Abstract
The engineering properties of loess are significantly influenced by seasonal wet and dry climates, the effects of which are essentially inseparable from variations of its structure. To realize the multiscale evaluation of the influence of wet/dry (WD) cycles on the intact loess structure, several WD cycles were applied to intact loess samples. The samples were then subjected to X-ray computed tomography, scanning electron microscopy, and nuclear magnetic resonance tests, paired with state-of-the-art image processing techniques to assess the evolution of the mesoscopic and microscopic structure (i.e., fissures, particles, and pores). The results indicate that the loess fissuring is gradual; that is, it commences in the first two cycles, propagates in three to five cycles, and reaches an equilibrium in six to ten cycles. In the equilibrium stage, the average width of the fissures is inhibited owing to the emergence of secondary fissures. The primary cause for the fissuring is uneven shrinkage (generating tensile stresses) inside and on the surface of the soil. Further, as the WD cycles progress, the orientation of the particles near the polar angle exhibits depolarization, the non-uniformity of the particles and pores increases, the particle roundness improves, and the pore curvature decreases. Moreover, the changes in pore structure include mesopore and macropore expansion, along with the generation of new micropores. These findings serve as a basis for understanding the structural variations in loess exposed to WD cycles, which can help explain changes in the engineering properties of loess in semiarid regions.
Similar content being viewed by others
References
Alonso EE, Romero E, Hoffmann C, García-Escudero E (2005) Expansive bentonite–sand mixtures in cyclic controlled-suction drying and wetting. Eng Geol 81:213–226. https://doi.org/10.1016/j.enggeo.2005.06.009
Anovitz LM, Cole DR (2015) Characterization and analysis of porosity and pore structures. Rev Miner Geochem 80:61–164. https://doi.org/10.2138/rmg.2015.80.04
ASTM (2007) Standard test method for particle-size analysis of soils. ASTM D422–63:West Conshohocken, PA
ASTM (2009) Standard test methods for laboratory determination of density (unit weight) of soil specimens. ASTM D7263–21:West Conshohocken, PA
ASTM (2010a) Standard test methods for laboratory determination of water (moisture) content of soil and rock by mass. ASTM D2216–19:West Conshohocken, PA
ASTM (2010b) Standard test methods for liquid limit, plastic limit, and plasticity index of soils. ASTM D4318–10:West Conshohocken, PA
ASTM (2010c) Standard test methods for specific gravity of soil solids by water pycnometer. ASTM D854–10:West Conshohocken, PA
ASTM (2011) Standard practice for classification of soils for engineering purposes (USCS). ASTM D2487–11:West Conshohocken, PA
ASTM (2014) Standard practices for preserving and transporting soil samples. ASTM D4220M-14:West Conshohocken, PA
Auvray R, Rosin-Paumier S, Abdallah A, Masrouri F (2014) Quantification of soft soil cracking during suction cycles by image processing. Eur J Environ Civ Eng 18:11–32. https://doi.org/10.1080/19648189.2013.840250
Caniego FJ, Martı́ MA, San José F (2003) Rényi dimensions of soil pore size distribution. Geoderma 112:205–216. https://doi.org/10.1016/S0016-7061(02)00307-5
Cetin H, Söylemez M (2004) Soil-particle and pore orientations during drained and undrained shear of a cohesive sandy silt clay soil. Can Geotech J 41:1127–1138. https://doi.org/10.1139/t04-055
Chen A, Airey GD, Thom N, Li Y (2022) Characterisation of fatigue damage in asphalt mixtures using X-ray computed tomography. Road Mater Pavement. https://doi.org/10.1080/14680629.2022.2029756
Dong J, Lyu H, Xu G, He C (2020) NMR-based study on soil pore structures affected by drying–wetting cycles. Arab J Sci Eng 45:4161–4169. https://doi.org/10.1007/s13369-020-04409-6
Duan X, Dong Q, Ye W, Zhou J, Oh E (2019a) Study on adverse effects of groundwater level rising induced by land creation engineering in hilly and gully area of the Loess Plateau. J Mt Sci-Engl 16:2739–2753. https://doi.org/10.1007/s11629-019-5549-x
Duan Z, Cheng W, Peng J, Wang Q, Chen W (2019b) Investigation into the triggering mechanism of loess landslides in the south Jingyang platform, Shaanxi province. B Eng Geol Environ 78:4919–4930. https://doi.org/10.1007/s10064-018-01432-8
Elsayed M, El-Husseiny A, Hussaini SR, Mahmoud M (2023) Experimental and simulation study on the estimation of surface relaxivity of clay minerals. Geoenergy Sci Eng. https://doi.org/10.1016/j.geoen.2023.212260
Estabragh AR, Moghadas M, Javadi AA (2015) Mechanical behaviour of an expansive clay mixture during cycles of wetting and drying inundated with different quality of water. Eur J Environ Civ Eng 19:278–289. https://doi.org/10.1080/19648189.2014.960098
Fu J, Thomas HR, Li C (2021) Tortuosity of porous media: image analysis and physical simulation. Earth-Sci Rev 212:103439. https://doi.org/10.1016/j.earscirev.2020.103439
Garbout A, Sturrock CJ, Armenise E, Ahn S, Simmons RW, Doerr S, Ritz K, Mooney SJ (2018) TopCap: a tool to quantify soil surface topology and subsurface structure. Vadose Zone J 17:170091. https://doi.org/10.2136/vzj2017.05.0091
Graham RC (1999) X-ray diffraction and the identification and analysis of clay minerals. Soil Sci 164:72–73. https://doi.org/10.1097/00010694-199901000-00011
Hattab M, Fleureau J-M (2011) Experimental analysis of kaolinite particle orientation during triaxial path. Int J Numer Anal Met 35:947–968. https://doi.org/10.1002/nag.936
He M, Ding M, Yuan Z, Zhao J, Luo B, Ma X (2023) Numerical simulation of rock bursts triggered by blasting disturbance for deep-buried tunnels in jointed rock masses. Comput Geotech 161:105609. https://doi.org/10.1016/j.compgeo.2023.105609
Hu W, Cheng W-C, Wang L, Xue Z-F (2022) Micro-structural characteristics deterioration of intact loess under acid and saline solutions and resultant macro-mechanical properties. Soil till Res 220:105382. https://doi.org/10.1016/j.still.2022.105382
Huang Z, Wei B, Zhang L, Chen W, Peng Z (2019) Surface crack development rules and shear strength of compacted expansive soil due to dry–wet cycles. Geotech Geol Eng 37:2647–2657. https://doi.org/10.1007/s10706-018-00784-y
Jaeger F, Grohmann E, Schaumann GE (2006) 1H NMR relaxometry in natural humous soil samples: Insights in microbial effects on relaxation time distributions. Plant Soil 280:209–222. https://doi.org/10.1007/s11104-005-3035-4
Jaeger F, Bowe S, Van As H, Schaumann GE (2009) Evaluation of 1H NMR relaxometry for the assessment of pore-size distribution in soil samples. Eur J Soil Sci 60:1052–1064. https://doi.org/10.1111/j.1365-2389.2009.01192.x
Jia H, Ding S, Zi F, Dong Y, Shen Y (2020) Evolution in sandstone pore structures with freeze-thaw cycling and interpretation of damage mechanisms in saturated porous rocks. CATENA 195:104915. https://doi.org/10.1016/j.catena.2020.104915
Julina M, Thyagaraj T (2019) Quantification of desiccation cracks using X-ray tomography for tracing shrinkage path of compacted expansive soil. Acta Geotech 14:35–56. https://doi.org/10.1007/s11440-018-0647-4
Kareh KM, Lee PD, Atwood RC, Connolley T, Gourlay CM (2014) Revealing the micromechanisms behind semi-solid metal deformation with time-resolved X-ray tomography. Nat Commun 5:4464. https://doi.org/10.1038/ncomms5464
Laird DA (2006) Influence of layer charge on swelling of smectites. Appl Clay Sci 34:74–87. https://doi.org/10.1016/j.clay.2006.01.009
Li G, Wang F, Ma W, Fortier R, Mu Y, Mao Y, Hou X (2018) Variations in strength and deformation of compacted loess exposed to wetting–drying and freeze-thaw cycles. Cold Reg Sci Technol 151:159–167. https://doi.org/10.1016/j.coldregions.2018.03.021
Li X, Hong B, Wang L, Li L, Sun J (2020a) Microanisotropy and preferred orientation of grains and aggregates (POGA) of the Malan loess in Yan’an, China: a profile study. B Eng Geol Environ 79:1893–1907. https://doi.org/10.1007/s10064-019-01674-0
Li Y, Zhang W, He S, Aydin A (2020b) Wetting-driven formation of present-day loess structure. Geoderma 377:114564. https://doi.org/10.1016/j.geoderma.2020.114564
Liu T, Ding Z (1998) Chinese loess and the paleomonsoon. Annu Rev Earth Planet Sci 26:111–145. https://doi.org/10.1146/annurev.earth.26.1.111
Liu C, Shi B, Zhou J, Tang C (2011) Quantification and characterization of microporosity by image processing, geometric measurement and statistical methods: application on SEM images of clay materials. Appl Clay Sci 54:97–106. https://doi.org/10.1016/j.clay.2011.07.022
Liu Z, Liu F, Ma F, Wang M, Bai X, Zheng Y, Yin H, Zhang G (2015) Collapsibility, composition, and microstructure of loess in China. Can Geotech J 53:673–686. https://doi.org/10.1139/cgj-2015-0285
Liu K, Hu W, Gao C, Ye W (2021a) Energy dissipation of an infinite damping beam supported by saturated poroelastic halfspace. Phys Scr 96:055220. https://doi.org/10.1088/1402-4896/abe9ef
Liu K, Ye W, Jing H (2021b) Shear strength and damage characteristics of compacted expansive soil subjected to wet–dry cycles: a multi-scale study. Arab J Geosci 14:2866. https://doi.org/10.1007/s12517-021-09260-z
Liu K, Ye W, Jing H (2021c) Shear strength and microstructure of intact loess subjected to freeze-thaw cycling. Adv Mater Sci Eng 2021:1173603. https://doi.org/10.1155/2021/1173603
Lu H, Li J, Wang W, Wang C (2015) Cracking and water seepage of Xiashu loess used as landfill cover under wetting–drying cycles. Environ Earth Sci 74:7441–7450. https://doi.org/10.1007/s12665-015-4729-4
Lu H, Xu S, Li D, Li J (2018) An experimental study of mineral and microstructure for undisturbed loess polluted by landfill leachate. KSCE J Civ Eng 22:4891–4900. https://doi.org/10.1007/s12205-017-1799-8
Luo Z, Zhu Z, Ruan H, Shi C (2015) Extraction of microcracks in rock images based on heuristic graph searching and application. Comput Geosci 85:22–35. https://doi.org/10.1016/j.cageo.2015.08.013
Ma T, Wei C, Yao C, Yi P (2020) Microstructural evolution of expansive clay during drying–wetting cycle. Acta Geotech 15:2355–2366. https://doi.org/10.1007/s11440-020-00938-4
MCPRC (2009) Ministry of construction of the People’s Republic of China: code for investigation of geotechnical engineering (GB50021–2001). China Architecture and Building Press, Beijing
Morriss C, Rossini D, Straley C, Tutunjian P, Vinegar H (1997) Core analysis by low-field NMR. Log Anal 38:84–93
Nan J, Peng J, Zhu F, Zhao J, Leng Y (2021) Multiscale characteristics of the wetting deformation of Malan loess in the Yan’an area, China. J Mt Sci-Engl 18:1112–1130. https://doi.org/10.1007/s11629-020-6490-8
Ng CWW, Sadeghi H, Hossen SKB, Chiu CF, Alonso EE, Baghbanrezvan S (2016) Water retention and volumetric characteristics of intact and re-compacted loess. Can Geotech J 53:1258–1269. https://doi.org/10.1139/cgj-2015-0364
Pécsi M (1990) Loess is not just the accumulation of dust. Quatern Int 7–8:1–21. https://doi.org/10.1016/1040-6182(90)90034-2
Peng J, Sun P, Igwe O, Li XA (2018) Loess caves, a special kind of geo-hazard on loess plateau, northwestern China. Eng Geol 236:79–88. https://doi.org/10.1016/j.enggeo.2017.08.012
Penumadu D, Dean J (2000) Compressibility effect in evaluating the pore-size distribution of kaolin clay using mercury intrusion porosimetry. Can Geotech J 37:393–405. https://doi.org/10.1139/t99-121
Pu S, Zhu Z, Zhao L, Song W, Wan Y, Huo W, Wang H, Yao K, Hu L (2020) Microstructural properties and compressive strength of lime or/and cement solidified silt: a multi-scale study. B Eng Geol Environ 79:5141–5159. https://doi.org/10.1007/s10064-020-01910-y
Re A, Corsi J, Demmelbauer M, Martini M, Mila G, Ricci C (2015) X-ray tomography of a soil block: a useful tool for the restoration of archaeological finds. Herit Sci 3:4. https://doi.org/10.1186/s40494-015-0033-6
Salles F, Bildstein O, Douillard JM, Jullien M, Raynal J, Van Damme H (2010) On the cation dependence of interlamellar and interparticular water and swelling in smectite clays. Langmuir 26:5028–5037. https://doi.org/10.1021/la1002868
Schindelin J, Arganda-Carreras I, Frise E, Kaynig V, Longair M, Pietzsch T, Preibisch S, Rueden C, Saalfeld S, Schmid B, Tinevez J-Y, White DJ, Hartenstein V, Eliceiri K, Tomancak P, Cardona A (2012) Fiji: an open-source platform for biological-image analysis. Nat Meth 9:676–682. https://doi.org/10.1038/nmeth.2019
Schult A, Shi G (1997) Hydration swelling of crystalline rocks. Geophys J Int 131:179–186. https://doi.org/10.1111/j.1365-246X.1997.tb00604.x
Starkloff T, Larsbo M, Stolte J, Hessel R, Ritsema C (2017) Quantifying the impact of a succession of freezing-thawing cycles on the pore network of a silty clay loam and a loamy sand topsoil using X-ray tomography. CATENA 156:365–374. https://doi.org/10.1016/j.catena.2017.04.026
Sun H, Liu X, Ye Z, Wang E (2021a) Experimental investigation of the nonlinear evolution from pipe flow to fissure flow during carbonate rock failures. B Eng Geol Environ 80:4459–4470. https://doi.org/10.1007/s10064-021-02210-9
Sun Y, Zhai C, Xu J, Cong Y, Zheng Y (2021b) Experimental study on pore structure evolution of coal in macroscopic, mesoscopic, and microscopic scales during liquid nitrogen cyclic cold-shock fracturing. Fuel 291:120150. https://doi.org/10.1016/j.fuel.2021.120150
Tang C, Shi B, Liu C, Zhao L, Wang B (2008) Influencing factors of geometrical structure of surface shrinkage cracks in clayey soils. Eng Geol 101:204–217. https://doi.org/10.1016/j.enggeo.2008.05.005
Tang C, Shi B, Liu C, Suo W, Gao L (2011) Experimental characterization of shrinkage and desiccation cracking in thin clay layer. Appl Clay Sci 52:69–77. https://doi.org/10.1016/j.clay.2011.01.032
Tang L, Wang K, Jin L, Yang G, Jia H, Taoum A (2018) A resistivity model for testing unfrozen water content of frozen soil. Cold Reg Sci Technol 153:55–63. https://doi.org/10.1016/j.coldregions.2018.05.003
Tang H, Duan Z, Wang D, Dang Q (2020) Experimental investigation of creep behavior of loess under different moisture contents. B Eng Geol Environ 79:411–422. https://doi.org/10.1007/s10064-019-01545-8
Tian H, Wei C, Wei H, Yan R, Chen P (2014) An NMR-based analysis of soil–water characteristics. Appl Magn Reson 45:49–61. https://doi.org/10.1007/s00723-013-0496-0
Tian H, Wei C, Lai Y, Chen P (2018) Quantification of water content during freeze–thaw cycles: a nuclear magnetic resonance based method. Vadose Zone J 17:160124. https://doi.org/10.2136/vzj2016.12.0124
Traskin VY (2009) Rehbinder effect in tectonophysics. Izv, Phys Solid Earth 45:952. https://doi.org/10.1134/S1069351309110032
Wang C, Zhang Z, Qi W, Fan S (2018) Morphological approach to quantifying soil cracks: application to dynamic crack patterns during wetting–drying cycles. Soil Sci Soc Am J 82:757–771. https://doi.org/10.2136/sssaj2017.03.0088
Wang H, Ni W, Li X, Li L, Yuan K, Nie Y (2021a) Predicting the pore size distribution curve based on the evolution mechanism of soil–water characteristic curve. Environ Earth Sci 81:23. https://doi.org/10.1007/s12665-021-10138-2
Wang P, Liu E, Zhi B (2021b) An elastic-plastic model for frozen soil from micro to macro scale. Appl Math Model 91:125–148. https://doi.org/10.1016/j.apm.2020.09.039
Wang S, Sun Q, Wang N, Luo T, Zhang H (2021c) High-temperature response characteristics of loess porosity and strength. Environ Earth Sci 80:547. https://doi.org/10.1007/s12665-021-09799-w
Wichtmann T, Triantafyllidis T (2009) Influence of the grain-size distribution curve of quartz sand on the small strain shear modulus Gmax. J Geotech Geoenviron 135:1404–1418. https://doi.org/10.1061/(ASCE)GT.1943-5606.0000096
Wu Z, Wong HS, Buenfeld NR (2017) Transport properties of concrete after drying-wetting regimes to elucidate the effects of moisture content, hysteresis and microcracking. Cem Concr Res 98:136–154. https://doi.org/10.1016/j.cemconres.2017.04.006
Xie X, Qi S, Zhao F, Wang D (2018) Creep behavior and the microstructural evolution of loess-like soil from Xi’an area, China. Eng Geol 236:43–59. https://doi.org/10.1016/j.enggeo.2017.11.003
Xu J, Li Y, Ren C, Lan W (2020) Damage of saline intact loess after dry–wet and its interpretation based on SEM and NMR. Soils Found 60:911–928. https://doi.org/10.1016/j.sandf.2020.06.006
Xu P, Zhang Q, Qian H, Yang F, Zheng L (2021) Investigating the mechanism of pH effect on saturated permeability of remolded loess. Eng Geol 284:105978. https://doi.org/10.1016/j.enggeo.2020.105978
Xu P, Qian H, Zhang Q, Li W, Ren W (2022a) Investigating saturated hydraulic conductivity of remolded loess subjected to CaCl2 solution of varying concentrations. J Hydrol 612:128135. https://doi.org/10.1016/j.jhydrol.2022.128135
Xu P, Qian H, Zhang Q, Shang J, Guo Y, Li M (2022b) Response mechanism of permeability change of remolded loess to seepage parameters. J Hydrol 612:128224. https://doi.org/10.1016/j.jhydrol.2022.128224
Xu P, Qian H, Chen J, Wang L, Abliz X, He X, Ma G, Liu Y (2023a) New insights into microstructure evolution mechanism of compacted loess and its engineering implications. B Eng Geol Environ 82:36. https://doi.org/10.1007/s10064-022-03058-3
Xu P, Qian H, Li S, Li W, Chen J, Liu Y (2023b) Geochemical evidence of fluoride behavior in loess and its influence on seepage characteristics: an experimental study. Sci Total Environ 882:163564. https://doi.org/10.1016/j.scitotenv.2023.163564
Xu P, Qian H, Li W, Ren W, Yang F, Wang L (2023c) New insights into the seepage behavior of heavy metal-contaminated loess and its underlying geochemical mechanism. J Hydrol 620:129476. https://doi.org/10.1016/j.jhydrol.2023.129476
Yan X, Duan Z, Sun Q (2021) Influences of water and salt contents on the thermal conductivity of loess. Environ Earth Sci 80:52. https://doi.org/10.1007/s12665-020-09335-2
Ye WJ, Li CQ (2019) The consequences of changes in the structure of loess as a result of cyclic freezing and thawing. B Eng Geol Environ 78:2125–2138. https://doi.org/10.1007/s10064-018-1252-3
Yu B, Li J (2004) A geometry model for tortuosity of flow path in porous media. Chin Phys Lett 21:1569–1571. https://doi.org/10.1088/0256-307x/21/8/044
Zhang D, Wang J, Chen C, Wang S (2020a) The compression and collapse behaviour of intact loess in suction-monitored triaxial apparatus. Acta Geotech 15:529–548. https://doi.org/10.1007/s11440-019-00829-3
Zhang S, Liu H, Chen W, Liu F (2020b) Strength of recompacted loess affected by coupling between acid-base pollution and freeze-thaw cycles. J Cold Reg Eng 34:04020024. https://doi.org/10.1061/(asce)cr.1943-5495.0000230
Acknowledgements
This work is supported by the National Natural Science Foundation of China (Grant No. 42072319).
Funding
National Natural Science Foundation of China, 42072319, Wanjun Ye.
Author information
Authors and Affiliations
Contributions
KL contributed to conceptualization, methodology, investigation, data curation, formal analysis, software, validation, visualization, and writing—original draft preparation, and writing—review and editing. WY contributed to conceptualization, methodology, resources, funding acquisition, visualization, and writing—review and editing. HJ contributed to conceptualization, investigation, supervision, validation, and writing—review and editing. All authors read and approved the final manuscript.
Corresponding author
Ethics declarations
Conflict of interest
The authors declare that they have no conflict of interest.
Additional information
Publisher's Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
About this article
Cite this article
Liu, K., Ye, W. & Jing, H. Multiscale evaluation of the structural characteristics of intact loess subjected to wet/dry cycles. Nat Hazards 120, 1215–1240 (2024). https://doi.org/10.1007/s11069-023-06253-x
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11069-023-06253-x