzins, D.W.: 3D full field strain analysis of polymerization shrinkage in a dental composite. Dent. Mater. 29, e161–e167 (2013). https://doi.org/10.1016/j.dental.2013.04.019CrossRef

45.

Frassetto, A., Navarra, C.O., Marchesi, G., Turco, G., Di Lenarda, R., Breschi, L., Ferracane, J.L., Cadenaro, M.: Kinetics of polymerization and contraction stress development in self-adhesive resin cements. Dent. Mater. 28, 1032–1039 (2012). https://doi.org/10.1016/j.dental.2012.06.003CrossRef

46.

Truffier-Boutry, D., Demoustier-Champagne, S., Devaux, J., Biebuyck, J.J., Mestdagh, M., Larbanois, P., Leloup, G.: A physico-chemical explanation of the post-polymerization shrinkage in dental resins. Dent. Mater. 22, 405–412 (2006). https://doi.org/10.1016/j.dental.2005.04.030CrossRef

47.

Li, J., Li, H., Fok, A.S.L., Watts, D.C.: Multiple correlations of material parameters of light-cured dental composites. Dent. Mater. 25, 829–836 (2009). https://doi.org/10.1016/j.dental.2009.03.011CrossRef

48.

Meira, J.B.C., Braga, R.R., Ballester, R.Y., Tanaka, C.B., Versluis, A.: Understanding contradictory data in contraction stress tests. J. Dent. Res. 90, 365–370 (2011). https://doi.org/10.1177/0022034510388039CrossRef

Title: Thermal and Mechanical Characteristics of Dual Cure Self-etching, Self-adhesive Resin Based Cement
Authors: Aleksandra Mitrovic
Nenad Mitrovic
Aleksandar Maslarevic
Vuk Adzic
Dejana Popovic
Milos Milosevic
Dusan Antonovic
Publisher: Springer International Publishing
Book: Experimental and Numerical Investigations in Materials Science and Engineering
Print ISBN: 978-3-319-99619-6

Electronic ISBN: 978-3-319-99620-2

Copyright Year: 2019
DOI: https://doi.org/10.1007/978-3-319-99620-2_1

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