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22.04.2017 | Original Paper

Flexible and free-standing films containing cobalt-doped nanocrystalline zinc oxide dispersed in polyvinylidene fluoride matrix: synthesis and characterization

verfasst von: Rajkumar Dey, Ritamay Bhunia, Shamima Hussain, Bibhash Ranjan Chakraborty, Radhaballav Bhar, Arun Kumar Pal

Erschienen in: Polymer Bulletin | Ausgabe 1/2018

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Abstract

Synthesis of free-standing flexible Co-ZnO/PVDF composite films is realized by sol–gel technique. Modulation of the optical and microstructural properties of the above composite films with Co-doped nanocrystalline ZnO loading in PVDF matrix was studied critically. Uniform dispersion of Co-doped ZnO in PVDF matrix was indicated by SIMS studies. Information on the bonding environment was obtained from X-ray photoelectron spectroscopy and Raman spectroscopy studies. A very strong peak at ~695 eV for core level spectra of F1s along with those for C1s, Zn2p and Co2p dominated the XPS spectra of the composite films. Presence of the predominant β-phase of PVDF along with peaks related to ZnO nanocrystals in the poled sample was observed in the Raman spectra.

Vorheriger Artikel Nanocomposite of polyrotaxane derivative and graphene with increased dielectric constant

Nächster Artikel Investigation of mechanical and thermal properties of the cetyltrimethylammonium bromide functionalized molybdenum disulfide (MoS2)/epoxy composites

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Titel: Flexible and free-standing films containing cobalt-doped nanocrystalline zinc oxide dispersed in polyvinylidene fluoride matrix: synthesis and characterization
verfasst von: Rajkumar Dey
Ritamay Bhunia
Shamima Hussain
Bibhash Ranjan Chakraborty
Radhaballav Bhar
Arun Kumar Pal
Publikationsdatum: 22.04.2017
Verlag: Springer Berlin Heidelberg
Erschienen in: Polymer Bulletin / Ausgabe 1/2018
Print ISSN: 0170-0839
Elektronische ISSN: 1436-2449
DOI: https://doi.org/10.1007/s00289-017-2032-0

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