Skip to main content
Erschienen in: Wood Science and Technology 6/2014

01.11.2014 | Original

Investigations of the pore-size distribution of wood in the dry and wet state by means of mercury intrusion porosimetry

verfasst von: Mario Zauer, Simone Hempel, Alexander Pfriem, Viktor Mechtcherine, André Wagenführ

Erschienen in: Wood Science and Technology | Ausgabe 6/2014

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

This paper deals with the determination of the pore-size distribution of untreated and thermally modified twin samples of Norway spruce (Picea abies (L.) Karst.) and sycamore maple (Acer pseudoplatanus L.) by means of mercury intrusion porosimetry. The investigations considered oven-dried and at 22 °C and 95 % relative humidity-conditioned samples. A special sample holder and a novel method for evacuation were developed for the measurements. This was necessary both to ensure that samples were positioned at a defined distance and the conditioned samples did not dry in an uncontrolled manner. The results clearly show that the climatic state influences the results. Thermal modification greatly alters the pore-size distribution of spruce. This can be largely attributed to the formation of intercellular spaces in the middle lamella as a result of cell-wall compression due to thermal modification. The alteration of the pore structure of maple due to thermal modification is not as pronounced as that of spruce.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Literatur
Zurück zum Zitat Bosshard HH (1974) Holzkunde. Mikroskopie des Holzes, Birkhäuser VerlagCrossRef Bosshard HH (1974) Holzkunde. Mikroskopie des Holzes, Birkhäuser VerlagCrossRef
Zurück zum Zitat Brischke C, Welzbacher CR, Brandt K, Rapp AO (2007) Quality control of thermally modified timber: interrelationship between heat treatment intensities and CIE L*a*b* color date on homogenized wood samples. Holzforschung 61:19–22CrossRef Brischke C, Welzbacher CR, Brandt K, Rapp AO (2007) Quality control of thermally modified timber: interrelationship between heat treatment intensities and CIE L*a*b* color date on homogenized wood samples. Holzforschung 61:19–22CrossRef
Zurück zum Zitat DIN 66133 (1993) Determination of pore volume distribution and specific surface area of solids by mercury intrusion DIN 66133 (1993) Determination of pore volume distribution and specific surface area of solids by mercury intrusion
Zurück zum Zitat DIN 52183 (1977) Testing of wood; determination of moisture content DIN 52183 (1977) Testing of wood; determination of moisture content
Zurück zum Zitat Fengel D (1966) Über die Veränderungen des Holzes und seiner Komponenten im Temperaturbereich bis 200°C—Dritte Mitteilung: thermisch und mechanisch bedingte Strukturänderungen bei Fichtenholz. Holz Roh Werkst 24:529–536CrossRef Fengel D (1966) Über die Veränderungen des Holzes und seiner Komponenten im Temperaturbereich bis 200°C—Dritte Mitteilung: thermisch und mechanisch bedingte Strukturänderungen bei Fichtenholz. Holz Roh Werkst 24:529–536CrossRef
Zurück zum Zitat Fengel J, Wegener G (2003) Wood: chemistry, ultrastructure. Reaction, Verlag Kessel Fengel J, Wegener G (2003) Wood: chemistry, ultrastructure. Reaction, Verlag Kessel
Zurück zum Zitat Griffin DM (1977) Water potential and wood-decay fungi. Annu Rev Phytopathol 15:319–329CrossRef Griffin DM (1977) Water potential and wood-decay fungi. Annu Rev Phytopathol 15:319–329CrossRef
Zurück zum Zitat Hill CAS (2006) Wood Modification: chemical, thermal and other processes. Wiley, ChichesterCrossRef Hill CAS (2006) Wood Modification: chemical, thermal and other processes. Wiley, ChichesterCrossRef
Zurück zum Zitat Hösli JP, Orfila C (1985) Mercury porosimetric approach on the validity of Darcy’s law in the axial penetration of wood. Wood Sci Technol 19:347–352 Hösli JP, Orfila C (1985) Mercury porosimetric approach on the validity of Darcy’s law in the axial penetration of wood. Wood Sci Technol 19:347–352
Zurück zum Zitat ISO 15901-1 (2005) Pore size distribution and porosity of solid materials by mercury porosimetry and gas adsorption—Part 1: mercury porosimetry ISO 15901-1 (2005) Pore size distribution and porosity of solid materials by mercury porosimetry and gas adsorption—Part 1: mercury porosimetry
Zurück zum Zitat Junghans K, Niemz P, Bächle F (2005) Investigations into the influence of thermal treatment on the porosity of spruce (In German). Holz Roh Werkst 63:243–244CrossRef Junghans K, Niemz P, Bächle F (2005) Investigations into the influence of thermal treatment on the porosity of spruce (In German). Holz Roh Werkst 63:243–244CrossRef
Zurück zum Zitat Pétrissans M, Gérardin P, El bakali I, Serraj M (2003) Wettability of heat-treated wood. Holzforschung 57:301–307CrossRef Pétrissans M, Gérardin P, El bakali I, Serraj M (2003) Wettability of heat-treated wood. Holzforschung 57:301–307CrossRef
Zurück zum Zitat Pfriem A (2011) Alteration of water absorption coefficient of spruce (Picea abies (L.) Karst.) due to thermal modification. Drvna Ind 62:311–313CrossRef Pfriem A (2011) Alteration of water absorption coefficient of spruce (Picea abies (L.) Karst.) due to thermal modification. Drvna Ind 62:311–313CrossRef
Zurück zum Zitat Pfriem A, Zauer M, Wagenführ A (2009) Alteration of the pore structure of spruce (Picea abies (L.) Karst.) and maple (Acer pseudoplatanus L.) due to thermal treatment as determined by helium pycnometry and mercury intrusion porosimetry. Holzforschung 63:94–98CrossRef Pfriem A, Zauer M, Wagenführ A (2009) Alteration of the pore structure of spruce (Picea abies (L.) Karst.) and maple (Acer pseudoplatanus L.) due to thermal treatment as determined by helium pycnometry and mercury intrusion porosimetry. Holzforschung 63:94–98CrossRef
Zurück zum Zitat Plötze M, Niemz P (2011) Porosity and pore size distribution of different wood types as determined by mercury intrusion porosimetry. Eur J Wood Prod 69:649–657CrossRef Plötze M, Niemz P (2011) Porosity and pore size distribution of different wood types as determined by mercury intrusion porosimetry. Eur J Wood Prod 69:649–657CrossRef
Zurück zum Zitat Scheiding W (2014) Introduction. Proceedings of 8th European TMT-Workshop, Dresden, Germany. pp 15–20 Scheiding W (2014) Introduction. Proceedings of 8th European TMT-Workshop, Dresden, Germany. pp 15–20
Zurück zum Zitat Schneider A (1979) Analysing the porosity of wood with the mercury porosimeter (In German). Holz Roh Werkst 37:295–302CrossRef Schneider A (1979) Analysing the porosity of wood with the mercury porosimeter (In German). Holz Roh Werkst 37:295–302CrossRef
Zurück zum Zitat Schneider A (1982) Investigations on the pore structure of particleboard by means of mercury porosimetry (In German). Holz Roh Werkst 40:415–420CrossRef Schneider A (1982) Investigations on the pore structure of particleboard by means of mercury porosimetry (In German). Holz Roh Werkst 40:415–420CrossRef
Zurück zum Zitat Schneider A (1983) Investigations on the suitability of mercury porosimetry for the evaluation of wood impregnability (In German). Holz Roh Werkst 41:101–107CrossRef Schneider A (1983) Investigations on the suitability of mercury porosimetry for the evaluation of wood impregnability (In German). Holz Roh Werkst 41:101–107CrossRef
Zurück zum Zitat Schneider A, Wagner L (1974) Determination of pore size distribution in wood with a mercury porosimeter (In German). Holz Roh Werkst 32:216–224CrossRef Schneider A, Wagner L (1974) Determination of pore size distribution in wood with a mercury porosimeter (In German). Holz Roh Werkst 32:216–224CrossRef
Zurück zum Zitat Scholz G, Zauer M, Van den Bulcke J, Van Loo D, Pfriem A, Van Acker J, Militz H (2010) Investigation on wax-impregnated wood. Part 2: study of void spaces filled with air by He pycnometry, Hg intrusion porosimetry, and 3D X-ray imaging. Holzforschung 64:587–593 Scholz G, Zauer M, Van den Bulcke J, Van Loo D, Pfriem A, Van Acker J, Militz H (2010) Investigation on wax-impregnated wood. Part 2: study of void spaces filled with air by He pycnometry, Hg intrusion porosimetry, and 3D X-ray imaging. Holzforschung 64:587–593
Zurück zum Zitat Siau JF (1995) Wood: influence of moisture on physical properties. Dept. of Wood Science and Forest Products, Virginia Polytechnic Institute and State University, Blacksburg Siau JF (1995) Wood: influence of moisture on physical properties. Dept. of Wood Science and Forest Products, Virginia Polytechnic Institute and State University, Blacksburg
Zurück zum Zitat Stayton CL, Hart CA (1965) Determining pore size distribution in softwoods with mercury porosimeter. Forest Prod J 15:435–440 Stayton CL, Hart CA (1965) Determining pore size distribution in softwoods with mercury porosimeter. Forest Prod J 15:435–440
Zurück zum Zitat Thygesen LG, Engelund ET, Hoffmeyer P (2010) Water sorption in wood and modified wood at high values of relative humidity. Part I: results for untreated, acetylated, and furfurylated Norway spruce. Holzforschung 64:315–323CrossRef Thygesen LG, Engelund ET, Hoffmeyer P (2010) Water sorption in wood and modified wood at high values of relative humidity. Part I: results for untreated, acetylated, and furfurylated Norway spruce. Holzforschung 64:315–323CrossRef
Zurück zum Zitat Trenard Y (1980) Comparison and interpretation of porosimeter curves obtained on some wood species. (In French). Holzforschung 34:139–146CrossRef Trenard Y (1980) Comparison and interpretation of porosimeter curves obtained on some wood species. (In French). Holzforschung 34:139–146CrossRef
Zurück zum Zitat Wagenführ R (1999) Anatomie des Holzes. DRW-Verlag, Leinfelden-Echterdingen Wagenführ R (1999) Anatomie des Holzes. DRW-Verlag, Leinfelden-Echterdingen
Zurück zum Zitat Wagenführ R (2007) Holzatlas. Carl Hanser Verlag, München Wagenführ R (2007) Holzatlas. Carl Hanser Verlag, München
Zurück zum Zitat Washburn EW (1921) The dynamics of capillary flow. Phys Rev 17:273–283CrossRef Washburn EW (1921) The dynamics of capillary flow. Phys Rev 17:273–283CrossRef
Zurück zum Zitat Windeisen E, Strobel C, Wegener G (2007) Chemical changes during the production of thermo-treated beech wood. Wood Sci Technol 41:523–536CrossRef Windeisen E, Strobel C, Wegener G (2007) Chemical changes during the production of thermo-treated beech wood. Wood Sci Technol 41:523–536CrossRef
Zurück zum Zitat Yamauchi T (2007) A method to determine lumen volume and collapse degree of pulp fibers by using bottleneck effect of mercury porosimetry. J Wood Sci 53:516–519CrossRef Yamauchi T (2007) A method to determine lumen volume and collapse degree of pulp fibers by using bottleneck effect of mercury porosimetry. J Wood Sci 53:516–519CrossRef
Zurück zum Zitat Zauer M (2011) Untersuchung zur Porenstruktur und kapillaren Wasserleitung im Holz und deren Änderung infolge einer thermischen Modifikation. Doctoral thesis, TU Dresden Zauer M (2011) Untersuchung zur Porenstruktur und kapillaren Wasserleitung im Holz und deren Änderung infolge einer thermischen Modifikation. Doctoral thesis, TU Dresden
Zurück zum Zitat Zauer M, Pfriem A (2009) Investigation of the pore structure of wood using nitrogen pycnometry and mercury intrusion porosimetry, Proceedings of the Workshop COST Action FP 0802 “Experimental and computational methods in wood micromechanics”, Vienna, Austria Zauer M, Pfriem A (2009) Investigation of the pore structure of wood using nitrogen pycnometry and mercury intrusion porosimetry, Proceedings of the Workshop COST Action FP 0802 “Experimental and computational methods in wood micromechanics”, Vienna, Austria
Zurück zum Zitat Zauer M, Pfriem A, Wagenführ A (2013) Toward improved understanding of the cell-wall density and porosity of wood determined by gas pycnometry. Wood Sci Technol 47:1197–1211CrossRef Zauer M, Pfriem A, Wagenführ A (2013) Toward improved understanding of the cell-wall density and porosity of wood determined by gas pycnometry. Wood Sci Technol 47:1197–1211CrossRef
Zurück zum Zitat Zauer M, Kretzschmar J, Großmann L, Pfriem A, Wagenführ A (2014a) Analysis of the pore-size distribution and fiber saturation point of native and thermally modified wood using differential scanning calorimetry. Wood Sci Technol 48:177–193CrossRef Zauer M, Kretzschmar J, Großmann L, Pfriem A, Wagenführ A (2014a) Analysis of the pore-size distribution and fiber saturation point of native and thermally modified wood using differential scanning calorimetry. Wood Sci Technol 48:177–193CrossRef
Zurück zum Zitat Zauer M, Prinz C, Emmerling F, Wagenführ A (2014b) Influence of thermal modification of wood on its sorption surface. Proceedings of 10th International Symposium on the Characterization of Porous Solids (COPS-X), Granada, Spain Zauer M, Prinz C, Emmerling F, Wagenführ A (2014b) Influence of thermal modification of wood on its sorption surface. Proceedings of 10th International Symposium on the Characterization of Porous Solids (COPS-X), Granada, Spain
Metadaten
Titel
Investigations of the pore-size distribution of wood in the dry and wet state by means of mercury intrusion porosimetry
verfasst von
Mario Zauer
Simone Hempel
Alexander Pfriem
Viktor Mechtcherine
André Wagenführ
Publikationsdatum
01.11.2014
Verlag
Springer Berlin Heidelberg
Erschienen in
Wood Science and Technology / Ausgabe 6/2014
Print ISSN: 0043-7719
Elektronische ISSN: 1432-5225
DOI
https://doi.org/10.1007/s00226-014-0671-y

Weitere Artikel der Ausgabe 6/2014

Wood Science and Technology 6/2014 Zur Ausgabe