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Journal of Materials Engineering and Performance

Published in:

14-12-2018

ZrB₂-SiC-Ta₄HfC₅/Ta₄HfC₅ Oxidation-Resistant Dual-Layer Coating Fabricated by Spark Plasma Sintering for C/C Composites

Authors: Changling Zhou, Yushi Qi, Yehong Cheng, Wenbo Han

Published in: Journal of Materials Engineering and Performance | Issue 1/2019

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Abstract

In this work, a ZrB₂-SiC-Ta₄HfC₅/Ta₄HfC₅ oxidation-resistant dual-layer coating was fabricated to improve the oxidation resistance of carbon–carbon (C/C) composites. The coating was prepared by pack cementation combined with the slurry paste method. Spark plasma sintering was used in the procedure. The as-prepared dual-layer coating was approximately 110 μm, and no distinct interface was observed between the coating and the matrix. The isothermal oxidation test results showed that the dual coating effectively prevented C/C composites from oxidizing. The weight loss of the coated samples was only 3.3 and 9.5% after oxidation at 1773 K for 20 h and ten thermal shock cycles between 1773 K and room temperature in air, respectively. The pores and microcracks were the main reason for the failure of the coating.

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Title: ZrB2-SiC-Ta4HfC5/Ta4HfC5 Oxidation-Resistant Dual-Layer Coating Fabricated by Spark Plasma Sintering for C/C Composites
Authors: Changling Zhou
Yushi Qi
Yehong Cheng
Wenbo Han
Publication date: 14-12-2018
Publisher: Springer US
Published in: Journal of Materials Engineering and Performance / Issue 1/2019
Print ISSN: 1059-9495
Electronic ISSN: 1544-1024
DOI: https://doi.org/10.1007/s11665-018-3807-7

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