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Erschienen in: Rare Metals 4/2014

01.08.2014

Formation of M n+1AX n phases in Ti–Cr–Al–C systems by self-propagating high-temperature synthesis

verfasst von: Guo-Bing Ying, Xiao-Dong He, Shan-Yi Du, Chun-Cheng Zhu, Yong-Ting Zheng, Yu-Ping Wu, Cheng Wang

Erschienen in: Rare Metals | Ausgabe 4/2014

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Abstract

In this paper, phase composition of the M n+1AX n phases by self-propagating high-temperature synthesis (SHS) was determined using Ti, Cr, Al, and carbon black as raw materials. And, phase composition and microstructures of the M n+1AX n phases-contained bulk by SHS with the pseudo-hot isostatic pressing (SHS/PHIP) were investigated in Ti–Cr–Al–C systems raw materials. Rietveld XRD refinement was introduced to study the lattice parameters and phase composition of the resultant phases from the SHSed and SHS/PHIPed samples. Ti2AlC x , Ti3AlC2x , and Cr2AlC x by SHS were detected in the Ti–Cr–Al–C systems, as well as the binary carbide of TiC and intermetallics. The mechanical properties of the synthesized bulk samples were determined, exhibiting a high strength and toughness compared with the typical monolithic M n+1AX n phase ceramics. It is indicated that the samples prepared by SHS/PHIP are identified to be a strategy for improving the mechanical properties of monolithic M n+1AX n phase.

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Metadaten
Titel
Formation of M n+1AX n phases in Ti–Cr–Al–C systems by self-propagating high-temperature synthesis
verfasst von
Guo-Bing Ying
Xiao-Dong He
Shan-Yi Du
Chun-Cheng Zhu
Yong-Ting Zheng
Yu-Ping Wu
Cheng Wang
Publikationsdatum
01.08.2014
Verlag
Nonferrous Metals Society of China
Erschienen in
Rare Metals / Ausgabe 4/2014
Print ISSN: 1001-0521
Elektronische ISSN: 1867-7185
DOI
https://doi.org/10.1007/s12598-013-0196-9

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