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2013 | OriginalPaper | Buchkapitel

9. Infrared Spectroscopy

verfasst von : Maria Zaharescu, Oana Cătălina Mocioiu

Erschienen in: Chemical Solution Deposition of Functional Oxide Thin Films

Verlag: Springer Vienna

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Abstract

One of the first and most frequently-used methods for the investigation of thin films obtained by chemical solution deposition is IR spectroscopy. Infrared spectroscopy (or vibration absorption spectroscopy) provides information about the covalent bonds in the chemical groups of the investigated materials. IR spectroscopy allows both the solutions used for film deposition and the films obtained to be investigated by using different deposition methods. The following characteristics are among the most important results obtained: composition of the initial reagents, molecular structure of the solutions obtained by mixing different reagents, reactions in the solutions during storage, influence of the type of solution (alcoholic or aqueous) on the characteristics of the deposited films, and crystallization by thermal treatment of the structure of as-deposited films which are usually amorphous.

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Literatur
1.
Zurück zum Zitat Harwood LM, Moody CJ (1989) Experimental organic chemistry: principles and practice. Wiley-Blackwell, Oxford, 292 p Harwood LM, Moody CJ (1989) Experimental organic chemistry: principles and practice. Wiley-Blackwell, Oxford, 292 p
2.
Zurück zum Zitat Pogany I, Banciu M (1972) Metode fizice in chimia organica. Stiintifica, Bucuresti, 106 p Pogany I, Banciu M (1972) Metode fizice in chimia organica. Stiintifica, Bucuresti, 106 p
3.
Zurück zum Zitat Lau WS (2001) Infrared characterization for microelectronics. World Scientific, Singapore Lau WS (2001) Infrared characterization for microelectronics. World Scientific, Singapore
4.
Zurück zum Zitat Balaban AT, Banciu M, Pogany I (1983) Aplicatii ale metodelor fizice in chimia organica. Stiintifica si Enciclopedica, Bucuresti, pp 13–38 (in romanian) Balaban AT, Banciu M, Pogany I (1983) Aplicatii ale metodelor fizice in chimia organica. Stiintifica si Enciclopedica, Bucuresti, pp 13–38 (in romanian)
5.
Zurück zum Zitat Nakamoto K (2009) Infrared and Raman spectra of inorganic and coordination compounds, part A, theory and application in inorganic chemistry. Wiley Nakamoto K (2009) Infrared and Raman spectra of inorganic and coordination compounds, part A, theory and application in inorganic chemistry. Wiley
6.
Zurück zum Zitat Coates J (2000) Interpretation of infrared spectra, a practical approach. In: Meyers RA (ed) Encyclopedia of analytical chemistry, vol 12. Wiley, Chichester, p 10817 Coates J (2000) Interpretation of infrared spectra, a practical approach. In: Meyers RA (ed) Encyclopedia of analytical chemistry, vol 12. Wiley, Chichester, p 10817
7.
Zurück zum Zitat Pouxviel JC, Boilot JP, Beloeil JC, Lallemand JY (1987) NMR study of the sol/gel poly-merization. J Non-Cryst Solids 89:345CrossRef Pouxviel JC, Boilot JP, Beloeil JC, Lallemand JY (1987) NMR study of the sol/gel poly-merization. J Non-Cryst Solids 89:345CrossRef
8.
Zurück zum Zitat Harris MT, Byers CH (1988) Effect of solvent on the homogeneous precipitation of titania by titanium ethoxide hydrolysis. J Non-Cryst Solids 103:49CrossRef Harris MT, Byers CH (1988) Effect of solvent on the homogeneous precipitation of titania by titanium ethoxide hydrolysis. J Non-Cryst Solids 103:49CrossRef
9.
Zurück zum Zitat Kundu D, Ganguli D (1986) Monolithic zirconia gels from metal-organic solutions. J Mater Sci Lett 5:293CrossRef Kundu D, Ganguli D (1986) Monolithic zirconia gels from metal-organic solutions. J Mater Sci Lett 5:293CrossRef
10.
Zurück zum Zitat Barringer EA, Bowen HK (1985) High-purity, monodisperse TiO2 powders by hydrolysis of titanium tetraethoxide. 1. Synthesis and physical properties. Langmuir 1:414CrossRef Barringer EA, Bowen HK (1985) High-purity, monodisperse TiO2 powders by hydrolysis of titanium tetraethoxide. 1. Synthesis and physical properties. Langmuir 1:414CrossRef
11.
Zurück zum Zitat Harris MT, Byers CH, Brunson RR (1988) A study of solvent effects on the synthesis of pure component and composite ceramic powders by metal alkoxide hydrolysis. Mater Res Soc Symp Proc 121:287CrossRef Harris MT, Byers CH, Brunson RR (1988) A study of solvent effects on the synthesis of pure component and composite ceramic powders by metal alkoxide hydrolysis. Mater Res Soc Symp Proc 121:287CrossRef
12.
Zurück zum Zitat Nabavi M, Doeuff S, Sanchez C, Livage J (1990) Chemical modification of metal alkoxides by solvents: a way to control sol–gel chemistry. J Non-Cryst Solids 121:31CrossRef Nabavi M, Doeuff S, Sanchez C, Livage J (1990) Chemical modification of metal alkoxides by solvents: a way to control sol–gel chemistry. J Non-Cryst Solids 121:31CrossRef
13.
Zurück zum Zitat Doeuff S, Henry M, Sanchez C, Livage J (1987) Hydrolysis of titanium alkoxides: modification of the molecular precursor by acetic acid. J Non-Cryst Solids 89:206CrossRef Doeuff S, Henry M, Sanchez C, Livage J (1987) Hydrolysis of titanium alkoxides: modification of the molecular precursor by acetic acid. J Non-Cryst Solids 89:206CrossRef
14.
Zurück zum Zitat Urlaub R, Posset U, Thull R (2000) FT-IR spectroscopic investigations on sol–gel-derived coatings from acid-modified titanium alkoxides. J Non-Cryst Solids 265:276CrossRef Urlaub R, Posset U, Thull R (2000) FT-IR spectroscopic investigations on sol–gel-derived coatings from acid-modified titanium alkoxides. J Non-Cryst Solids 265:276CrossRef
15.
Zurück zum Zitat Kim CY, Sekino T, Yamamoto Y, Niihara K (2005) The synthesis of lead-free ferroelectric Bi1/2Na1/2TiO3 thin film by solution-sol–gel method. J Sol–Gel Sci Technol 33:307CrossRef Kim CY, Sekino T, Yamamoto Y, Niihara K (2005) The synthesis of lead-free ferroelectric Bi1/2Na1/2TiO3 thin film by solution-sol–gel method. J Sol–Gel Sci Technol 33:307CrossRef
16.
Zurück zum Zitat Barbe CJ, Harmer MA, Scherer GW (1997) Sol–gel synthesis of potassium titanyl phosphate: solution chemistry and gelation. J Sol–Gel Sci Technol 9:183 Barbe CJ, Harmer MA, Scherer GW (1997) Sol–gel synthesis of potassium titanyl phosphate: solution chemistry and gelation. J Sol–Gel Sci Technol 9:183
17.
Zurück zum Zitat Predoana L, Jitianu A, Malic B, Zaharescu M (2012) Study of the gelling process in the La-Co-citric acid system. J Am Ceram Soc 95:1068 Predoana L, Jitianu A, Malic B, Zaharescu M (2012) Study of the gelling process in the La-Co-citric acid system. J Am Ceram Soc 95:1068
18.
Zurück zum Zitat Guan XH, Liu Q, Chen GH, Shang C (2005) Surface complexation of condensed phosphate to aluminum hydroxide: an ATR-FTIR spectroscopic investigation. J Colloid Interf Sci 289:319CrossRef Guan XH, Liu Q, Chen GH, Shang C (2005) Surface complexation of condensed phosphate to aluminum hydroxide: an ATR-FTIR spectroscopic investigation. J Colloid Interf Sci 289:319CrossRef
19.
Zurück zum Zitat Abbas MH, Davidson G (1994) Vibrational spectra of X2O7 n− anions. Spectrochim Acta Part A 50:1153CrossRef Abbas MH, Davidson G (1994) Vibrational spectra of X2O7 n− anions. Spectrochim Acta Part A 50:1153CrossRef
20.
Zurück zum Zitat Ivashkevich LS, Lyutsko VA, Nikanovich MV (1988) Calculation of the vibrational spectrum of the triphosphate anion. J Appl Spectrosc 2:180CrossRef Ivashkevich LS, Lyutsko VA, Nikanovich MV (1988) Calculation of the vibrational spectrum of the triphosphate anion. J Appl Spectrosc 2:180CrossRef
21.
Zurück zum Zitat Rulmont A, Winand JM, Tarte P (1991) Nouvelles solutions solides LI(MIV)2 -x(NIV)x(PO4)3 (L = Li, Na M, N = Ge, Sn, Ti, Zr, Hf) synthèse et étude par diffraction x et conductivité ionique. J Solid State Chem 93:341CrossRef Rulmont A, Winand JM, Tarte P (1991) Nouvelles solutions solides LI(MIV)2 -x(NIV)x(PO4)3 (L = Li, Na M, N = Ge, Sn, Ti, Zr, Hf) synthèse et étude par diffraction x et conductivité ionique. J Solid State Chem 93:341CrossRef
22.
Zurück zum Zitat Scorates G (2001) Infrared and Raman characteristic group frequencies: tables and charts. Wiley, New York Scorates G (2001) Infrared and Raman characteristic group frequencies: tables and charts. Wiley, New York
23.
Zurück zum Zitat Gong W (2001) A real time in situ ATR-FTIR spectroscopic study of linear phosphate adsorption on titania surfaces. Int J Miner Process 63:147CrossRef Gong W (2001) A real time in situ ATR-FTIR spectroscopic study of linear phosphate adsorption on titania surfaces. Int J Miner Process 63:147CrossRef
24.
Zurück zum Zitat Michelmore A, Gong W, Jenkins P, Ralston JJ (2000) The interaction of linear polyphosphates with titanium dioxide surfaces. Phys Chem Chem Phys 2:2985CrossRef Michelmore A, Gong W, Jenkins P, Ralston JJ (2000) The interaction of linear polyphosphates with titanium dioxide surfaces. Phys Chem Chem Phys 2:2985CrossRef
25.
Zurück zum Zitat Zarzycki J (1991) Glasses and the vitreous state. Cambridge University Press, Cambridge, p 114 Zarzycki J (1991) Glasses and the vitreous state. Cambridge University Press, Cambridge, p 114
26.
Zurück zum Zitat Lashgari K, Westin GK (1999) Preparation of PZT film and powder by sol–gel technique using Ti- and Zr-alkoxides and a novel Pb-precursor; Pb(NO3)2 1.5EO3. J Sol–Gel Sci Technol 13(1–3):865 Lashgari K, Westin GK (1999) Preparation of PZT film and powder by sol–gel technique using Ti- and Zr-alkoxides and a novel Pb-precursor; Pb(NO3)2 1.5EO3. J Sol–Gel Sci Technol 13(1–3):865
27.
Zurück zum Zitat Ion ED, Malič B, Arčon I, Padežnik Gomilšek J, Kodre A, Kosec M (2010) Characterization of lanthanum zirconate prepared by a nitrate-modified alkoxide synthesis route: from sol to crystalline powder. J Eur Ceram Soc 30:569CrossRef Ion ED, Malič B, Arčon I, Padežnik Gomilšek J, Kodre A, Kosec M (2010) Characterization of lanthanum zirconate prepared by a nitrate-modified alkoxide synthesis route: from sol to crystalline powder. J Eur Ceram Soc 30:569CrossRef
28.
Zurück zum Zitat Hardy A, Van Elshocht S, Adelmann C, Kittl JA, De Gendt S, Heyns M, D’Haen J, D’Olieslaeger M, Van Bael MK, Van den Rul H, Mullens J (2010) Strontium niobate high-k dielectrics: film deposition and material properties. Acta Mater 58:216CrossRef Hardy A, Van Elshocht S, Adelmann C, Kittl JA, De Gendt S, Heyns M, D’Haen J, D’Olieslaeger M, Van Bael MK, Van den Rul H, Mullens J (2010) Strontium niobate high-k dielectrics: film deposition and material properties. Acta Mater 58:216CrossRef
29.
Zurück zum Zitat Aronne A, Sigaev VN, Champagnon B, Fanelli E, Califano V, Usmanova LZ (2005) The origin of nanostructuring in potassium niobiosilicate glasses by Raman and FTIR spectroscopy. J Non-Cryst Solids 351:3610CrossRef Aronne A, Sigaev VN, Champagnon B, Fanelli E, Califano V, Usmanova LZ (2005) The origin of nanostructuring in potassium niobiosilicate glasses by Raman and FTIR spectroscopy. J Non-Cryst Solids 351:3610CrossRef
30.
Zurück zum Zitat Ziolek M, Nowak I (2003) Characterization techniques employed in the study of niobium and tantalum-containing materials. Catal Today 78:543CrossRef Ziolek M, Nowak I (2003) Characterization techniques employed in the study of niobium and tantalum-containing materials. Catal Today 78:543CrossRef
31.
Zurück zum Zitat Ko YS, Jang HT, Ahn WS (2007) Hydrothermal synthesis and characterization of niobium-containing silicalite-1 molecular sieves with MFI structure. J Ind Eng Chem 13:764 Ko YS, Jang HT, Ahn WS (2007) Hydrothermal synthesis and characterization of niobium-containing silicalite-1 molecular sieves with MFI structure. J Ind Eng Chem 13:764
32.
Zurück zum Zitat Nyquist RA, Putzig CL, Leugers MA (1997) Handbook of infrared and Raman spectra of inorganic compounds and organic salts. Academic, San Diego, CA Nyquist RA, Putzig CL, Leugers MA (1997) Handbook of infrared and Raman spectra of inorganic compounds and organic salts. Academic, San Diego, CA
33.
Zurück zum Zitat Prasetyoko D, Ramli Z, Endud S, Nur H (2005) Preparation and characterization of bifunctional oxidative and acidic catalysts Nb2O5/TS-1 for synthesis of diols. Mater Chem Phys 93:443CrossRef Prasetyoko D, Ramli Z, Endud S, Nur H (2005) Preparation and characterization of bifunctional oxidative and acidic catalysts Nb2O5/TS-1 for synthesis of diols. Mater Chem Phys 93:443CrossRef
34.
Zurück zum Zitat Tellier J, Kuščer D, Malič B, Cilenšek J, Škarabot M, Kovač J, Gonçalves G, Muševič I, Kosec M (2010) Transparent, amorphous and organics-free ZnO thin films produced by chemical solution deposition at 150 °C. Thin Solid Films 518:5134CrossRef Tellier J, Kuščer D, Malič B, Cilenšek J, Škarabot M, Kovač J, Gonçalves G, Muševič I, Kosec M (2010) Transparent, amorphous and organics-free ZnO thin films produced by chemical solution deposition at 150 °C. Thin Solid Films 518:5134CrossRef
35.
Zurück zum Zitat Tolstoy VP, Chernychova IV, Skryshevsky VA (2003) Handbook of infrared spectroscopy of ultrathin films. John Wiley, New YorkCrossRef Tolstoy VP, Chernychova IV, Skryshevsky VA (2003) Handbook of infrared spectroscopy of ultrathin films. John Wiley, New YorkCrossRef
36.
Zurück zum Zitat Jitaru I, Berger D, Fruth V, Novac A, Stanica N, Rusu F (2000) Lanthanum chromites doped with divalent transition metals. Ceram Int 26:193CrossRef Jitaru I, Berger D, Fruth V, Novac A, Stanica N, Rusu F (2000) Lanthanum chromites doped with divalent transition metals. Ceram Int 26:193CrossRef
37.
Zurück zum Zitat Stanulis A, Hardy A, Dobbelaere C, D’Haen J, Van Bael M, Kareiva A (2012) SnO2 thin films from an aqueous citrato peroxo Sn(IV) precursor. J Sol–Gel Sci Technol 62:57CrossRef Stanulis A, Hardy A, Dobbelaere C, D’Haen J, Van Bael M, Kareiva A (2012) SnO2 thin films from an aqueous citrato peroxo Sn(IV) precursor. J Sol–Gel Sci Technol 62:57CrossRef
Metadaten
Titel
Infrared Spectroscopy
verfasst von
Maria Zaharescu
Oana Cătălina Mocioiu
Copyright-Jahr
2013
Verlag
Springer Vienna
DOI
https://doi.org/10.1007/978-3-211-99311-8_9

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