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Journal of Materials Science
Erschienen in: Journal of Materials Science 13/2021

27.01.2021 | Energy materials

Fast and facile synthesis of carbonate-modified NiFe layered double hydroxide nanosheets by dielectric barrier discharge microplasma: mechanism and application in enhanced water oxidation

verfasst von: Zhipeng Wang, Jiahui Zhang, Qiang Wang, Xue Jiang, Ke Huang, Xiaoli Xiong

Erschienen in: Journal of Materials Science | Ausgabe 13/2021

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Abstract

A fast and facile approach was designed to fabricate carbonate (Ci)-modified NiFe layered double hydroxide (LDH) nanosheets array on carbon cloth (CC) by dielectric barrier discharge (DBD) microplasma. The whole synthetic process can be completed within 1 h at ambient temperature and pressure. The prepared NiFe LDH-Ci/CC emerges a superior catalytic activity for oxygen evolving reaction in alkaline media, which only demands an overpotential of 240 mV at 20 mA cm−2 with a high stability for at least 90 h, and shows an excellent turnover frequency value of 0.323 mol O2 s−1 at 350 mV. Time-resolved measurements of direct emission spectra for nitrogen second positive system N2(C-B) were measured in the DBD microplasma discharge. And a high vibrational temperature (Tvib, 3100 K) and rotational temperature (Trot, 340 K) were obtained, indicating a great chemical reactivity. In addition, the intermediate products of hydroxyl radicals (·OH) were identified and the possible synthesis mechanism was tentatively proposed.

Graphical abstract

A fast and facile approach was designed to fabricate NiFe LDH-Ci/CC by DBD microplasma.
Vorheriger Artikel Fabrication of reduced graphene oxide/manganese oxide ink for 3D-printing technology on the application of high-performance supercapacitors
Nächster Artikel Porous spinel-type (Al0.2CoCrFeMnNi)0.58O4-δ high-entropy oxide as a novel high-performance anode material for lithium-ion batteries

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Metadaten
Titel
Fast and facile synthesis of carbonate-modified NiFe layered double hydroxide nanosheets by dielectric barrier discharge microplasma: mechanism and application in enhanced water oxidation
verfasst von
Zhipeng Wang
Jiahui Zhang
Qiang Wang
Xue Jiang
Ke Huang
Xiaoli Xiong
Publikationsdatum
27.01.2021
Verlag
Springer US
Erschienen in
Journal of Materials Science / Ausgabe 13/2021
Print ISSN: 0022-2461
Elektronische ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-021-05798-1

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