Skip to main content
Log in

Micro-computer tomography—An aid in the investigation of structural changes in lead zirconate titanate ceramics after temperature-humidity bias testing

  • Published:
Journal of Electroceramics Aims and scope Submit manuscript

Abstract

Lead zirconate titanate ceramic actuators are extensively used in electronic and electro-mechanical devices. Under humid conditions with a d.c. bias leakage currents increase power consumption In some materials the increasing leakage current is accompanied by the evolution of features on the anode surface, but little is known of any changes to the internal structure of the material. This research applies an advanced imaging technique (micro-computer tomography) to non-destructively investigate these features. This allows the evolution of internal features over time to be studied. The findings reveal that the microstructure of the ceramic was significantly altered during environmental testing.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5

Similar content being viewed by others

References

  1. B. Andersen, et al, in Actuator 2004, Bremen, June 2004, p. 64.

  2. J. Pritchard, C.R. Bowen, F. Lowrie, Br. Ceram. Trans. 100, 265 (2001) doi:10.1179/096797801681549

    Article  CAS  Google Scholar 

  3. H.H.A. Krueger, D. Berlincourt, J. Acoust. Soc. Am. 33, 1339 (1961) doi:10.1121/1.1908435

    Article  ADS  Google Scholar 

  4. M.G. Cain, M. Stewart, M.G. Gee, Degradation of Piezoelectric Materials (National Physical Laboratory, Teddington, 1999)

    Google Scholar 

  5. G.B. Hounsfield, A Method of and apparatus for examination of a body by radiation such as X or Gamma radiation, in, Great Britian (1972).

  6. G.N. Hounsfield, Br. J. Radiol. 46, 1016 (1973)

    Article  PubMed  CAS  Google Scholar 

  7. D. Braz, L.M.G. da Motta, R.T. Lopes, Appl. Radiat. Isot. 50, 661 (1999), doi:10.1016/S0969–8043(98)00122–5

    Article  CAS  Google Scholar 

  8. A.C. Kak, Proc. IEEE 67, 1245 (1979), doi:10.1109/PROC.1979.11440

    Article  Google Scholar 

  9. P.E. Sinnett-Jones, M. Browne, W. Ludwig, J.Y. Buffiere, I. Sinclair, Biomaterials. 26, 6460 (2005), doi:10.1016/j.biomaterials.2005.04.064

    Article  PubMed  CAS  Google Scholar 

  10. I. P. Lipscomb, P. M. Weaver, J. Swingler, J. W. McBride, Sens. Actuators 142, 2 (2008)

    Article  CAS  Google Scholar 

  11. F.H. Kreuger, U. Fromm, Jpn. J. Appl. Phys. Part 1—Regular Papers Short Notes & Review Papers 33, 1079 (1994)

    CAS  Google Scholar 

  12. X.H. Zhang, F. Rong, Z.K. Jia, F.J. Ke, M.F. Xia, Y.L. Bai, Theor. Appl. Fract. Mech. 41, 381 (2004) doi:10.1016/j.tafmec.2003.11.020

    Article  CAS  Google Scholar 

  13. C.F. Gao, N. Noda, Appl. Phys. Lett. 86 (2005)

  14. M. Goldman, A. Goldman, J. Gatellet, IEE Proc. Sci. Meas. Technol. 142, 11 (1995) doi:10.1049/ip-smt:19951633

    Article  CAS  Google Scholar 

  15. P.J. Withers, Mater. Today. 10, 26 (2007) doi:10.1016/S1369–7021(07)70305-X

    Article  CAS  Google Scholar 

  16. H. Tsuritani, T. Sayama, K. Uesugi, T. Takayanagi, T. Mori, J. Electron. Packaging 129, 434 (2007) doi:10.1115/1.2804093

    Article  CAS  Google Scholar 

Download references

Acknowledgement

This project (APAHOE) is co-funded by the Technology Strategy Board's Collaborative Research and Development programme, following an open competition (www.innovateuk.org). The authors would also like to thank project partner NPL Ltd, and Diameter Ltd for their contribution.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to I. P. Lipscomb.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Lipscomb, I.P., Weaver, P.M., Swingler, J. et al. Micro-computer tomography—An aid in the investigation of structural changes in lead zirconate titanate ceramics after temperature-humidity bias testing. J Electroceram 23, 72–75 (2009). https://doi.org/10.1007/s10832-008-9537-8

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10832-008-9537-8

Keywords

Navigation