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Review of small specimen test techniques for irradiation testing

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Abstract

Small specimen test technology has evolved out of the necessity to develop and monitor materials proposed for or used in nuclear power generation systems. Development of materials for improved cladding and in-core structures for fission reactors and assessment of core materials and pressure vessel steels already under irradiation necessitated the use of specimens which fit into existing irradiation space or which could be extracted from irradiated structures, such as cladding or ducts. Interest in simulating neutron irradiation by light and heavy ion irradiation led to the development of thin foil and wire geometry specimens. Further, interest in developing materials for fusion reactors has added additional constraints on specimen sizes associated with available irradiation volumes in existing and proposed high-energy neutron irradiation facilities. Consequently, a wide array of specimen geometries and test techniques has now been developed. It is the purpose of this paper to review these techniques and examine their status, problems, and potential for future applications.

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References

  1. C.D. Williams:React. Technol., 1970, vol. 13 (2), pp. 147–69.

    CAS  Google Scholar 

  2. J.A.L. Robertson:Irradiation Effects in Nuclear Fuels, AEC Monograph, Gordon and Breach, New York, NY, 1969.

    Google Scholar 

  3. M. Simnad:Fuel Element Experiences in Nuclear Reactors, AEC Monograph, Gordon and Breach, New York, NY, 1971.

    Google Scholar 

  4. S.N. Buckley: inProperties of Reactor Materials and the Effects of Radiation Damage, D.J. Littler, ed., Butterworth’s, London, 1962, p. 39.

    Google Scholar 

  5. D.G. Franklin, G.E. Lucas, and A.L. Bernent:Creep of Zirconium Alloys in Nuclear Reactors, ASTM STP 815, ASTM, Philadelphia, PA, 1983.

    Google Scholar 

  6. Weld. Res. Bull., Aug. 1972, no. 175.

  7. D.L. Styris, R.H. Jones, O.K. Harling, G.L. Kulcinski, and R.P. Marshall: Report No. BNWL-1961, Battelle Pacific Northwest Laboratories, Richland, WA, 1975.

    Google Scholar 

  8. G.L. Kulcinski, J.J. Laidler, and D.G. Doran:Radiat. Eff., 1971, vol. 7, pp. 195–202.

    Article  CAS  Google Scholar 

  9. R.S. Nelson, D.J. Mazey, and J.A. Hudson:J. Nucl. Mater., 1970, vol. 37, pp. 1–12.

    Article  CAS  Google Scholar 

  10. R.J. McElroy, J.A. Hudson, and R.J. Francis: Report No. AERE-R-7998, Harwell Laboratories, United Kingdom Atomic Energy Authority, Harwell, United Kingdom, 1976.

    Google Scholar 

  11. P.L. Hendrick: Sc.D. Thesis, Massachusetts Institute of Technology, Cambridge, MA, 1975.

    Google Scholar 

  12. Proc. Workshop on Correlation of Neutron and Charged Particle Damage, J.O. Stiegler, ed., USERDA, CONF-760673, Oak Ridge, TN, 1976.

  13. G.E. Lucas: Sc.D. Thesis, Massachusetts Institute of Technology, Cambridge, MA, 1978.

    Google Scholar 

  14. R.H. Jones and D.L. Styris: Report No. BNWL-SA-5955, Battelle Pacific Northwest Laboratories, Richland, WA, 1976.

    Google Scholar 

  15. Draft Recommended Practice for the Measurement of Mechan ical Properties during Charged Particle Irradiation, Task Group A, E10.08, ASTM, Philadelphia, PA, May 1978.

  16. The Fusion Reactor Materials Program Plan, Report No. DOE/ ET-0032/2, U.S. Department of Energy, Washington, DC, July 1978.

  17. Experimenter’s Guide, RTNS-II Facility, M-094, Lawrence Livermore Laboratory, Livermore, CA, 1978.

  18. J.W. Hagan, E.K. Opperman, and A.L. Trego:J. Nucl. Mater., 1984, vol. 122–123, pp. 958–62.

    Article  Google Scholar 

  19. N.F. Panayotou, R.J. Puigh, and E.K. Opperman:J. Nucl. Mater., 1981, vol. 103–104, pp. 1523–26.

    Article  Google Scholar 

  20. S. Jitsukawa: inReport of the US Japan Workshop on Small Specimen Testing Techniques, Department of Fuels and Materials Research, Japan Atomic Energy Research Institute, Ibaraki-ken, Japan, 1988, pp. 145–60.

    Google Scholar 

  21. S.P. Keeler and W.A. Backofen:Trans. ASM, 1963, vol. 56, p. 25.

    Google Scholar 

  22. G.E. Dieter: inDuctility, ASM, Metals Park, OH, 1968.

    Google Scholar 

  23. M.J. Barba:Mem. Soc. Ing. Civils, 1880, Part I, p. 682.

  24. R.W. Armstrong:J. Mech. Phys. Solids, 1961, vol. 9, p. 196.

    Article  CAS  Google Scholar 

  25. N. Igata, K. Miyahara, C. Tada, D. Blasl, and G. Lucas:Radiat. Eff., 1986, vol. 101, pp. 131–46.

    Article  Google Scholar 

  26. A. Kohyama, K. Asakira, K. Hanada, K. Asano, and H. Matsui: inProc. 14th Symp. on the Effects of Radiation on Materials, ASTM, Andover, MA, June 1988, in press.

    Google Scholar 

  27. M.L. Hamilton and H.L. Heinisch: inProc. 14th Symp. on the Effects of Radiation on Materials, ASTM, Andover, MA, June 1988, in press.

    Google Scholar 

  28. K.P. Dubrovin, S.T. Konobeyevsky, B. Milevitsky, L.D. Panteleyev, P.A. Platonov, and N.F. Pavdyuk: inProperties of Reactor Materials and the Effects of Radiation Damage, D.J. Littler, ed., Butterworth’s, London, 1962.

    Google Scholar 

  29. R.V. Hesketh: inProperties of Reactor Materials and the Effects of Radiation Damage, D.J. Littler, ed., Butterworth’s, London, 1962.

    Google Scholar 

  30. E.R. Gilbert and B.A. Chin:Nucl. Technol., 1981, vol. 52, p. 273.

    CAS  Google Scholar 

  31. A.J. Lovell, B.A. Chin, and E.R. Gilbert:J. Mater. Sci., 1981, vol. 16, p. 870.

    Article  CAS  Google Scholar 

  32. E.R. Gilbert and B.A. Chin: ASTM STP 725, ASTM, Philadelphia, PA, 1981, pp. 665–79.

  33. R.J. Puigh and R.E. Schenter: ASTM STP 870, ASTM, Philadelphia, PA, 1985, pp. 795–802.

  34. E.R. Gilbert and CD. Blackburn:J. Eng. Mater. Technol., 1977, vol. 99, p. 168.

    CAS  Google Scholar 

  35. E.K. Opperman, J.L. Straalsund, G.L. Wire, and R.H. Howell:Nucl. Technol., 1979, vol. 42, p. 71.

    CAS  Google Scholar 

  36. P. Jung and N.M. Afify:J. Nucl. Mater., 1988, vol. 155–157, pp. 1019–24.

    Article  Google Scholar 

  37. A.D. Marwick:J. Nucl. Mater., 1975, vol. 55, p. 259.

    Article  CAS  Google Scholar 

  38. D. Tabor:The Hardness of Metals, Clarendon Press, London, 1951.

    Google Scholar 

  39. G.E. Lucas and N.F. Panayotou:J. Nucl. Mater., 1981, vol. 103–104, pp. 1527–32.

    Article  Google Scholar 

  40. G.E. Lucas, G.R. Odette, R. Maiti, and J.W. Sheckherd: ASTM STP 956, ASTM, Philadelphia, PA, 1987, pp. 379–94.

  41. J. Mancuso, J. Spitznagel, R.P. Shogan, and J. Holland: ASTM STP 725, ASTM, Philadelphia, PA, 1981, p. 38.

  42. K. Furuya and J. Moteff:Metall. Trans. A, 1981, vol. 12A, pp. 1303–11.

    Google Scholar 

  43. J.R. Cahoon, W.H. Broughton, and A.R. Kutzak:Metall. Trans., 1971, vol. 2, pp. 1979–83.

    CAS  Google Scholar 

  44. P. Au, G.E. Lucas, J.W. Sheckherd, and G.R. Odette: inNon-destructive Evaluation in the Nuclear Industry, ASM, Metals Park, OH, 1981, pp. 597–610.

    Google Scholar 

  45. F. Haggag and G.E. Lucas:Metall. Trans. A, 1983, vol. 14A, pp. 1607–13.

    Google Scholar 

  46. K. Shinohara, G.E. Lucas, and G.R. Odette:J. Nucl. Mater., 1986, vol. 133–134, pp. 326–31.

    Google Scholar 

  47. E. Meyer:Z. Ver. Deut. Ing., 1908, vol. 52, p. 645.

    CAS  Google Scholar 

  48. J.A. Brinell:Congr. Int. Method d’Essai, Paris, 1900.

  49. H.A. Francis:Trans. ASME, 1976, Series H, vol. 2, p. 272.

    Google Scholar 

  50. R. Boklen: inThe Science of Hardness Testing and Its Applications, J. Wetbrook and H. Conrad, eds., ASM, Metals Park, OH, 1973, p. 109.

    Google Scholar 

  51. M. Jayakumar and G.E. Lucas:J. Nucl. Mater., 1984, vol. 122–123, pp. 840–44.

    Article  Google Scholar 

  52. J.B. Pethica, R. Hutchings, and W.C. Oüver:Phil. Mag., 1983, vol. 48, pp. 593–606.

    Article  CAS  Google Scholar 

  53. J.B. Pethica: inIon Implantation into Metals, V. Ashwal, ed., Pergamon Press, Oxford, 1982, pp. 147–56.

    Google Scholar 

  54. S. Zinkle and W.C. Oliver:J. Nucl. Mater., 1986, vol. 141–143, pp. 548–52.

    Article  Google Scholar 

  55. D. Tabor: ASTM STP 889, ASTM, Philadelphia, PA, 1986.

  56. F.G. Yost: SAND 82-0795J, Sandia National Laboratory, 1982.

  57. J.M. Baik, J. Kameda, and O. Buck: ASTM STP 888, ASTM, Philadelphia, PA, 1986, pp. 92–110.

  58. M.P. Manahan, A.S. Argon, and O.K. Harling:J. Nucl. Mater., 1981, vol. 103–104, pp. 1545–50.

    Article  Google Scholar 

  59. G.E. Lucas, A. Okada, and M. Kiritani:J. Nucl. Mater., 1986, vol. 141–143, pp. 532–35.

    Article  Google Scholar 

  60. F.H. Huang, M.L. Hamilton, and G.L. Wire:Nucl. Technol., 1982, vol. 57, pp. 234–42.

    CAS  Google Scholar 

  61. M.P. Manahan, A.E. Browning, A.S. Argon, and O.K. Harling: ASTM STP 888, ASTM, Philadelphia, PA, 1986, pp. 17–49.

  62. O.K. Harling, M. Lee, D.-S. Sohn, G. Kohse, and C.W. Lau: ASTM STP 888, ASTM, Philadelphia, PA, 1986, pp. 50–65.

  63. M. Dooley, G.E. Lucas, and J.W. Sheckherd:J. Nucl. Mater., 1981, vol. 103–104, pp. 1533–36.

    Article  Google Scholar 

  64. Amit K. Ghosh:Metall. Trans. A, 1976, vol. 7A, pp. 523–33.

    CAS  Google Scholar 

  65. A. Okada, G.E. Lucas, and M. Kiritani:Trans. Jpn. Inst. Met., 1988, vol. 29 (2), pp. 99–108.

    CAS  Google Scholar 

  66. G. Khose, M. Ames, and O.K. Harling:J. Nucl. Mater., 1986, vol. 141–143, pp. 513–17.

    Article  Google Scholar 

  67. T. Misawa, T. Actachi, M. Saito, and Y. Hamaguchi:J. Nucl. Mater., 1987, vol. 150, p. 194.

    Article  CAS  Google Scholar 

  68. X. Mao, T. Shoji, and H. Takahashi:J. Test. Eval., 1987, vol. 15, p. 30.

    Google Scholar 

  69. G.E. Lucas, J.W. Sheckherd, G.R. Odette, and S. Panchanadeeswaran:J. Nucl. Mater., 1984, vol. 122–123, pp. 429–32.

    Article  Google Scholar 

  70. G.E. Lucas, J.W. Sheckherd, and G.R. Odette: ASTM STP 888, ASTM, Philadelphia, PA, 1986, pp. 112–40.

  71. P.S. Kullen, H.H. Smith, and D.J. Michel:J. Nucl. Mater., 1988, vol. 158, pp. 57–63.

    Article  CAS  Google Scholar 

  72. H.H. Smith and D.J. Michel:Mater. Sci. Eng., in press.

  73. K. Abe: inReport of the US Japan Workshop on Small Specimen Testing Techniques, Department of Fuels and Materials Research, Japan Atomic Energy Research Institute, Ibaraki-ken, Japan, 1988, pp. 107–12.

    Google Scholar 

  74. S. Nunomura, Y. Higo, T. Nishijima, and G. Forie: inReport of the US Japan Workshop on Small Specimen Testing Techniques, Department of Fuels and Materials Research, Japan Atomic Energy Research Institute, Ibaraki-ken, Japan, 1988, pp. 113–23.

    Google Scholar 

  75. W.R. Corwin and A.M. Hougland: ASTM STP 888, ASTM, Philadelphia, PA, 1986, pp. 325–38.

  76. G.E. Lucas, G.R. Odette, J.W. Sheckherd, P. McConnell, and J. Perrin: ASTM STP 888, ASTM, Philadelphia, PA, 1986, pp. 305–24.

  77. W.L. Hu: inADIP Semiannual Progress Report for the Period Ending September 30, 1982, Report No. DOE/ER-0045/9, U.S. Department of Energy, Washington, DC, 1982, pp. 225–71.

    Google Scholar 

  78. H. Kayano, Y. Sasaki, A. Kimura, M. Narui, and T. Kikuchi: inReport of the US Japan Workshop on Small Specimen Testing Techniques, Department of Fuels and Materials Research, Japan Atomic Energy Research Institute, Ibaraki-ken, Japan, 1988, pp. 135–44.

    Google Scholar 

  79. B.S. Louden, A.S. Kumar, F.A. Garner, M.L. Hamilton, and W.L. Hu:J. Nucl. Mater., 1988, vol. 155–157, pp. 662–67.

    Article  Google Scholar 

  80. G.E. Lucas, G.R. Odette, J.W. Sheckherd, and M.K. Krishnadev:Fusion Technol., 1986, Parts 2A and 2B, vol. 10 (3), pp. 728–33.

    CAS  Google Scholar 

  81. R.A. Wullaert, D.R. Ireland, and A.S. Tetelman: ASTM STP 484, ASTM, Philadelphia, PA, 1970, p. 20.

  82. A.P. Green and B.B. Hundy:J. Mech. Phys. Solids, 1956, vol. 4, p. 128.

    Article  Google Scholar 

  83. W. Server:J. Test. Eval., 1978, vol. 6 (1), p. 29.

    Article  Google Scholar 

  84. M. Grounes: ASTM STP 426, ASTM, Philadelphia, PA, 1967, pp. 224–59.

  85. A.S. Tetelman and A.J.R. McEvily:Fracture of Structural Materials, Wiley, New York, NY, 1967.

    Google Scholar 

  86. J.R. Rice:J. Appl. Mech., 1968, vol. 35, p. 379.

    Google Scholar 

  87. 1981 Annual Book of ASTM Standards, Part 10, ASTM, Philadelphia, PA, 1981, pp. 673–92.

  88. F. Haggag and J.H. Underwood:Int. J. Fract., 1984, vol. 26, pp. R63-R65.

    Article  Google Scholar 

  89. R.O. Ritchie, G.G. Garrett, and J.F. Knott:Int. J. Fract., 1971, vol. 7, pp. 462–67.

    Article  Google Scholar 

  90. F. Huang and G.L. Wire:J. Eng. Mater. Technol., 1979, vol. 101, p. 403.

    Article  CAS  Google Scholar 

  91. F. Huang and G.L. Wire:J. Nucl. Mater., 1981, vol. 104, pp. 1511–15.

    Article  CAS  Google Scholar 

  92. F. Huang: ASTM STP 888, ASTM, Philadelphia, PA, 1986, pp. 290–304.

  93. X. Mao, H. Takahashi, and T. Shoji:J. Test. Eval., 1988, vol. 16.

  94. G.R. Odette, G.E. Lucas, R. Maiti, and J.W. Sheckherd:J. Nucl. Mater., 1986, vol. 133–134, pp. 849–52.

    Google Scholar 

  95. G.G. Chell:Met. Technol., 1977, vol. 4 (3), p. 136.

    Google Scholar 

  96. A.L. Lowe and W.A. Pavinich: ASTM STP 956, ASTM, Philadelphia, PA, 1987, pp. 358–68.

  97. F.M. Haggag, W. Server, W.G. Reuter, and J.M. Beeston: ASTM STP 870, ASTM, Philadelphia, PA, 1985, pp. 548–62.

  98. K.C. Liu and M.L. Grossbeck: ASTM STP 888, ASTM, Philadelphia, PA, 1986, pp. 276–89.

  99. H. Mizubayashi and S. Okuda: inReport of the US Japan Workshop on Small Specimen Testing Techniques, Department of Fuels and Materials Research, Japan Atomic Energy Research Institute, Ibaraki-ken, Japan, 1988, pp. 230–45.

    Google Scholar 

  100. B.A. Chin, G.R. Rao, H.T. Lin, E. Lee, M.L. Grossbeck, and S.J. Zinkle: inReport of the US Japan Workshop on Small Specimen Testing Techniques, Department of Fuels and Materials Research, Japan Atomic Energy Research Institute, Ibaraki-ken, Japan, 1988, pp. 170–79.

    Google Scholar 

  101. A.M. Ermi and L.A. James: ASTM STP 888, ASTM, Philadelphia, PA, 1986, pp. 261–75.

  102. A. Ermi and B.A. Chin:J. Nucl. Mater., 1981, vol. 103–104, pp. 1505–10.

    Article  Google Scholar 

  103. A. Ermi, R.E. Bauer, B.A. Chin, and J.L. Straalsund:J. Eng. Mater. Technol., 1981, vol. 103, pp. 240–45.

    Article  Google Scholar 

  104. R.J. Puigh, R.E. Bauer, A.M. Ermi, and B.A. Chin:J. Nucl. Mater., 1981, vol. 103–104, pp. 1501–04.

    Article  Google Scholar 

  105. G.E. Lucas, G.R. Odette, M.R. Krishnadev, M.R. Romanyi, and L. Cutler:Microstruct. Sci., 1986, vol. 13, pp. 55–73.

    CAS  Google Scholar 

  106. F.M. Haggag, W.L. Server, G.E. Lucas, G.R. Odette, and J.W. Sheckherd:Proc. Int. Conf. on Fatigue, Stress Corrosion,Fracture Mechanics, and Failure Analysis, ASM, 1985, vol. XII.

  107. D. Braski and P.J. Maziasz:J. Nucl. Mater., 1984, vol. 122–123, pp. 338–42.

    Article  Google Scholar 

  108. J.A. Conlin and J.W. Woods: inADIP Semiannual Progress Report for the Period Ending September 30, 1984, Report No. DOE/ER-0045/13, U.S. Department of Energy, Washington, DC, 1984, pp. 66–67.

    Google Scholar 

  109. N. Panayotou, S.D. Atkin, R.J. Puigh, and B.A. Chin: ASTM STP 888, ASTM, Philadelphia, PA, 1986, pp. 201–19.

  110. H.L. Heinisch, S.D. Atkin, and C. Martinez:J. Nucl. Mater., 1986, vol. 141–143, pp. 807–15.

    Article  Google Scholar 

  111. A. Kohyama, K. Asakura, and N. Igata:J. Nucl. Mater., 1986, vol. 141–143, pp. 921–25.

    Article  Google Scholar 

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This paper is based on a presentation made in the symposium “Irradiation-Enhanced Materials Science and Engineering” presented as part of the ASM INTERNATIONAL 75th Anniversary celebration at the 1988 World Materials Congress in Chicago, IL, September 25–29, 1988, under the auspices of the Nuclear Materials Committee of TMS-AIME and ASM-MSD.

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Lucas, G.E. Review of small specimen test techniques for irradiation testing. Metall Trans A 21, 1105–1119 (1990). https://doi.org/10.1007/BF02698242

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