nach oben

Cellulose

Erschienen in:

01.04.2011

Jute as raw material for the preparation of microcrystalline cellulose

verfasst von: M. Sarwar Jahan, Abrar Saeed, Zhibin He, Yonghao Ni

Erschienen in: Cellulose | Ausgabe 2/2011

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config

KI-gestützte Suche

Aus

Abstract

Cellulose was extracted at a yield of 59.8% from jute fibres based on the formic acid/peroxyformic acid process at an atmospheric pressure. The amounts of dissolved lignin and hemicelluloses were determined in the spent liquor. The results showed that the spent liquor contained 10.6% total sugars and 10.9% lignin (based on jute). Microcrystalline cellulose (MCC) was further prepared from the jute cellulose based on the acid hydrolysis technique. A very high yield, 48–52.8% (based on the jute raw material) was obtained. The acid hydrolysate of cellulose contained 2.7% glucose and 0.2% xylose. The MCC samples obtained from two different conditions, one at a low acidity and the other at a high acidity, were characterized by means of Thermo Gravimetric Analysis, Fourier Transform Infrared, X-ray detraction, Scanning Electron Micrograph, and Transmission Electron Micrograph techniques.

Vorheriger Artikel Effect of pre-acid-hydrolysis treatment on morphology and properties of cellulose nanowhiskers from coconut husk

Nächster Artikel Probing palaeoclimatology through quantitation by mass spectrometry of the products of enzyme hydrolysis of α-cellulose

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

über 67.000 Bücher
über 390 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Maschinenbau + Werkstoffe

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

über 102.000 Bücher
über 537 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Finance + Banking
Management + Führung
Marketing + Vertrieb
Maschinenbau + Werkstoffe
Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Alemdar A, Sain M (2008) Isolation and characterization of nanofibres from agricultural residues—wheat straw and soy hulls. Bioresour Technol 99(6):1664–1671CrossRef

Amidon TE, Christopher DW, Shupe AM, Wang Y, Graves M, Liu S (2008) Biorefinery: conversion of woody biomass to chemicals, energy and materials. J Biobased Mater Bioenergy 2(2):100–120CrossRef

Amidon TE, Liu S (2009) Water-based woody biorefinery. Biotechnol Adv 27(5):542–550CrossRef

Andersson S, Serimaa R, Paakkari T, Pekka S, Pesonen E (2003) Crystallinity of wood and the size of cellulose crystallites in Norway spruce (Picea abies). J Wood Sci 49(6):1435

Batitista OA (1975) Microcrystal polymer science. McGraw Hill, New York, p 17

Bhatnagar A, Sain M (2005) Processing of cellulose nanofiber-reinforced composites. J Reinforced Plast Compos 24:1259–1268

Bothast RJ, Nichols NN, Dien BS (1999) Fermentations with new recombinant organisms. Biotechnol Prog 15:867–875CrossRef

Cao Y, Tan H (2004) Structural characterization of cellulose with enzymatic treatment. J Mole Struct 705(1–3):189–193CrossRef

Cetin NS, Ozmen NU (2002) Use of organosolv lignin in phenol-formaldehyde resins for particleboard production I. Organosolv lignin modified resins. Int J Adhes Adhesives 22(6):477–480CrossRef

Chambost V, Mcnutt J, Stuart PR (2008) Guided tour: implementing the forest biorefinery (FBR) at existing pulp and paper mills. Pulp Paper Canada 109(7):1–9

Chandrakant P, Bisaria VS (1998) Simultaneous bioconversion of cellulose and hemicellulose to ethanol. Crit Rev Biotechnol 18:295–331CrossRef

Dong XM, Revol J-F, Gray DG (1998) Effect of microcrystallite preparation conditions on the formation of colloid crystals of cellulose. Cellulose 5(1):19–32CrossRef

Eichhorn SJ, Young RJ (2001) The Young’s modulus of a microcrystalline cellulose. Cellulose 8:197–207CrossRef

Fahma F, Iwamoto S, Hori N, Twata T, Takemura A (2010) Isolation, preparation, and characterization of nanofibers from oil palm empty-fruit-bunch (OPEFB). Cellulose 17:977–985CrossRef

Fengel D, Wegener G (1989) Wood chemistry, ultrastructure, reactions, Paperback edition edn. Walter de Gruyter, Berlin

Gassan J, Bledzki A (2001) Thermal degradation of flax and jute fibers. J Appl Polym Sci 82:1417–1422CrossRef

He Z, Ni Y, Zhang E (2004a) Further understanding on the cationic demand of dissolved substances during peroxide bleaching of a Spruce TMP. J Wood Chem Technol 24(2):153–168CrossRef

He Z, Ni Y, Zhang E (2004b) Alkaline darkening and its relationship to peroxide bleaching of mechanical pulp. J Wood Chem Technol 24(2):1–12

He Z, Ni Y, Zhang E (2005) Further understanding on the sodium borohydride assisted peroxide bleaching of mechanical pulps (the P-R process). Appita J 58(1):72–76

Hermans PH, Weidinger A (1950) Quantitative investigation of X-ray diffraction by “amorphous” polymers and some other noncrystalline substances. J Polymer Sci 5:269–281CrossRef

Jahan MS (2009) Studies on the effect of prehydrolysis and amine in cooking liquor on producing dissolving pulp from jute (Corchorus capsularis). Wood Sci Technol 43:213–224CrossRef

Jahan MS, Mun SP (2009) Isolation and characterization of lignin from tropical and temperate hardwood. Bangladesh J Sci Ind Res 44(3):271–280

Jahan MS, Chowdhury DAN, Islam MK, Islam MS (2007a) Organic pulping of jute and its mechanism. Cellulose Chem Technol 41(2–3):137–147

Jahan MS, Chowdhury DAN, Islam MK (2007b) Atmospheric formic acid pulping and TCF bleaching of dhaincha (Sesbania aculeata), kash (Saccharum spontaneum) and banana stem (Musa Cavendish). Ind Crop Prod 26(3):324–331CrossRef

Jahan MS, Chowdhury DAN, Islam MK (2007c) Pulping of dhaincha (Sesbania aculeata). Cellulose Chem Technol 41:413–421

Jahan MS, Maruf AA, Quaiyyum MA (2007d) Comparative studies of pulping of jute fiber, jute cutting and jute caddis. Bangladesh J Sci Ind Res 42(4):425–434

Jahan MS, Saeed A, Ni Y, He Z (2009) Pre-extraction and its impact on the alkaline pulping of bagasse. J Biobased Mater Bioenergy 3(4):380–385CrossRef

Jimenez L, Torre M, Maestre J, Ferrer Perez F (1998) Delignification of wheat straw by use of low molecular weight organic acid. Holzforschung 52(2):191–196CrossRef

Kham L, Bigot YE, Delmas M, Avignon G (2005) Delignification of wheat straw using a mixture of carboxylic acids and peroxoacids. Ind Crops Prod 21:9–15

Kubo S, Uraki Y, Sano Y (1998) Preparation of carbon fibers from softwood lignin by atmospheric acetic acid pulping. Carbon 36(7–8):1119–1124CrossRef

Lam HQ, Bigot YL, Delmas M, Avignon G (2001) Formic acid pulping of rice straw. Ind Crop Prod 14:65–71CrossRef

Lee SY, Mohan DJ, Kang IA, Doh GH, Lee S, Han SK (2009) Nanocellulose reinforced PVA composite films: effects of acid treatment and filler loading. Fibers Polym 10(1):77–82CrossRef

Leonard YM, Martin PA (2002) Chemical modification of hemp, sisal, jute, and kapok fibers by alkalization. J Appl Polymer Sci 84:2222–2234CrossRef

Leschinnsky M, Sixta H, Patt R (2009) Detailed mass balances of the autohydrolysis of Eucalyptus globulus at 170 °C. BioRes 4(2):687–703

Li H, Saeed A, Jahan MS, Ni Y, van Heiningen ARP (2010) Hemicellulose removal from hardwood chips in the pre-hydrolysis step of the kraft-based dissolving pulp production. J Wood Chem Technol 30(1):48–60CrossRef

Liu Z, Fatehi P, Jahan MS, Ni Y (2010) Separation of lignocellulosic materials by combined processes of pre-hydrolysis and ethanol extraction. doi:10.1016/j.biortech.2010.08.049

Mathew AP, Oksman K, Sain M (2005) Mechanical properties of biodegradable composites from poly lactic acid (PLA) and microcrystalline vellulose (MCC). J Appl Polym Sci 97:2014–2025CrossRef

Moran JI, Alvarez VA, Cyras VP, Vazquez A (2008) Extraction of cellulose and preparation of nanocellulose from sisal fibers. Cellulose (Dordrecht, Netherlands) 15(1):149–159

Muurinen E (2000) Organosolv pulping—a review and distillation study related to peroxy acid pulping. Ph.D Thesis, Faculty of Technology, University of Oulu, Finland

Oh SY, Dong YI, Younsook S, Gon S (2005) FTIR analysis of cellulose treated with sodium hydroxide and carbon dioxide. Carbohydr Res 340(3):417–428CrossRef

Pan X, Sano P (2005) Fractionation of wheat straw by atmospheric acetic acid process. Bioresour Technol 96:1256–1263CrossRef

Ragauskas AJ, Nagy M, Kim DH, Eckert CA, Hallett JP, Liotta CL (2006) From wood to fuels: integrating biofuels and pulp production. Ind Biotechnol 2(1):55–65CrossRef

Ray PK (1969) On the degree of crystallinity in jute and mesta fibers in different states of purifications and moisture conditions. J Appl Polym Sci 13(12):2593–2600CrossRef

Poppius K, Mustonen R, Huovila T, Sundquist J (1991) Milox pulping with acetic acid/peroxy acid. Paperi ja Puu 73(2):154–158

Sain M, Panthapulakkal S (2006) Bioprocess preparation of wheat straw fibers and their characterization. Ind Crop Prod 23(1):1–8CrossRef

Sakurada I, Nukushina Y, Ito T (1962) Experimental determination of the elastic modulus of crystalline regions of oriented polymers. J Polym Sci 57:651–660CrossRef

Samir ASA, Alloin F, Dufresne A (2005) Review of recent research into cellulosic whiskers, their properties and their application in nanocomposite field. Biomacromolecules 6:612–626CrossRef

Samir ASA, Alloin F, Paillet M, Dufresne A (2004) Tangling effect in fibrillated cellulose reinforced nanocomposites. Macromolecules 37:4313–4316CrossRef

Satheesh MNK, Mohanty AK, Erickson L, Misra M (2009) Lignin and its applications with polymers. J Biobased Mater Bioenergy 3(1):1–24

Sedlak M, Ho YWN (2004) Production of ethanol from cellulosic biomass hydrolysates using genetically engineered saccharomyces yeast capable of cofermenting glucose and xylose. Appl Biochem Biotechnol 114(1–3):403–416CrossRef

Seisto A, Poppius KL (1997) Peroxyformic acid pulping of nonwood plants by the milox method—part 1: pulping and bleaching. Tappi J 80(9):215–221

Sugiama J, Persson J, Chanzy H (1991) Combined infrared and electron diffraction study of the polymerization of native cellulose. Macromolecules 24:2461–2466CrossRef

Sun XF, Xu F, Sun RC, Fowler P, Baird MS (2005) Characteristics of degraded cellulose obtained from steam-exploded wheat straw. Carbohydr Res 340(1):97–106CrossRef

Sun Y, Lin L, Deng H, Li J, He B, Sun R, Ouyang P (2008) Structural changes of bamboo cellulose in formic acid. BioResources 3(2):297–315

van Heiningen ARP (2006) Converting a kraft pulp mill into an integrated forest biorefinery. Pulp Paper Canada 107(6):38–43

Wang H, Li H, Lu Y (2009) Preparation and characterization of micro- and nano-fibrils from jute. Fibers Polym 10(4):442–445CrossRef

Wang L, Han G, Zhang Y (2007) Comparative study of composition, structure and properties of Apocynum venetum fibers under different pretreatments. Carbohydr Polym 69(2):391–397CrossRef

Yang H, Yan R, Chen H, Dong HL, Zheng C (2007) Characteristics of hemicellulose, cellulose and lignin pyrolysis. Fuel 86:1781–1788CrossRef

Yoon SH, MacEwan K, van Heiningen A (2008) Hot-water pre-extraction from loblolly pine (Pinus taeda) in an integrated forest products biorefinery. Tappi J 7:27–31

Yu X, Atalla RH (1998) A staining technique for evaluating the pore structure variations of micricrystalline cellulose powders. Powder Technol 98:135–138CrossRef

Titel: Jute as raw material for the preparation of microcrystalline cellulose
verfasst von: M. Sarwar Jahan
Abrar Saeed
Zhibin He
Yonghao Ni
Publikationsdatum: 01.04.2011
Verlag: Springer Netherlands
Erschienen in: Cellulose / Ausgabe 2/2011
Print ISSN: 0969-0239
Elektronische ISSN: 1572-882X
DOI: https://doi.org/10.1007/s10570-010-9481-z

Springer Professional

Abstract

Bitte loggen Sie sich ein, um Zugang zu Ihrer Lizenz zu erhalten.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Technik"

Springer Professional "Wirtschaft+Technik"

Weitere Artikel der Ausgabe 2/2011

Application of the crystalline volume fraction for characterizing the ultrastructural organization of wood

Decolourization of vat dyes on cotton fabric with infrared laser light

Isolation and characterization of the cellulose synthase genes PpCesA6 and PpCesA7 in Physcomitrella patens

Neutron crystallographic and molecular dynamics studies of the structure of ammonia-cellulose I: rearrangement of hydrogen bonding during the treatment of cellulose with ammonia

Physical and chemical analysis of plasma-treated cotton fabric subjected to wrinkle-resistant finishing

N-(2-(2-Pyridyl)ethyl)chitosan (PEC) for Pd(II) and Pt(IV) sorption from HCl solutions