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Synthesis and Characterization of Nickel Oxide Nanoparticles from Ni(salen) as Precursor

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Abstract

Nickel oxide nanoparticles have been synthesized by thermal treatment of N,N′-(bis(salicylidene)-ethylene-1,2-diamine)Nickel(II); [Ni(salen)]; as precursor which has been synthesized via two methods: [Ni(salen)] were obtained by solid state reaction in absence solvent and co-precipitation reaction in presence of propanol as solvent, respectively. Nickel oxide nanoparticles were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and Fourier transform infrared spectroscopy.

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Acknowledgments

The authors are grateful to the council of Iran National Science Foundation and University of Kashan for supporting this work by Grant No. (159271/16).

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Correspondence to Masoud Salavati-Niasari.

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Khansari, A., Enhessari, M. & Salavati-Niasari, M. Synthesis and Characterization of Nickel Oxide Nanoparticles from Ni(salen) as Precursor. J Clust Sci 24, 289–297 (2013). https://doi.org/10.1007/s10876-012-0521-8

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  • DOI: https://doi.org/10.1007/s10876-012-0521-8

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