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S solution. ZnS nanoparticles were synthesized under ultrasonic radiation. They were studied by X-ray diffraction (XRD), transmission electron microscopy (TEM), UV spectrophotometry, and X-rayphotoelectron spectrometry (XPS). XRD revealed that the ZnS nanoparticles prepared have a zincblende structure. TEM observations showed that the ZnS nanoparticles are in a spherical form with an average diameter of 40 nm. XPS results proved that, for our sample, the binding energies of Zn 2p and S 2p are the same as those of bulk single-crystal, but the full widths at half maximum of the XPS peaks are larger than those of bulk single-crystal.
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Received: 22 September 1997/Accepted: 5 January 1998
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Xu, J., Ji, W., Lin, J. et al. Preparation of ZnS nanoparticles by ultrasonic radiation method . Appl Phys A 66, 639–641 (1998). https://doi.org/10.1007/s003390050725
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DOI: https://doi.org/10.1007/s003390050725