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Solidification of high-speed tool steels

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Abstract

Gradient solidification and differential thermal analysis (DTA) experiments were used to study the process of solidification and the solidification microstructure of 11 alloys comprising the composition range of customary commercial high-speed steels (with the exception of cobalt-alloyed grades). Also included are a number of experimental high-speed steels alloyed with niobium. The results include the effects of alloy composition and cooling rate on the width of the solidification interval and on the sequence of the solidification reactions; the types of eutectics formed (austenite with M6C, M2C, or MC) and their volume fractions; the chemical compositions of the ledeburitic and primary carbides; and the relation between the chemistry of the carbides and that of the melt. Special attention is given to the formation and composition of heterogeneously nucleated primary MC particles and to the chemistry and stability of eutectic M2C, which is important as a precursor to MC and M6C in the microstructure of finished (hot-worked and heat-treated) material.

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References

  1. K. Stiller, L.-E. Svensson, P.R. Howell, Wang Rong, H.-O. Andrén, and G.L. Dunlop,Acta Metall., 1984, vol. 32, pp. 1457–67.

    Article  CAS  Google Scholar 

  2. H. Fischmeister, S. Karagöz, and H.-O. Andrén,Acta Metall., 1988, vol. 36, pp. 817–25.

    Article  CAS  Google Scholar 

  3. S. Karagöz, E. Kudielka, and H. Fischmeister:Microchim. Acta, 1981, Suppl. II, pp. 391–419.

    Article  Google Scholar 

  4. H. Fischmeister, S. Karagöz, I. Liem, J. Paul, and M. Poech:Acta Stereol., 1986, vol. 5 (2), pp. 287–97.

    CAS  Google Scholar 

  5. S. Karagöz and H. Fischmeister:Steel Research, 1987, vol. 1, pp. 46–51.

    Google Scholar 

  6. H. Fischmeister, I. Liem, and S. Karagöz:Pract. Metallogr., 1987, Sonderband 15, pp. 323–32.

    Google Scholar 

  7. S. Karagöz, I. Liem, E. Bischoff, and H. Fischmeister:Metall. Trans. A, in press.

  8. H. Fischmeister, S. Karagöz, E. Kudielka, and J. Püber:Proc. Coll. Acters Speciaux, St. Etienne, 1983, Circle d'Etudes des Mètaux, St. Etienne, 1983, paper 6.

    Google Scholar 

  9. R. Riedl, S. Karagöz, H. Fischmeister, and F. Jeglitsch:Steel Research, 1987, vol. 58, pp. 339–52.

    CAS  Google Scholar 

  10. H. Fischmeister:Specialty Steels and Hard Metals, N.R. Comins and J.B. Clark, eds., Pergamon Press, Oxford, 1983, pp. 127–40.

    Google Scholar 

  11. S. Karagöz and H. Fischmeister:Steel Research, 1987, vol. 58, pp. 353–61.

    Google Scholar 

  12. H. Fischmeister, J. Paul, and S. Karagöz:Pract. Metallogr., 1988, vol. 25, pp. 28–40.

    Google Scholar 

  13. H. Fischmeister and L.R. Olsson:Cutting Tool Materials, ASM, Metals Park, OH, 1981, pp. 111–31.

    Google Scholar 

  14. K. Kuo:J. Iron Steel Inst., 1955, vol. 177, pp. 218–27.

    Google Scholar 

  15. R.W. Kraft:Solidification, ASM, Metals Park, OH, 1971, pp. 275–94.

    Google Scholar 

  16. R.H. Barkalow, R.W. Kraft, and J.I. Goldstein:Metall. Trans., 1972, vol. 3, pp. 919–26.

    Article  CAS  Google Scholar 

  17. P.O. Mellberg and H. Sandberg:Scand. J. Metall., 1973, vol. 2, pp. 83–86.

    CAS  Google Scholar 

  18. E.J. Galda and R.W. Kraft:Metall. Trans., 1974, vol. 5, pp. 1727–33.

    Article  CAS  Google Scholar 

  19. H. Fredriksson:Met. Sci., 1976, vol. 10, pp. 77–86.

    Article  CAS  Google Scholar 

  20. H. Fredriksson and S. Brising:Scand. J. Metall., 1976, vol. 5, pp. 268–75.

    CAS  Google Scholar 

  21. H. Fredriksson and M. Nica:Scand. J. Metall., 1979, vol. 8, pp. 243–53.

    CAS  Google Scholar 

  22. A.S. Ballantyne and A. Mitchell:Solidification and Casting of Metals, Metals Soc., London, 1979, no. 192, pp. 363–70.

    Google Scholar 

  23. H. Brandis and K. Wiebking,DEW-Techn. Ber., 1971, vol. 11, pp. 158–65.

    CAS  Google Scholar 

  24. H. Müller and C. Weiss: Dr. Ing. Thesis, Bergakademie Freiberg. VEB Deutscher Verlag Grundstoffind, Leipzig, German Democratic Republic, 1977.

  25. R. Riedl and H. Fischmeister:Berg- und Huettenm. Monatsh., 1984, vol. 129, pp. 131–35.

    CAS  Google Scholar 

  26. M.A. Taha, H. Jacobi, M. Imagumbai, and K. Schwerdtfeger:Metall. Trans. A, 1982, vol. 13A, pp. 2131–41.

    Google Scholar 

  27. S. Karagöz and H. Fischmeister:Pract. Metallogr., 1983, Sonderband 4, pp. 90–100.

    Google Scholar 

  28. E. Horn and H. Brandis:DEW-Techn. Ber., 1971, vol. 11, pp. 147–54.

    CAS  Google Scholar 

  29. G. Steven, A.E. Nehrenberg, and T.V. Philip:Trans. ASM, 1964, vol. 57, pp. 925–48.

    CAS  Google Scholar 

  30. Anon.:A Guide to the Solidification of Steels, Jernkontoret, Stockholm, Sweden, 1977, pp. 162.

  31. B. Frykendahl: Tekn. Dr. Thesis, Royal Institute of Technology, Stockholm, Sweden, 1978.

  32. R.H. Barkalow: Ph.D. Thesis, Lehigh University, Bethlehem, PA, 1971.

  33. A. Suzuki and Y. Nagaoka:J. JIM, 1969, vol. 33, pp. 658–63.

    Google Scholar 

  34. T. Edvardsson, and H. Fredriksson, and I. Svensson:Met. Sci., 1976, vol. 10, pp. 298–306.

    CAS  Google Scholar 

  35. H. Jacobi:Giessen und Erstarren von Stahl, EGKS Conf., Luxemburg, 1977, Verlag Stahleisen, Düsseldorf, Federal Republic of Germany, pp. 108–42.

    Google Scholar 

  36. B.A. Rickinson and D.H. Kirkwood:Solidification and Casting of Metals, Metals Soc., London, 1979, pp 44–52.

    Google Scholar 

  37. J.D. Hunt:Solidification and Casting of Metals, Metals Soc., London, 1979, pp. 3–9.

    Google Scholar 

  38. W.D. Kurz and D.J. Fisher:Acta Metall., 1981, vol. 29, pp. 11–20.

    Article  CAS  Google Scholar 

  39. R. Trivedi:Metall. Trans. A, 1984, vol. 15A, pp. 977–82.

    CAS  Google Scholar 

  40. R. Riedl, K. Löcker, and F. Jeglitsch:Pract. Metallogr., 1986, vol. 23, pp. 374–99.

    CAS  Google Scholar 

  41. M.E. Glicksman and P.W. Voorhees:Metall, Trans. A, 1984, vol. 15A, pp. 995–1001.

    CAS  Google Scholar 

  42. U. Feurer and R. Wunderlin:Fachber, DGM, DGM-SB 38/ 667/X, Oberursel, Federal Republic of Germany, 1977.

  43. T.Z. Kattamis, J.C. Coughlin, and M.C. Flemings:Trans. TMS-AIME, 1967, vol. 239, pp. 1504–11.

    CAS  Google Scholar 

  44. M.C. Flemings, T.F. Bower, T.Z. Kattamis, and H.D. Brody: AMC Contract Report No. DA-19-020-Ord-5706 (A), 122 H, Massachusetts Institute of Technology, Cambridge, MA.

  45. S.-C. Huang and M.E. Glicksman:Acta Metall., 1981, vol. 29, pp. 701–15.

    Article  CAS  Google Scholar 

  46. D.J. Allen and J.D. Hunt:Solidification and Casting of Metals, Metals Soc., London, 1979, pp. 39–43.

    Google Scholar 

  47. R. Riedl and H. Fischmeister:Metall. Trans. A, in press.

  48. H. Tensi and H. Fuchs:Z. Metallkd., 1983, vol. 74, pp. 351–57.

    CAS  Google Scholar 

  49. H. Tensi and H. Fuchs:Giessereiforschung, 1983, vol. 35, pp. 61–68.

    Google Scholar 

  50. Y.-K. Jang and F. Jeglitsch:Z. Metallkd., 1985, vol. 76, pp. 717–23.

    CAS  Google Scholar 

  51. J.D. Hunt and K.A. Jackson:Trans. AIME, 1967, vol. 239, pp. 864–67.

    CAS  Google Scholar 

  52. Y. Sedov, Y.A. Geller, L.S. Kremnev, and A.G. Gordesiani:Metalloved. Term. Obrab. Met., 1975, pp. 4–9.

  53. D.J. Fisher and W. Kurz:Acta Metall., 1980, vol. 28, pp. 777–94.

    Article  CAS  Google Scholar 

  54. H.E. Exner and J. Paul:Met. Sci., 1983, vol. 17, pp. 141–43.

    Article  CAS  Google Scholar 

  55. J.V. Wood:Solidification and Casting of Metals, Metals Soc., London, 1979, pp. 179–83.

    Google Scholar 

  56. S. Karagöz and H. F. Fischmeister:Metall. Trans. A, 1988, vol. 19A, pp. 1395–401.

    Google Scholar 

  57. H.F. Fischmeister, S. Karagöz, S. Larsson, I. Liem, and P. Sotkovszki:Pract. Metallogr., 1987, Sonderband 18, pp. 467–78.

    CAS  Google Scholar 

  58. R. Riedl, S. Karagöz, and H. Fischmeister:Z. Metallkd., 1983, vol. 74, pp. 199–205.

    CAS  Google Scholar 

  59. Y.N. Taran and A.M. Nesterenko:Izv. Akad. Nauk SSSR, Met., 1981, vol. 5, pp. 213–17.

    Google Scholar 

  60. Y.N. Malinochka, M.A. Olikhova, L.N. Bagnyuk, and Y.S. Shmelev:Met. Sci. Heat Treat. (USSR), 1982, vol. 24, pp. 3–8.

    Article  Google Scholar 

  61. S. Karagöz, R. Riedl, M.R. Gregg, and H. Fischmeister:Pract. Metallogr., 1983, Sonderband 14, pp. 369–82;The Charles Hatchett Award Papers, 1986, The Institute of Metals, London, and CBMM, São Paulo, 1986, pp. 15–19.

    Google Scholar 

  62. L.D. Moskevich, N.N. Kurasov, and N.E. Evlampieva:Met. Sci. Heat Treat. (USSR), 1979, vol. 21, pp. 459–63.

    Article  Google Scholar 

  63. K. Bungardt, E. Haberling, A. Rose, and H.H. Weigand:DEW-Techn. Ber., 1972, vol. 12, pp. 111–13.

    CAS  Google Scholar 

  64. A. Fischer and E. Kohlhaas,Pract. Metallogr., 1975, vol. 12, pp. 393–406.

    CAS  Google Scholar 

  65. Y.N. Taran, P.F. Nizhninovskaya, L.M. Snagovskii, S.B. Vukelich, and A.M. Nesterenko:Metalloved. Term. Obrab. Met., 1979, pp. 46–59.

  66. E. Horn:DEW-Techn. Ber., 1972, vol. 12, pp. 217–24.

    CAS  Google Scholar 

  67. H. Fredricksson, M. Hillert, and M. Nica,Scand. J. Metall., 1979, vol. 8, pp. 115–22.

    Google Scholar 

  68. S. Karagöz, K. Schur, and H. Fischmeister:Beitr. Elektronen-mikroskop. Direktabb. Oberfl., 1982, vol. 15, pp. 235–38.

    Google Scholar 

  69. J.V. Wood and I.R. Sare:Proc. 2nd Int. Conf. Rapidly Quenched Metals, Massachusetts Institute of Technology, Cambridge, MA, 1975, pp. 87–94.

  70. Y.-K. Jang, M. Poech, and F. Jeglitsch.Pract. Metallogr., 1985, Sonderband 16, pp. 393–403.

    CAS  Google Scholar 

  71. T.K. Jones and T. Mukherjee:J. Iron Steel Inst., 1970, vol. 208, pp. 90–92.

    CAS  Google Scholar 

  72. E. Haberling and P. Gümpel:TEW-Techn. Ber., 1980, vol. 6, pp. 127–31.

    CAS  Google Scholar 

  73. D. Krump and O. Gründler:Microchim. Acta, 1975, Suppl. 6, pp. 49–64.

    Google Scholar 

  74. H.H. Weigand and E. Haberling:TEW-Techn. Ber., 1975, vol. 1, pp. 110–21.

    CAS  Google Scholar 

  75. G. Lennartz and G. Preis:DEW-Techn. Ber., 1973, vol. 13, pp. 55–59.

    CAS  Google Scholar 

  76. S. Karagöz: Dr.Mont. Thesis, Austrian School of Mines (Montanuniversität), Leoben, Austria, 1982.

  77. H. Ortmann: Dr.Ing. Thesis, RWTH Aachen, Federal Republic of Germany, 1976.

  78. H. Brandis, E. Haberling, and H.H. Weigand:Proc. Symp. Ferrous Metall. Comm. AIME, 109th Annual Meeting. Las Vegas, NV, 1980, AIME, Warrendale, PA, 1980, pp. 1–18.

  79. M.R. Gomashchi and C.M. Sellars:Met. Sci., 1984, vol. 18, pp. 44–48.

    Article  Google Scholar 

  80. G. Steven, J.J. Hauser, T.A. Neumeyer, and J.M. Capenos:Trans. ASM, 1969, vol. 62, pp. 180–94.

    CAS  Google Scholar 

  81. D.B. Clayton:Metallurgia, 1965, vol. 71, pp. 247–50.

    CAS  Google Scholar 

  82. C. Kim, V. Biss, and W.F. Hosford:Metall. Trans. A, 1982, vol. 13A, pp. 185–91.

    CAS  Google Scholar 

  83. M. Bergström:Mater. Sci. Eng., 1977, vol. 27, pp. 257–69.

    Article  Google Scholar 

  84. R. Kieffer and F. Benesovsky:Hartstoffe, Springer, Wien, Austria, 1963, pp. 257–63.

    Google Scholar 

  85. R. Kieffer, H. Nowotny, A. Heckel, P. Ettmayr, and L. Ilsner:Monatsh. Chemie., 1968, vol. 99, pp. 1020–27.

    Article  CAS  Google Scholar 

  86. G.P. Dimitrieva and A.K. Shurin:Sov. Powder Met. Ceram., 1980, vol. 19, pp. 699–702.

    Article  Google Scholar 

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Fischmeister, H.F., Riedl, R. & Karagöz, S. Solidification of high-speed tool steels. Metall Trans A 20, 2133–2148 (1989). https://doi.org/10.1007/BF02650299

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