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Metallurgist
Published in: Metallurgist 7-8/2012

01-11-2012

Use of impedance spectroscopy for evaluating pipe steel susceptibility towards hydrogenation and hydrogen cracking

Authors: E. S. Ivanov, P. P. Stepanov, Yu. V. Ryabov, D. V. Kudashov, A. L. Klyuev

Published in: Metallurgist | Issue 7-8/2012

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Abstract

Impedance spectroscopy is used for different melts of steel 09GSF to show the difference in behavior of steel with and without hydrogenation. An equivalent circuit is proposed describing satisfactorily the impedance spectra obtained, and its parameters R p , R ct , R s , CPE_dl are determined. A correlation is found between steel susceptibility to hydrogen cracking (CLR) and impedance parameters R p and R ct . Values of R p and R ct increase linearly with an increase in CLR. The possibility is demonstrated of using impedance spectroscopy for evaluating steel susceptibility towards hydrogenation and hydrogen cracking.
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Literature
1.
NACE Standard TM 0177–2006, Standard Test Method. Laboratory Testing of Metals for Resistance to Sulfide Cracking under Stress and Corrosion Cracking under Stress in H 2 S-Containing Media.
2.
E. Barsoukov and J. R. MacDonald, Impedance Spectroscopy: Theory, Experiment, and Application, Wiley-Interscience (2005).
3.
Z. B. Stoinov, B. M. Grafov, B. Savova-Stoinova, and V. V. Elkin, Electrochemical Impedance [in Russian], Nauka, Moscow (1991).
4.
A. A. Klyuev, Z. A. Rotenberg, and V. V. Batrakov, “Impedance of passive iron electrode in the presence of reducing agent solution,” Elektrokhimiya, 41, 97–101 (2005).
5.
Chu-NanCao, “On the impedance plane displays for irreversible electrode reactions based on the stability conditions of the steady-state. I. One state variable besides electrode potential,” Electrochim. Acta, 35, 831 (1990). CrossRef
Metadata
Title
Use of impedance spectroscopy for evaluating pipe steel susceptibility towards hydrogenation and hydrogen cracking
Authors
E. S. Ivanov
P. P. Stepanov
Yu. V. Ryabov
D. V. Kudashov
A. L. Klyuev
Publication date
01-11-2012
Publisher
Springer US
Published in
Metallurgist / Issue 7-8/2012
Print ISSN: 0026-0894
Electronic ISSN: 1573-8892
DOI
https://doi.org/10.1007/s11015-012-9621-9

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