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Journal of Materials Science: Materials in Electronics
Erschienen in: Journal of Materials Science: Materials in Electronics 19/2020

02.09.2020

Impact of phase segregation on optical and electrochemical property of BiPO4 nanostructures for energy storage applications

verfasst von: Prakash Chand, Aman Joshi, Vishal Singh

Erschienen in: Journal of Materials Science: Materials in Electronics | Ausgabe 19/2020

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Abstract

In the present paper, we report the influence of phase segregation (hexagonal and monoclinic phase) of facile microwave-assisted BPO (BiPO4) nanostructures on optical and electrochemical properties for supercapacitor applications. The XRD patterns reveal pure phase formation of both the samples of BiPO4 synthesized at 300 °C and 600 °C (JCPDS #15-0766 and JCPDS #43-0637). Phase transition of BiPO4 from hexagonal to monoclinic phase obtained by sintering the sample (BP600) at 600 °C. The FWHM values of the X-ray diffraction peaks observed to decrease with an increase in sintering temperature, which can be ascribed to the enhancement of the crystallite size. The synthesized samples of BiPO4 are in the nanometer dimension, which also revealed through FESEM examination. FTIR, Raman, and PL spectroscopy also revealed the crystal structure symmetry distinction among the hexagonal and monoclinic BiPO4 phase. Specific capacity calculated from GCD (galvanostatic charge and discharge) analysis for BP300 and BP600 samples is 1074 Cg−1 and 451 Cg−1, correspondingly, at the current density of 1 Ag−1. The investigation divulges that the phase segregation plays a considerable utility in tuning the electrochemical performance of BiPO4 nanostructures as active electrode material for next-generation electrochemical capacitors application.
Vorheriger Artikel SnO2 nanoparticles synthesized with Citrus aurantifolia and their performance in photocatalysis
Nächster Artikel Fabrication of rGO/α-Fe2O3 electrodes: characterization and use in photoelectrocatalysis

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Metadaten
Titel
Impact of phase segregation on optical and electrochemical property of BiPO4 nanostructures for energy storage applications
verfasst von
Prakash Chand
Aman Joshi
Vishal Singh
Publikationsdatum
02.09.2020
Verlag
Springer US
Erschienen in
Journal of Materials Science: Materials in Electronics / Ausgabe 19/2020
Print ISSN: 0957-4522
Elektronische ISSN: 1573-482X
DOI
https://doi.org/10.1007/s10854-020-04243-4

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