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Journal of Materials Science: Materials in Electronics
Erschienen in: Journal of Materials Science: Materials in Electronics 15/2019

12.07.2019

Influence of La/B ratio on the structure, sinterability and crystallization of La2O3–B2O3–CaO glass–ceramics

verfasst von: Weijun Zhang, Fenglin Wang, Xingyu Chen, Haijun Mao

Erschienen in: Journal of Materials Science: Materials in Electronics | Ausgabe 15/2019

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Abstract

To have a better understanding on the characteristics of La2O3–B2O3–CaO (LBC) glass–ceramics designed for low temperature co-fired ceramic applications, LBC glass–ceramics with La/B ratio changing from 1:6.0 to 1:3.0 were prepared, and the network structure, sinterability, crystalline phase composition and crystallization kinetics of synthesized LBC glass–ceramics were investigated. The increase of La/B ratio would reduce the content of [BO4] units in the network structure, and decrease the glass transition temperature as well as the softening temperature of LBC glass–ceramics. But low La/B ratio of glass could cause serious foaming during sintering process. The change of La/B ratio would influence the position as well as intensity of crystalline peaks on DSC curves, and the composition and microstructure of crystalline phases were also affected. The crystallization activation energies of LBC glass–ceramics were 157.9–498.7 kJ/mol, which raised up with the increase of La/B ratio.
Vorheriger Artikel Influence of Ni and Cu electrodeposits on the interfacial reaction between SAC305 solder and the Bi2(Te,Se)3 thermoelectric material
Nächster Artikel Influences of platinum doping concentrations and operation temperatures on oxygen sensitivity of Pt/SnO2/Pt resistive gas sensors

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Metadaten
Titel
Influence of La/B ratio on the structure, sinterability and crystallization of La2O3–B2O3–CaO glass–ceramics
verfasst von
Weijun Zhang
Fenglin Wang
Xingyu Chen
Haijun Mao
Publikationsdatum
12.07.2019
Verlag
Springer US
Erschienen in
Journal of Materials Science: Materials in Electronics / Ausgabe 15/2019
Print ISSN: 0957-4522
Elektronische ISSN: 1573-482X
DOI
https://doi.org/10.1007/s10854-019-01853-5

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